Heat-insulating molding compound, heat-insulating molded article, and production method for same
A formed body and heat insulation technology, which is applied in the directions of heat exchange equipment, chemical instruments and methods, mechanical equipment, etc., can solve the problems of application field limitation, time-deteriorated preparation cost, and limitation of heat insulators, etc.
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[0072] Hereinafter, the present invention is specifically described with reference to Examples.
[0073] Preparation method of airgel particles
[0074] Prepare tetramethoxysilane oligomer ("methyl silicate 51", purchased from COLCOATCO., Ltd., its average molecular weight is 470) as alkoxysilane, ethanol (special grade reagent, purchased from nacalaitesqueinc.) and water As a solvent, and 0.01mol / l ammonia water as a catalyst. Mix 1 mol of tetramethoxysilane oligomer, 120 mol of ethanol, 20 mol of water and 2.16 mol of ammonia water to prepare a sol-like reaction solution.
[0075] Thereafter, the sol-like reaction solution was put into a bottle, and then left to gel at normal temperature to produce a gelled compound.
[0076] Then, put the above-mentioned gelled compound into a place filled with liquefied carbon dioxide at a temperature of 18°C and a pressure of 5.4MPa (55kgf / cm 2 ) in a pressure vessel, and the ethanol in the gelled compound was replaced by carbon diox...
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