Preparation method of alcohol-soluble acrylic rosin resin
An acrylic rosin and alcohol-soluble technology, which is applied in the field of rosin processing, can solve the problems of easy volatilization, air pollution, and high printing costs, and achieve the effects of increased competitiveness, high softening point, and good alcohol solubility
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[0016] Below in conjunction with example, the present invention is described in further detail:
[0017] A kind of preparation method of alcohol-soluble acrylic rosin resin comprises the following steps:
[0018] A. First put 210Kg of rosin into the reactor for heating, when the temperature of the rosin material reaches 150°C to 160°C, start the stirrer of the reactor, and then add 0.21Kg of 4,4`-thio Two (6-tert-butyl-3-methylphenol) reacted and continued heating;
[0019] B. When the temperature of the material in the reactor reaches 195°C to 200°C, add 15.8Kg of acrylic acid into the reactor, and seal the reactor, then react 2 at the pressure of the reactor at 0.1 MPa to 0.3 MPa Hour;
[0020] C. After the reaction described in step B is completed, the reactor is depressurized and emptied, 8.8Kg of glycerin is added, and heated to 250° C. to 255° C. for esterification for 1 hour;
[0021] D. After the reaction in step C is over, turn on the vacuum pump to evacuate the re...
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