High-strength high-resilience medical TPE (thermoplastic elastomer) tourniquet and preparation method thereof
A high-strength and resilient technology, applied in the field of medical TPE tourniquet and its preparation, can solve the problem of difficulty in obtaining high cross-linking density
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[0042] Another aspect of the present invention provides a method for preparing a high-strength, high-resilience tourniquet, comprising the following steps:
[0043] (1) After mixing the raw materials by weight, granulate through twin-screw extrusion;
[0044] (2) Vacuum injection molding the product obtained in step (1) into a mold at 170° C. to 200° C., and maintain the injection molding temperature for 8 hours under vacuum conditions, and then cool and solidify.
[0045] In one embodiment, the injection molding temperature in the step (2) is 195°C.
[0046] The applicant unexpectedly found that the cross-linking density of the tourniquet can be further increased by vacuum injection molding and maintaining high temperature under vacuum conditions. This is because graphene oxide contains a large number of carboxyl groups, which can undergo Friedel-Crafts acylation reaction with the benzene ring on the styrene unit in SEBS and MAH-g-SEBS under high temperature and vacuum dehyd...
Embodiment 1~8 and comparative example 1
[0067] Prepare high-strength, high-resilience medical TPE tourniquet according to the formula in the following table, and the preparation method is as follows (the consumption of the following components is all parts by weight):
[0068] (1) After mixing the raw materials by weight, granulate through twin-screw extrusion;
[0069] (2) Vacuum injection molding the product obtained in step (1) into a mold at 195° C., and maintain the injection molding temperature for 8 hours under vacuum conditions, and then cool and solidify.
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