A kind of tungsten-based heavy alloy rod with hardness gradient change and preparation method thereof
A tungsten-based heavy alloy, hardness gradient technology, applied in the direction of metal material coating process, coating, solid diffusion coating, etc., can solve the problems of reducing the overall elongation and increasing the risk of breaking the core material of armor-piercing bullets, etc. Effect of Dynamic Yield Strength
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Embodiment 1
[0027] Example 1: Preparation of Tungsten-based Heavy Alloy Rod with Molybdenum Gradient Structure
[0028] First, 50% (volume fraction) of 2.5 micron molybdenum powder and calcined alumina powder were ball milled and mixed for 3 hours. Embed the sintered 92W-5.6Ni-2.4Fe alloy rod with a diameter of 12mm in a molybdenum boat or corundum boat filled with Mo powder + alumina powder, and put it into a vacuum furnace with molybdenum or tungsten sheets as heating elements. Draw out the air in the furnace to below 5Pa, raise the temperature to 1350°C at a rate of 10°C / min, keep the temperature for 2 hours, and cool down to room temperature with the furnace. From the surface of the alloy rod to 2.5mm below the surface layer, the microhardness of the alloy rod decreases continuously from 380HV to 220HV.
Embodiment 2
[0029] Embodiment 2: the preparation of the graded structure tungsten-based heavy alloy bar of infiltration Ti
[0030] First, 50% (volume fraction) of 25-micron titanium powder and calcined alumina powder were ball milled and mixed for 3 hours. Embed the sintered 92W-5.6Ni-2.4Fe alloy rod with a diameter of 12mm in a molybdenum boat or corundum boat filled with Ti powder + alumina powder, and put it into a vacuum furnace with a molybdenum or tungsten sheet as a heating element. Draw out the air in the furnace to below 5Pa, raise the temperature to 1300°C at a rate of 10°C / min, keep it warm for 2 hours, and cool down to room temperature with the furnace. From the surface of the alloy rod to 2.5mm below the surface layer, the microhardness of the alloy rod decreases continuously from 395HV to 320HV.
Embodiment 3
[0031] Embodiment 3: Preparation of gradient structure tungsten-based heavy alloy cladding Cr
[0032] First, 50% (volume fraction) of 16-micron Cr powder was ball-milled and mixed with calcined alumina powder for 3 hours. Embed the sintered 92W-5.6Ni-2.4Fe alloy rod with a diameter of 12mm in a molybdenum boat or corundum boat filled with Cr powder + alumina powder, and put it into a vacuum furnace with molybdenum or tungsten sheets as heating elements. Draw out the air in the furnace to below 5Pa, raise the temperature to 1300°C at a rate of 10°C / min, keep it warm for 2 hours, and cool down to room temperature with the furnace. From the surface of the alloy rod to 2.5mm below the surface layer, the microhardness of the alloy rod decreases continuously from 373HV to 335HV.
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