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Hydrophobic expanded perlite and preparation method thereof

A technology for expanding perlite and perlite, which is applied in the field of flame retardant materials and heat preservation, can solve the problems that the water repellent cannot be uniformly dispersed and the amount of the water repellant is large, and achieve excellent waterproof effect, reduce production cost and uniform waterproof effect. Effect

Inactive Publication Date: 2014-12-10
SOUTHWEST UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] It can be seen that the existing method for preparing hydrophobic expanded perlite is simply to mix the water-repellent agent with the expanded perlite, the amount of the water-repellent agent is relatively large, and the water-repellent agent cannot be uniformly dispersed

Method used

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  • Hydrophobic expanded perlite and preparation method thereof
  • Hydrophobic expanded perlite and preparation method thereof
  • Hydrophobic expanded perlite and preparation method thereof

Examples

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Embodiment 1

[0030] The present embodiment prepares the method for hydrophobic expanded perlite, comprises the following steps:

[0031] 1), take perlite ore and silane coupling agent and fully stir and mix at room temperature;

[0032] 2) Put the mixed material at 400°C for 15-20min to dry;

[0033] 3) Put the dried material at 1100°C and roast for 3s to obtain the product.

[0034] In this example:

[0035] Step 1) The particle size of the obtained perlite ore is 20-30 mesh; the obtained silane coupling agent is vinyltriethoxysilane; the mass ratio of the perlite ore and the silane coupling agent is 1000:3;

[0036] Step 2) the moisture content of the mixed material after drying is ≤2%;

[0037] The hydrophobicity of the hydrophobic expanded perlite obtained in the present embodiment is 97%, and the bulk density is 112Kg / m 3 , The operating temperature range is -190~830℃.

Embodiment 2

[0039] The present embodiment prepares the method for hydrophobic expanded perlite, comprises the following steps:

[0040] 1), take perlite ore and silane coupling agent and fully stir and mix at room temperature;

[0041] 2) Put the mixed material at 400°C for 15-20min to dry;

[0042] 3) Put the dried material at 1100°C and roast for 3s to obtain the product.

[0043] In this example:

[0044] Step 1) The particle size of the obtained perlite ore is 20-30 mesh; the obtained silane coupling agent is octyltriethoxysilane; the mass ratio of the perlite ore and the silane coupling agent is 1000:3;

[0045] Step 2) the moisture content of the mixed material after drying is ≤2%;

[0046] The hydrophobicity of the hydrophobic expanded perlite obtained in the present embodiment is 98%, and the bulk density is 118Kg / m 3 , The operating temperature range is -180~810℃.

Embodiment 3

[0048] The present embodiment prepares the method for hydrophobic expanded perlite, comprises the following steps:

[0049] 1), take perlite ore and silane coupling agent and fully stir and mix at room temperature;

[0050] 2) Put the mixed material at 400°C for 15-20min to dry;

[0051] 3) Put the dried material at 1100°C and roast for 3s to obtain the product.

[0052] In this example:

[0053] Step 1) The particle size of the obtained perlite ore is 50-60 mesh; the obtained silane coupling agent is vinyltriethoxysilane; the mass ratio of the perlite ore and the silane coupling agent is 1000:3;

[0054] Step 2) the moisture content of the mixed material after drying is ≤2%;

[0055] The hydrophobicity of the hydrophobic expanded perlite obtained in the present embodiment is 98%, and the bulk density is 126Kg / m 3 , The operating temperature range is -170~830℃.

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Abstract

The invention discloses a method for preparing hydrophobic expanded perlite. The method comprises the steps of firstly mixing perlite ore and a silane coupling agent at the room temperature, then drying the mixture under 400-500 DEG C, and finally roasting the dried material at 1000-1300 DEG C to obtain the product, wherein the particle size of the perlite ore is less than or equal to 60 meshes, and the mass ratio of the perlite ore to the silane coupling agent is (1000:1)-(1000:5). According to the method for preparing hydrophobic expanded perlite, the hydrophobic expanded perlite is obtained by the steps of directly mixing the perlite ore and the silane coupling agent, and then carrying out medium temperature baking and high temperature roasting, the production technology and equipment are simple, and the production cost is greatly reduced; the hydrophobic rate of the expanded perlite produced according to the method disclosed by the invention is greater than or equal to 90 percent, and the expanded perlite has a uniform and excellent waterproof effect under the condition of no any hydrophobic agents, and can be used for producing heat insulation layers of building energy-saving plates and oil (gas) pipelines.

Description

technical field [0001] The invention belongs to the field of thermal insulation and flame-retardant materials, and relates to perlite products, in particular to a method for preparing hydrophobic expanded perlite and its products. Background technique [0002] Expanded perlite is a porous, white granular material made of natural perlite ore, which is crushed, screened, and calcined at high temperature. 3 ), low thermal conductivity (0.05~0.15kcal / m h ℃), wide temperature range (-200~800℃), good chemical stability (pH=7), non-toxic, tasteless, non-combustible, sound-absorbing, non-corrosive And other advantages, has been widely used in new construction, furniture decoration, petrochemical, high-grade coatings and other industries. [0003] However, the existing expanded perlite has the problem of easy water absorption, and its mass water absorption rate is usually as high as 500% to 800%, which makes expanded perlite products absorb a large amount of water during constructio...

Claims

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Application Information

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IPC IPC(8): C04B20/06
Inventor 陈久存李文君刘茵沁李长明
Owner SOUTHWEST UNIVERSITY
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