Electrophotographic photoreceptor

A technology of electrophotography and photoreceptor, which is applied in the fields of optics, electrography, instruments, etc., can solve the problems such as difficulty in developing the sensitivity characteristics, and achieve the effect of excellent sensitivity characteristics

Inactive Publication Date: 2018-09-14
KYOCERA DOCUMENT SOLUTIONS INC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Here, in general, there is a problem that it is difficult to exhibit sufficient sensitivity characteristics when using an electron transport agent in a material contained in an organic photoreceptor.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Synthetic example 1

[0080] The naphthalimide derivative represented by the following general formula (1-2) was synthesized according to the following reaction equation 3.

[0081] [Electron Transport Agent (ETM-1)]

[0082] 【Chemical formula 8】

[0083]

[0084] [Reaction equation 3]

[0085] 【Chemical formula 9】

[0086]

[0087] In reaction equation 3(a-2), 0.875 g (1 mmol) of compound (A-12), 0.812 g (4 mmol) of 2-bromoanisole sulfide, 58 mg (0.05 mmol) of tetrakis(triphenylphosphine) palladium and iodine A toluene solution of 19 mg (0.1 mmol) of cuprous oxide was refluxed and stirred for 10 hours under a nitrogen atmosphere at a temperature of 110° C. to obtain a reaction solution.

[0088] The toluene solvent in the resulting reaction solution was distilled off and purified by column chromatography to obtain 0.6 g of compound (A-22) (yield: 85%).

[0089] In the reaction equation 3(b-2), a solution of 0.708g (1mmol) of compound (A-22), 10ml of acetic acid and 10ml of chloroform was cooled with ice, and...

Synthetic example 2

[0094] The naphthalimide derivative represented by the following general formula (1-3) is synthesized according to the following reaction equation 4.

[0095] [Electron Transport Agent (ETM-2)]

[0096] 【Chemical formula 10】

[0097]

[0098] [Reaction equation 4]

[0099] 【Chemical formula 11】

[0100]

[0101] In reaction equation 4(a-3), 0.78 g (1 mmol) of compound (A-13), 0.81 g (4 mmol) of 2-bromoanisole sulfide, 58 mg (0.05 mmol) of tetrakis(triphenylphosphine) palladium and iodine A toluene solution of 19 mg (0.1 mmol) of cuprous oxide was refluxed and stirred at a temperature of 110° C. for 10 hours under a nitrogen atmosphere to obtain a reaction solution.

[0102] The toluene solvent in the resulting reaction solution was distilled off and purified by column chromatography to obtain 0.49 g of compound (A-23) (yield: 80%).

[0103] Next, in reaction equation 4 (b-3), a solution of 0.61 g (1 mmol) of compound (A-23), 10 ml of acetic acid and 10 ml of chloroform is cooled with ice...

Synthetic example 3

[0107] The naphthalimide derivative represented by the following general formula (1-4) was synthesized according to the following reaction equation 5.

[0108] [Electron Transport Agent (ETM-3)]

[0109] 【Chemical formula 12】

[0110]

[0111] [Reaction equation 5]

[0112] 【Chemical formula 13】

[0113]

[0114] In reaction equation 5(a-4), 1.17 g (1 mmol) of compound (A-14), 1.62 g (4 mmol) of 2-bromoanisole sulfide, 58 mg (0.05 mmol) of tetrakis(triphenylphosphine) palladium and iodine A toluene solution of 19 mg (0.1 mmol) of cuprous oxide was refluxed and stirred at a temperature of 110° C. for 10 hours under a nitrogen atmosphere to obtain a reaction solution.

[0115] The toluene solvent of the obtained reaction solution was distilled off and purified by column chromatography to obtain 0.66 g of compound (A-24) (yield: 80%).

[0116] Next, in reaction equation 5(b-4), a solution of 0.83 g of compound (A-24), 10 ml of acetic acid and 10 ml of chloroform was cooled with ice, and the...

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PUM

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Abstract

An electrophotographic photosensitive member includes a photosensitive layer containing a naphthalenediimide derivative represented by the following formula (1) or (2). In the formula (1) or (2), R 1 represents an alkyl group having 1 to 10 carbon atoms, an aryl group having 6 to 12 carbon atoms and optionally having an alkyl group having 1 to 10 carbon atoms, an aralkyl group having 7 to 12 carbon atoms, a cycloalkyl group having 3 to 10 carbon atoms, or an alkoxy group having 1 to 6 carbon atoms.

Description

Technical field [0001] The invention relates to an electrophotographic photoreceptor. Background technique [0002] As an electrophotographic photoreceptor provided in an image forming apparatus or the like, an organic photoreceptor containing a binder resin, a charge generating agent, a hole transporting agent as a charge transporting agent, an electron transporting agent, and the like is known. Compared with inorganic photoreceptors using inorganic materials such as amorphous silicon, such organic photoreceptors are easier to manufacture, and because the selection of photoreceptor materials can be diversified, it has the advantage of high degree of freedom in structural design. [0003] Furthermore, in order for an image forming apparatus using an organic photoreceptor to form a high-quality image, the material contained in the organic photoreceptor in the electrophotographic photoreceptor is required to have sufficient sensitivity characteristics. [0004] Here, especially regard...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G03G5/04
CPCG03G5/0629G03G5/065G03G5/0651G03G5/0659
Inventor 冈田英树
Owner KYOCERA DOCUMENT SOLUTIONS INC
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