Preparation method of glass ceramic
A technology of glass ceramics and glass powder, which is applied in the field of glass ceramics preparation to achieve excellent optical properties and high insulation reliability
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Embodiment 1
[0031] (1) preparation comprises the first glass of following composition (mass %, by oxide):
[0032] 30% by mass of magnesium borosilicate glass powder, 30% of alumina filler powder, 30% by mass of Y 2 o 3 and 10% by mass of rare earth ion Ce / Eu, the magnesium borosilicate glass powder contains 68% by mass of SiO in terms of oxide 2 , 10 mass% B 2 o 3 , 10 mass% Al 2 o 3 , 22% by mass MgO. Wherein, the mole fractions of Ce and Eu are both 0.5%.
[0033] (2) The first heat treatment time at 650°C is 20h, and the second heat treatment time at 700°C is 68h.
[0034] According to tests, the crystallization rate of the glass phase in the ceramic sintered body obtained by sintering reaches 55% by volume ratio, and the high-refractive-index filler powder is a ceramic whose refractive index exceeds 1.95.
Embodiment 2
[0036] (1) preparation comprises the first glass of following composition (mass %, by oxide):
[0037] 32% by mass of magnesium borosilicate glass powder, 35% of alumina filler powder, 20% by mass of Y 2 o 3and 13% by mass of rare earth ion Ce / Eu mixture, the magnesium borosilicate glass powder contains 68% by mass of SiO in terms of oxide 2 , 10 mass% B 2 o 3 , 10 mass% Al 2 o 3 , 22% by mass MgO. Wherein, the molar fractions of Ce and Eu are both 1.0%.
[0038] (2) The first heat treatment time at 660°C is 22h, and the second heat treatment time at 750°C is 60h.
[0039] According to tests, the crystallization rate of the glass phase in the ceramic sintered body obtained by sintering reaches 52% by volume ratio, and the high-refractive-index filler powder is a ceramic whose refractive index exceeds 1.95.
Embodiment 3
[0041] (1) preparation comprises the first glass of following composition (mass %, by oxide):
[0042] 34% by mass of magnesium borosilicate glass powder, 38% of alumina filler powder, 16% by mass of Y 2 o 3 and 12% by mass of rare earth ions Ho / Tm / Yb, the magnesium borosilicate glass powder containing 60% by mass of SiO in terms of oxides 2 , 10 mass% B 2 o 3 , 10 mass% Al 2 o 3 , 20% by mass MgO. Wherein, the mole fractions of Ho, Tm and Yb are all 1.0%.
[0043] (2) The first heat treatment time at 680°C is 25h, and the second heat treatment time at 750°C is 70h.
[0044] According to the test, the crystallization ratio of the glass phase in the ceramic sintered body obtained by sintering reaches 53% by volume ratio, and the high-refractive-index filler powder is a ceramic whose refractive index exceeds 1.97.
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