Flame-retardant sheet and flame-retardant composite member
A flame-retardant composite and sheet technology, which is applied in the direction of railway car body parts, lighting device parts, film/sheet adhesives, etc., can solve the problem of low flexibility, low non-combustibility, and non-combustibility of light-scattering sheets. Insufficient performance and other problems, to achieve the effect of excellent flame retardancy, strength improvement, high flame retardancy
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[0208] Now, the present invention will be described more specifically by way of examples and comparative examples. However, the present invention is by no means limited to these. It should be noted that in the following description, "parts" and "%" are by weight unless otherwise specified.
Synthetic example 1
[0210] 50 g of a colloidal silica solution (trade name: SNOWTEXOS, manufactured by Nissan Chemical Industries, Ltd., solid content concentration: 20%) with an average particle diameter of 8 nm to 11 nm and 84 g of 2-propanol were charged to a device including a stirrer, a reflux condenser, and Nitrogen gas is introduced into the container of the tube. Concentrated nitric acid was added to adjust the acidity (pH) of the resulting liquid to be in the range of 2-4. Next, the temperature of the mixture was raised to 70° C., and then, using a dropping funnel, 25 g of a silsesquioxane compound having a reactive methoxysilyl group at a molecular terminal (commercial Name: X-40-9225, manufactured by Shin-Etsu Chemical Co., Ltd., methoxyl content: 24%), the liquid prepared was added dropwise to the mixture over 1.25 hours to carry out the colloidal reaction of the silsesquioxane compound Reactions on the surface of silica particles.
[0211] Next, a liquid prepared by dissolving 75 g...
Synthetic example 2
[0213] 50 g of a colloidal silica solution (trade name: SNOWTEXOS, manufactured by Nissan Chemical Industries, Ltd., solid content concentration: 20%) with an average particle diameter of 8 nm to 11 nm and 84 g of 2-propanol were charged to a device including a stirrer, a reflux condenser, and Nitrogen gas is introduced into the container of the tube. Concentrated nitric acid was added to adjust the acidity (pH) of the resulting liquid to be in the range of 2-4. Next, the temperature of the mixture was raised to 70° C., and then, using a dropping funnel, 10 g of a silsesquioxane compound having a reactive methoxysilyl group at a molecular terminal (commercial Name: X-40-9225, manufactured by Shin-Etsu Chemical Co., Ltd., methoxyl content: 24%), the liquid prepared was added dropwise to the mixture over 0.5 hours to carry out the silsesquioxane compound and colloidal Reactions on the surface of silica particles.
[0214]Next, a liquid prepared by dissolving 90 g of a polysilo...
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