Acrylic emulsion adhesive composition comprising nano sized latex particles having a mono-modal particle size distribution, and production method for same
An acrylic emulsion and acrylic technology, applied in the direction of film/sheet adhesives, non-polymer adhesive additives, non-polymer organic compound adhesives, etc., can solve hardening, filtration problems, sticky High adhesive strength, high processability and productivity, and high sustainability can be achieved without problems such as reduced adhesion
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Embodiment 1
[0050] The acrylic emulsion PSA composition according to one embodiment of the present invention may be prepared through the following process.
[0051] To a 3L glass reactor equipped with a thermostat, a stirrer, a dropping funnel, a nitrogen injection tube and a reflux condenser, were added 360 g of distilled water and 5 g (30 wt %) of sodium laureth sulfate and 10 g of (30 wt%) Sodium Lauryl Sulfate. While stirring the resulting solution, the air inside the reactor was replaced with nitrogen, and the temperature therein was raised to 80° C. and maintained for 60 minutes in a nitrogen protective atmosphere.
[0052] Separately from the emulsion preparation process, to prepare a pre-emulsion, 50 g (30 wt%) sodium laureth sulfate, 15 g (60 wt %) dioctyl sodium sulfosuccinate, 2 g sodium carbonate, 2 g methylene A solution composed of sodium propylsulfonate and 300g distilled water and 330g butyl acrylate (BA) , 930g 2-ethylhexyl acrylate (2-EHA), 110g vinyl acetate, 76g acry...
Embodiment 2
[0057] An acrylic emulsion resin was prepared in the same manner as in Example 1, except that the amount of 30 wt% sodium lauryl sulfate was twice that used in the emulsion preparation process.
Embodiment 3
[0059] In addition to the amount of 30wt% sodium lauryl polyoxyethylene ether sulfate and 30wt% sodium lauryl sulfate in the surfactant is 30wt% sodium lauryl polyoxyethylene ether sulfate and 30wt% sodium lauryl sulfate used in the emulsion preparation process Except twice the amount of sodium alkyl sulfate, acrylic emulsion resin was prepared in the same manner as in Example 1.
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