Pollution resistant matting aqueous paint composition and forming method thereof
A pollution-resistant, water-based coating technology, applied in coatings, devices for coating liquid on the surface, etc., can solve problems such as coating film pollution, and achieve excellent weather resistance
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[0100] Hereinafter, although an Example demonstrates this invention more concretely, this invention is not limited to these Examples. In addition, "parts" and "%" in the following examples mean "parts by mass" and "% by mass", respectively.
[0101] Manufacture of water-based resin
manufacture example 1
[0103] 350 parts of deionized water and 10 parts of Newcol 707SF (Note 1) were added to a reaction vessel equipped with a thermometer, a thermostat, a stirrer, and a dropping device, stirred and mixed in a nitrogen stream, and the temperature was raised to 85°C. Next, 3% of the pre-emulsion part and 80 parts of 2.5% ammonium persulfate aqueous solution which emulsified the component of the following composition were added in reaction container, and it held at 85 degreeC for 20 minutes.
[0104]
[0105] Then, the remaining pre-emulsion and 80 parts of 2.5% ammonium persulfate aqueous solution were dripped in the reaction container over 4 hours, and aging was performed for 2 hours after the dropwise addition was completed. Then, it cooled to 30 degreeC, and adjusted so that the solid content may be 47 % and pH may become 8.0 using ammonia water and deionized water. Next, it discharged|emitted while filtrating with the nylon cloth of 200 meshes, and obtained the water-based r...
manufacture example 2~4
[0108] In said manufacture example 1, except having made the monomer composition into the compounding shown in following Table 1, it synthesize|combined similarly to manufacture example 1, and obtained water-based resin (A-2) - (A-4).
[0109] [Table 1]
[0110]
[0111] Manufacture of White Pigment Component Dispersion Paste
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