D-phase vanadium dioxide nano-star powder and preparation method thereof
A technology of vanadium dioxide nano and vanadium dioxide powder, which is applied in the field of D-phase vanadium dioxide nano star powder and its preparation, which can solve the problems of complicated process and unfavorable application, and achieve difficult agglomeration, low production cost, and easy preparation The effect of simple method
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Embodiment 1
[0033] The concrete steps of preparation are:
[0034] Step 1: First, according to the weight ratio of 0.05:5, ammonium metavanadate was dissolved in deionized water and stirred for 0.5 h to obtain ammonium metavanadate aqueous solution. Then, 80wt% formic acid solution was added dropwise into the ammonium metavanadate aqueous solution under stirring to obtain a mixed solution with a pH value of 3.
[0035] In step 2, the mixed solution is placed in an airtight state, and reacted at 180° C. for 3 days to obtain a reaction solution. Then the reaction solution is subjected to solid-liquid separation, washing and drying in sequence; wherein, the solid-liquid separation process is centrifugation, the rotational speed and time of centrifugation are respectively 5000r / min and 10min, and the washing process is to use deionized water and ethanol to The separated solids were washed alternately for 3 times. During the cleaning, the solids were separated by centrifugation. The temperatu...
Embodiment 2
[0037] The concrete steps of preparation are:
[0038]Step 1: First, according to the weight ratio of 0.055:5, ammonium metavanadate was dissolved in deionized water and stirred for 0.6 h to obtain an ammonium metavanadate aqueous solution. Then, 83wt% formic acid solution was added dropwise into the ammonium metavanadate aqueous solution under stirring to obtain a mixed solution with a pH value of 2.5.
[0039] In step 2, the mixed solution is placed in an airtight state and reacted at 190° C. for 2.5 days to obtain a reaction solution. Then the reaction solution is subjected to solid-liquid separation, washing and drying in sequence; wherein, the solid-liquid separation process is centrifugation, the rotational speed and time of centrifugation are 6000r / min and 9min respectively, and the washing process is to use deionized water and ethanol to The separated solids were washed alternately for 3 times, and the solids were separated by centrifugation during cleaning. The tempe...
Embodiment 3
[0041] The concrete steps of preparation are:
[0042] Step 1: First, according to the weight ratio of 0.06:5, ammonium metavanadate was dissolved in deionized water and stirred for 0.75h to obtain ammonium metavanadate aqueous solution. Then, 85wt% formic acid solution was added dropwise to the ammonium metavanadate aqueous solution under stirring to obtain a mixed solution with a pH value of 2.
[0043] In step 2, the mixed solution is placed in an airtight state, and reacted at 200° C. for 2 days to obtain a reaction solution. Then the reaction solution is subjected to solid-liquid separation, washing and drying in sequence; wherein, the solid-liquid separation process is centrifugation, the rotational speed and time of centrifugation are respectively 7500r / min and 7.5min, and the washing process is to use deionized water and ethanol The separated solid matter was alternately washed 4 times, the solid matter was separated by centrifugation during washing, and the temperatu...
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