Highly-wear-resistant TPE foaming shoe material and preparation method thereof
A high wear-resistant, shoe material technology, applied in footwear, applications, clothing, etc., can solve the problems of reducing the width and breadth of foamed rubber, wear resistance, and anti-slip performance.
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[0063] (1) Preparation of epoxy silane modified polypyrrole prepolymer
[0064] Weigh a certain amount of polyphosphoric acid in a three-necked flask, connect the gas inlet, drying pipe, gas outlet and mechanical stirrer, feed inert gas, add 1 mole of tetraamine after 3-5min, and the polyphosphoric acid and The ratio of tetramine is 180g / 10mmol. After tetramine is uniformly dispersed and dissolved in polyphosphoric acid, add 0.5-0.95 moles of tetraacid, and then add phosphorus pentoxide to enhance the absorption of water in the reaction product, and start stirring at the same time Raise the temperature to 200°C, and react at this temperature for 20 hours; after the temperature of the reaction system is cooled to 150°C, pour it into deionized water, and wash repeatedly to remove polyphosphoric acid; then pour the product into the product with a mass fraction of 7%-10% Stir in an aqueous sodium hydroxide solution for 24 hours, then repeatedly wash with deionized water to remove ...
Embodiment 1
[0162] After mixing 100 parts by weight of A1, 140 parts by weight of B1, 5 parts by weight of C1, 10 parts by weight of D1, 1 part by weight of E1 and 1 part by weight of F1, granulate by twin-screw extrusion;
[0163] Vacuum injection mold the product obtained above into a mold at 190°C, keep the temperature for 5 hours, then cool and solidify to obtain a preliminary product;
[0164] Soak the above preliminary product in polyphosphoric acid, keep it at 140° C. for 5 hours, wash it with deionized water until it is neutral, and dry it in vacuum to obtain a foamed shoe material.
Embodiment 2
[0166] After mixing 100 parts by weight of A2, 140 parts by weight of B2, 5 parts by weight of C1, 10 parts by weight of D1, 1 part by weight of E1 and 1 part by weight of F1, granulate by twin-screw extrusion;
[0167] Vacuum injection mold the product obtained above into a mold at 190°C, keep the temperature for 5 hours, then cool and solidify to obtain a preliminary product;
[0168] Soak the above preliminary product in polyphosphoric acid, keep it at 140° C. for 5 hours, wash it with deionized water until it is neutral, and dry it in vacuum to obtain a foamed shoe material.
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