A kind of preparation method and product of micron bi4ti3o12 cuboid
A cuboid, micron-scale technology, applied in chemical instruments and methods, inorganic chemistry, bismuth compounds, etc., can solve problems such as serious agglomeration and difficulty in controlling the shape of bismuth titanate, and achieve simple preparation process, easy large-scale production, and easy control Effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0035] 1) Weigh 5.1 mmol of tetrabutyl titanate, add it dropwise into deionized water, and control the concentration of tetrabutyl titanate to 0.4 mol / L.
[0036] 2) Weigh 6.8 mmol of bismuth nitrate pentahydrate, add it into the suspension prepared in step 1), and stir thoroughly.
[0037] 3) Weigh 0.04 mol of potassium hydroxide, add to the suspension solution prepared in step 2), and stir for at least 30 minutes.
[0038] 4) Weigh 0.125 mmol polyvinyl alcohol (PVA), dissolve it in deionized water, and control the concentration of PVA to be 0.0125 mol / L.
[0039] 5) In the stirring state, add the PVA solution prepared in step 4) dropwise to the suspension prepared in step 3), and disperse through sufficient stirring and ultrasonic vibration, and then use deionized water to adjust its volume. 4 / 5 of the volume of the inner tank of the reaction kettle, and the precursor solution is obtained at this time.
[0040] 6) Add the precursor solution prepared in step 5) into the inn...
Embodiment 2
[0043] 1) Weigh 5.1 mmol of tetrabutyl titanate, add it dropwise into deionized water, and control the concentration of tetrabutyl titanate to 0.6 mol / L.
[0044] 2) Weigh 6.8 mmol of bismuth nitrate pentahydrate, add it into the suspension prepared in step 1), and stir thoroughly.
[0045] 3) Weigh 0.04 mol of potassium hydroxide, add to the suspension solution prepared in step 2), and stir for at least 30 minutes.
[0046] 4) Weigh 0.12 mmol polyvinyl alcohol (PVA), dissolve it in deionized water, and control the concentration of PVA to be 0.012 mol / L.
[0047] 5) In the stirring state, add the PVA solution prepared in step 4) dropwise to the suspension prepared in step 3), and disperse through sufficient stirring and ultrasonic vibration, and then use deionized water to adjust its volume. 4 / 5 of the volume of the inner tank of the reaction kettle, and the precursor solution is obtained at this time.
[0048] 6) Add the precursor solution prepared in step 5) into the inner t...
Embodiment 3
[0051] 1) Weigh 5.1 mmol of tetrabutyl titanate, add it dropwise into deionized water, and control the concentration of tetrabutyl titanate to 0.6 mol / L.
[0052] 2) Weigh 6.8 mmol of bismuth nitrate pentahydrate, add it into the suspension prepared in step 1), and stir thoroughly.
[0053] 3) Weigh 0.04 mol of potassium hydroxide, add to the suspension solution prepared in step 2), and stir for at least 30 minutes.
[0054] 4) Weigh 0.13 mmol polyvinyl alcohol (PVA), dissolve it in deionized water, and control the concentration of PVA to be 0.013 mol / L.
[0055] 5) In the stirring state, add the PVA solution prepared in step 4) dropwise to the suspension prepared in step 3), and disperse through sufficient stirring and ultrasonic vibration, and then use deionized water to adjust its volume. 4 / 5 of the volume of the inner tank of the reaction kettle, and the precursor solution is obtained at this time.
[0056] 6) Add the precursor solution prepared in step 5) into the inner...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More