A kind of skin care scrub and preparation method thereof
A technology of scrub and carbonized powder, which is applied in the field of skin cleansing products, can solve the problems of poor scrubbing effect, no antibacterial, dirt absorption, complex scrub formula and other problems of whitening scrub, achieving unique formula, excellent affinity, Easy to prepare
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Embodiment 1
[0026] The preparation method of the skin care scrub in the present embodiment comprises the following steps.
[0027] (1) Silkworm cocoons are peeled off and pupae removed to obtain the cocoon layer. With a mass percentage of 0.5% Na 2 CO 3 Scouring the cocoon layer with aqueous solution twice, 30 minutes each time, the scouring temperature is 100°C, and the liquor ratio is 1:100. After scouring, it is fully washed with distilled water and dried naturally to obtain silk fiber. With 50% CaCl by mass percentage 2 The aqueous solution dissolves the silk fiber, the dissolution temperature is 98°C, the bath ratio is 1:25, and the time is 5 minutes. The solution obtained after dissolving is poured into a cellulose dialysis membrane (molecular component 12,000-14,000), and dialyzed in running water for 3 days. The dialyzed solution was air-dried and concentrated to obtain an aqueous silk fibroin solution. Add water-soluble sericin (molecular weight 2×103 ), to a water-soluble ...
Embodiment 2
[0038] The preparation method of the skin care scrub in the present embodiment comprises the following steps.
[0039] (1) Dissolve silk fibroin fibers with calcium chloride, water and ethanol solution with a molar ratio of 1:8:2, the dissolution temperature is 70°C, the bath ratio is 1:25, and the time is 10 minutes. The solution obtained after dissolving is poured into a cellulose dialysis membrane (molecular component 12,000-14,000), and dialyzed in running water for 3 days. The dialyzed solution was air-dried and concentrated to obtain an aqueous silk fibroin solution. Add water-soluble sericin (molecular weight 5×10 3 ), to a water-soluble sericin concentration of 0.2% w / v, adding water-soluble carboxymethyl chitosan (molecular weight 5×10 4 , DSatO 0.5, DSatN 0.3), until the concentration of water-soluble carboxymethyl chitosan is 0.4% w / v, and then stand at 60°C until the solution becomes a translucent silk gel.
[0040] (2) Select new rice husks of the year, remove ...
Embodiment 3
[0054] The preparation method of the skin care scrub in the present embodiment comprises the following steps.
[0055] (1) Silkworm cocoons are peeled off and pupae removed to obtain the cocoon layer. Scouring the cocoon layer twice with 0.4% neutral soap solution by mass, 1 hour each time, the scouring temperature is 100°C, and the bath ratio is 1:100. After scouring, it is fully washed with distilled water and dried naturally to obtain silk fiber. Use a ternary solvent mixed with lithium bromide, ethanol, and water at a weight ratio of 45:53:2 to heat and dissolve silk fibroin fibers at a temperature of 60°C. The bath ratio is 1:50. The solution obtained after dissolving is poured into a cellulose dialysis membrane (molecular component 12,000-14,000), and dialyzed in running water for 3 days. The dialyzed solution was air-dried and concentrated to obtain an aqueous silk fibroin solution. Add water-soluble sericin (molecular weight 6×10 4 ), to a water-soluble sericin co...
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