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Alcohol-soluble mixed solvent and production method thereof

A technology of mixing solvents and production methods, which can be used in inks, household utensils, applications, etc., can solve the problems of serious gel tendency, low gloss, poor transparency, etc., and achieve the effect of low amine value, high transparency, and clear solvent color

Inactive Publication Date: 2015-09-09
无锡市方成彩印包装有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] It is a common method to use benzene-soluble gravure surface printing products in the outer packaging industry, but it is not suitable for food outer packaging safety standards. In order to ensure food safety, it is necessary to use solvents that do not contain benzene and ketones. Alcohol-soluble polyurethane inks have been promoted in China. With the development of plastic packaging, there are still some deficiencies in the quality of domestic alcohol-soluble solvents added to inks, such as darker color, poor transparency, low gloss, serious tendency to gel, etc.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] Embodiment one: a kind of alcohol-soluble mixed solvent, it comprises alcohol solvents such as alcohol-soluble polyamide resin and isopropanol solvent or ethanol solvent, the weight ratio of alcohol-soluble polyamide resin and alcohol solvent is 2:8, alcohol-soluble polyamide resin The amide resin is composed of raw materials in the following weight proportions: 25-35 parts of dimer acid, 15-25 parts of monoacid and 35-50 parts of ethylenediamine. Specifically, 30 parts of dimer acid, 25 parts of monoacid, and 45 parts of ethylenediamine.

[0015] The production method of the above-mentioned alcohol-soluble mixed solvent: (1) weighing 30 parts of dimer acid, 25 parts of monoacid, and 45 parts of ethylenediamine as raw materials by weight, totaling 500 L;

[0016] (2) Put the weighed dimer acid, monoacid, and ethylenediamine into the reaction kettle, pump air to the pressure in the reaction kettle to 2.5MPa with a vacuum pump, and then carry out polycondensation reaction...

Embodiment 2

[0019] Embodiment two: a kind of alcohol-soluble mixed solvent, it comprises alcohol solvents such as alcohol-soluble polyamide resin and isopropanol solvent or ethanol solvent, alcohol-soluble polyamide resin and alcohol solvent weight ratio are 2:8, alcohol-soluble polyamide resin The amide resin is composed of raw materials in the following weight proportions: 25-35 parts of dimer acid, 15-25 parts of monoacid and 35-50 parts of ethylenediamine. Specifically, 35 parts of dimer acid, 25 parts of monoacid, and 40 parts of ethylenediamine.

[0020] The production method of the above-mentioned alcohol-soluble mixed solvent: (1) weighing 35 parts of raw materials dimer acid, 25 parts of monoacid, and 40 parts of ethylenediamine, totaling 500L;

[0021] (2) Put the weighed dimer acid, monoacid, and ethylenediamine into the reaction kettle, pump air with a vacuum pump until the pressure in the reaction kettle reaches 2.5MPa, and then carry out polycondensation reaction for 50 minu...

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PUM

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Abstract

The invention relates to the technical field of mixed solvents and particularly relates to an alcohol-soluble mixed solvent and a production method thereof. By the production method, the mixed solvent can be prepared conveniently. The prepared mixed solvent is clear and transparent in color, does not separate out precipitate, has excellent properties and is free of benzene and ketone to ensure the safety requirement of outer packing for foods. The mixed solvent comprises alcohol-soluble polyamide resin and an alcohol solvent which are at a weight ratio of 2:8, wherein the alcohol-soluble polyamide resin is prepared from the following raw materials in parts by weight: 25-35 parts of dimer acid, 15-25 parts of monomer acid and 35-50 parts of ethylenediamine. The production method comprises the following steps: adding weighed dimer acid, monomer acid and ethylenediamine into a reaction kettle; sucking air with a vacuum pump so that the pressure in the reaction kettle reaches 2.5MPa, and carrying out polycondensation reaction for 45min to obtain the alcohol-soluble polyamide resin; and mixing the alcohol-soluble polyamide resin with the alcohol solvent according to a weight ratio of 2:8 to obtain the alcohol-soluble mixed solvent.

Description

technical field [0001] The invention relates to the technical field of mixed solvents, in particular to an alcohol-soluble mixed solvent and a production method. Background technique [0002] At present, alcohol-soluble plastic printing has been widely promoted and popularized in Southeast Asia, Eastern Europe and other countries. [0003] It is a common method to use benzene-soluble gravure surface printing products in the outer packaging industry, but it is not suitable for food outer packaging safety standards. In order to ensure food safety, it is necessary to use solvents that do not contain benzene and ketones. Alcohol-soluble polyurethane inks have been promoted in China. With the development of plastic packaging, there are still some shortcomings in the quality of domestic alcohol-soluble solvents added to inks, such as darker color, poor transparency, low gloss, and serious tendency to gel. Contents of the invention [0004] In order to solve the above problems, ...

Claims

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Application Information

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IPC IPC(8): C09D11/033
CPCC09D11/033
Inventor 方波
Owner 无锡市方成彩印包装有限公司
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