Reactively compatibilized butyl rubber/polyamide TPV (thermoplastic vulcanzate) and preparation method thereof
A thermoplastic vulcanizate, reactive compatibilization technology, applied in the field of polymer materials, can solve the problems of high requirements of industrial production and the inability to achieve compatibilization effect.
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Embodiment 1
[0024] The basic composition and mass parts of the selected raw materials are as follows:
[0025]
[0026]
[0027] Wherein the basic composition and mass ratio of self-made compatibilizer are:
[0028] Halogen-free butyl rubber 100;
[0029] Glycidyl methacrylate 0.01;
[0030] Dicumyl peroxide 1
[0031] According to the above formula, first melt and mix halogen-free butyl rubber, glycidyl methacrylate, and dicumyl peroxide in a Haake internal mixer at 150°C for 5 minutes to obtain graft-modified halogen-free butyl rubber; then mix the dried polyamide 1010 with halogen-free butyl rubber at 190°C, add graft-modified halogen-free butyl rubber and antioxidants in proportion, wait until the mixture is uniform, and then discharge and cool to room temperature ; then mix with anti-aging agent, plasticizer, vulcanizing agent and vulcanization aid at room temperature to obtain a rubber-plastic premix; place the rubber-plastic premix in a screw extruder, set the vulcanizatio...
Embodiment 2
[0035] The basic composition and mass parts of the selected raw materials are as follows:
[0036]
[0037]
[0038] Wherein the basic composition and mass ratio of self-made compatibilizer are:
[0039] Chlorobutyl Rubber 100
[0040] 1,2-epoxybutene 0.5
[0041] Dicumyl peroxide 0.1
[0042] According to the above formula, chlorinated butyl rubber, 1,2-epoxybutene, and dicumyl peroxide were melted and mixed in a Haake internal mixer at 170°C for 8 minutes to obtain graft-modified butyl chloride. base rubber; then mix the dried polyamide 1212 and chlorinated butyl rubber at 200°C, add graft-modified chlorinated butyl rubber and antioxidants in proportion, wait until the mixture is uniform, and then discharge and cool to room temperature; then mix it with anti-aging agent, plasticizer, vulcanizing agent and vulcanization aid at room temperature to obtain a rubber-plastic premix; put the rubber-plastic premix in a screw extruder, set the vulcanization temperature to 20...
Embodiment 3
[0046] The basic composition and mass parts of the selected raw materials are as follows:
[0047]
[0048]
[0049] Wherein the basic composition and mass ratio of self-made compatibilizer are:
[0050] Bromobutyl Rubber 100
[0051] Acrylic anhydride 5
[0052] Dicumyl peroxide 3
[0053] According to the above formula, first melt and mix bromobutyl rubber, acrylic anhydride, and dicumyl peroxide in a Haake internal mixer at 190°C for 10 minutes to obtain graft-modified bromobutyl rubber; then bake Mix dry polyamide 12 and bromobutyl rubber at 210°C, add graft-modified bromobutyl rubber and antioxidants in proportion, wait for the mixture to be uniform, and then discharge and cool to room temperature; Mix with anti-aging agent, plasticizer, vulcanizing agent and vulcanization auxiliary agent to obtain rubber and plastic premix; put the rubber and plastic premix in the screw extruder, set the vulcanization temperature to 190°C, and the speed to 700rpm, and dynamicall...
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