Automatic titration method and application

An automatic titration and titration technology, which is applied in the direction of chemical analysis by titration, which can solve the problems of difference in titration end point, lack of judgment standards, and poor repeatability of rinsing test.

Active Publication Date: 2015-12-02
CHINA HOUSEHOLD ELECTRIC APPLIANCE RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The second titration method is generally used in scientific research work, and is rarely used in actual production.
[0004] Most titrators use the first titration method, but the first method has the following problems: (1) The automatic titration process is very prone to drop over the end point, because the chemical reaction has hysteresis, and the performance is different due to different solutions , often when the titrator finds that it has reached or is close to the end point, it will be difficult to grasp its speed, so in actual use, most of these automatic titrators use manual titration function, the so-called "automatic titration" is just a decoration; (2) Even if "Automatic titration" is achievable, but also lacks a unified judgment standard, that is, how long to judge after reaching the end p

Method used

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  • Automatic titration method and application

Examples

Experimental program
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Effect test

Embodiment 1

[0049] A kind of automatic titration method of embodiment 1 specifically comprises the following steps:

[0050] (1) Sampling and sample pretreatment: take the sample solution to be tested, filter it through a microporous membrane, and put it into a sample loading container;

[0051] (2) Titrator preset: After inserting the burette and pH probe into the sample container, set the pre-stirring time of the titrator to 0.5min, the delay time to 20s, the speed 1 to 1mL / min, and the speed 2 to 0.1mL / min. min, the pH value of the speed control point, the pH value of the end point and the speed control amount of 15%;

[0052] (3) Titration in the first stage: after the test starts, pre-stirring is carried out. After the pre-stirring is over, the titrator starts titration at a set speed 1 until the pH value of the sample to be tested reaches the pH value of the speed control point;

[0053] (4) Titration in the second stage: after the pH value of the sample reaches the pH value of the...

Embodiment 2

[0059] A kind of automatic titration method of embodiment 2 specifically comprises the following steps:

[0060] (1) Sampling and sample pretreatment: take the sample solution to be tested, filter it through a water-based microporous membrane, and put it into a sample loading container;

[0061] (2) Titrator preset: After inserting the burette and pH probe into the sample container, set the pre-stirring time of the titrator to 2min, delay time to 30s, speed 1 to 3mL / min, speed 2 to 1mL / min, The pH value of the speed control point, the pH value of the end point and the speed control amount of 50%;

[0062] (3) Titration in the first stage: after the test starts, pre-stirring is carried out. After the pre-stirring is over, the titrator starts titration at a set speed 1 until the pH value of the sample to be tested reaches the pH value of the speed control point;

[0063] (4) Titration in the second stage: after the pH value of the sample reaches the pH value of the speed contro...

Embodiment 3

[0069] A kind of automatic titration method of embodiment 3 specifically comprises the following steps:

[0070] (1) Sampling and sample pretreatment: take the sample solution to be tested, filter it through a water system 0.45 μm microporous membrane, and put it into a sample loading container;

[0071] (2) Titrator preset: After inserting the burette and pH probe into the sample container, set the pre-stirring time of the titrator to 1min, the delay time to 10s, the speed 1 to 2mL / min, and the speed 2 to 0.5mL / min , the pH value of the speed control point, the pH value of the end point and the speed control amount of 30%;

[0072] (3) Titration in the first stage: after the test starts, pre-stirring is carried out. After the pre-stirring is over, the titrator starts titration at a set speed 1 until the pH value of the sample to be tested reaches the pH value of the speed control point;

[0073] (4) Titration in the second stage: after the pH value of the sample reaches the ...

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Abstract

The invention discloses an automatic titration method which includes the following steps of 1, sampling and sample pretreatment, 2, titrator presetting, 3, first-stage titration, 4, second-stage titration, 5, speed-regulation control quantity point post-titration and 6, data acquisition. The automatic titration method is a test method capable of accurately and scientifically judging the titration end point, the mode of setting speed-regulation control point and speed-regulation control quantity is adopted, and the refinement of the titration process is guaranteed; meanwhile, after the speed-regulation control quantity point is reached, a mode of dropwise adding and delayed judgment is adopted, so that the accuracy of the titration end point can be effectively guaranteed. A fully automatic mode is adopted for the automatic titration method, the influences, on the measurement result, of manual operation are avoided, and the measurement result is high in accuracy and good in repeatability; the automatic titration method can be used for rinse performance tests.

Description

technical field [0001] The invention relates to an automatic titration method and its application, belonging to the technical field of household appliances. Background technique [0002] Rinsing performance, that is, the ability of a washing machine to remove laundry powder and residual pollutants, is an important item for washing machine performance testing. The detection methods for rinsing performance in the current washing machine standards of various countries are different, and the detection principles can be roughly divided into two categories: one is to use a certain component of washing powder as an indicator to detect the changes before and after rinsing to determine the rinsing performance of the washing machine. For example, the alkalinity method used by my country and IEC (International Electrotechnical Commission) is to detect the change of alkaline substances in washing powder. The washing machine standard currently being revised in the United States is to de...

Claims

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Application Information

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IPC IPC(8): G01N31/16
Inventor 岳京松张晓赵爽
Owner CHINA HOUSEHOLD ELECTRIC APPLIANCE RES INST
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