Humectant for cigarettes and application thereof
The technology of moisturizing agent and apple for cigarettes is applied in the field of cigarette additives to achieve the effects of obvious effect, simple equipment and simple and applicable process.
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Embodiment 1
[0029] After washing the fresh apples, weigh 1000g of apples and cut them into small pieces, put them in a juicer, add 500g of water for beating, pour out the beaten apple juice, add 3000g of water to dilute the apple juice, add After adjusting the pH to 2 with dilute sulfuric acid, place it in a constant temperature water bath at 75°C for 2 hours for hydrolysis. After the hydrolysis is complete, filter while it is hot, wash the filter residue with hot water at 55°C for 3 times, collect and combine the filtrates. The combined filtrate is adjusted to filtrate pH to 5 with dilute ammonia water, and aluminum sulfate solution is slowly added dropwise, centrifuged after salting out at 55° C. and 48% water), stirred, desalted for 0.5h, filtered, added water to wash the hydrolyzed precipitate, and dried at a constant temperature of 50° C. to obtain component A with a weight of 127 g. Weigh 500g of wolfberry and crush it, add 500g of 40-60°C hot water to soak for 3 hours, filter to re...
Embodiment 2
[0031] After washing the fresh apples, weigh 1000g of apples and cut them into small pieces, then place them in a juicer, add 2000g of water for beating, pour out the beaten apple juice, then add 5000g of water to dilute the apple juice, add After adjusting the pH to 3 with dilute sulfuric acid, place it in a constant temperature water bath at 95°C for 4 hours for hydrolysis. After the hydrolysis is complete, filter while hot, wash the filter residue with hot water at 65°C for 6 times, and combine the filtrates after collection. The filtrate after merging is adjusted filtrate pH to 5 with dilute ammonia water, slowly adds aluminum sulfate solution dropwise, centrifuges after salting out at 65 ℃ for 3h, the precipitation after centrifugation is with 125ml desalination solution (2%HCl, 50% ethanol and 48% water), stirred, desalted for 4 hours, filtered, added water to wash the hydrolyzed precipitate, and dried at a constant temperature of 70° C. to obtain component 1 with a weigh...
Embodiment 3
[0033] After washing the fresh apples, weigh 1000g of apples and cut them into small pieces, put them in a juicer, add 1000g of water for beating, pour out the beaten apple juice, add 4000g of water to dilute the apple juice, add After adjusting the pH to 2.5 with dilute sulfuric acid, place it in a constant temperature water bath at 80°C for 3 hours for hydrolysis. After the hydrolysis is complete, filter while it is hot, wash the filter residue with hot water at 60°C for 5 times, collect and combine the filtrates. The combined filtrate is adjusted to filtrate pH to 5 with dilute ammonia water, and aluminum sulfate solution is slowly added dropwise, centrifuged after salting out at 60° C. and 48% water), stirred, desalted for 2 hours, filtered, added water to wash the hydrolyzed precipitate, and dried at a constant temperature of 60° C. to obtain component 1 with a weight of 109 g. Weigh 500g of wolfberry and crush it, add 500g of 50°C hot water to soak for 4 hours, filter to...
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