Adhesive tape
A technology of adhesive tape and gel rate, applied in the direction of adhesive, adhesive type, film/sheet adhesive, etc., can solve the problems of weakened surface release effect, irregular mold surface, and floating of the bonding surface, etc. , to achieve the effect of increasing gel rate and molecular weight, improving work efficiency, and improving anti-reflection
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[0055] Example 1
[0056] 30 parts by weight of acrylic acid, 2.5 parts by weight of AIBN, 55 parts by weight of vinyl acetate, and 900 parts by weight of butyl acrylate were blended, and nitrogen replacement was performed for 2 hours. Under nitrogen substitution, polymerization was performed at 60°C for 6 hours to obtain an acrylic polymer (1) having a weight average molecular weight of 500,000 and a gel fraction of 45%.
[0057] 100 parts by weight of the acrylic polymer (1) and 2 parts by weight of a trifunctional isocyanate-based compound (trade name "CORONATEL", manufactured by Nippon Polyurethane Co., Ltd.) were uniformly mixed to obtain an acrylic adhesive (1).
[0058] The acrylic adhesive (1) was coated on a fluorinated ethylene-propylene polymer FEP (75 μm in thickness) as a substrate so that the thickness after drying was 30 μm, and after drying, an adhesive tape (1) was obtained.
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[0059] Example 2
[0060] 40 parts by weight of acrylic acid, 3.0 parts by weight of AIBN, 55 parts by weight of vinyl acetate, and 900 parts by weight of butyl acrylate were blended, and nitrogen replacement was performed for 2 hours. Under nitrogen substitution, polymerization was carried out at 60°C for 6 hours to obtain an acrylic polymer (2) having a weight average molecular weight of 600,000 and a gel fraction of 55%.
[0061] 100 parts by weight of the acrylic polymer (2) and 2 parts by weight of the trifunctional isocyanate-based compound (trade name "CORONATEL", manufactured by Nippon Polyurethane Co., Ltd.) were uniformly mixed to obtain an acrylic adhesive (2).
[0062] The above-mentioned acrylic adhesive (2) was coated on a fluorinated ethylene-propylene polymer FEP (75 μm in thickness) as a substrate so that the thickness after drying was 30 μm, and after drying, an adhesive tape (2) was obtained.
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[0063] Example 3
[0064] Repeat the steps of Example 1, except that the above-mentioned acrylic adhesive (1) of Example 1 is coated on the polytetrafluoroethylene PTFE (thickness of 75μm) as the base material so that the thickness after drying is 30μm. After drying, an adhesive tape (3) is obtained.
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