Composition containing montelukast and desloratadine and preparation method thereof
A technology of desloratadine and montelukast sodium, which is applied in the field of the combination of montelukast sodium and desloratadine and its preparation, and can solve the problems of cumbersome taking, frequent use, poor drug compliance of children, etc. , to achieve the effect of taking convenience and improving solubility
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Embodiment 1
[0027] Prescription composition of montelukast sodium / desloratadine granules: specification 4mg / 5mg (calculated as montelukast / desloratadine), prescription volume is 1000 bags.
[0028]
[0029] Preparation Process:
[0030] 1) Preparation of desloratadine-β-cyclodextrin inclusion compound
[0031] Add 5.30g of desloratadine to the reactor at room temperature and dissolve in 50ml of absolute ethanol; obtain the absolute ethanol solution of desloratadine; add 20.00g of β-cyclodextrin to the reactor and add 250ml of distilled water , make a saturated aqueous solution at 60°C, keep warm, and set aside. The above desloratadine absolute ethanol solution was slowly dripped into the stirred saturated aqueous solution, and when turbidity appeared, a white precipitate gradually precipitated out. After continuing to stir for 1 hour, continue stirring to room temperature, and finally cooled with an ice bath, and waited for the precipitate to separate out. After completion, suction f...
Embodiment 2
[0036] Prescription composition of Montelukast Sodium / Desloratadine Tablets: specification 10mg / 5mg (calculated as Montelukast / Desloratadine), prescription quantity is 1000 tablets.
[0037]
[0038] Preparation Process:
[0039] 1) Preparation of desloratadine-β-cyclodextrin inclusion compound
[0040] Add 5.30g of desloratadine to the reactor at room temperature and dissolve in 50ml of absolute ethanol; obtain the absolute ethanol solution of desloratadine; add 20.00g of β-cyclodextrin to the reactor and add 250ml of distilled water , make a saturated aqueous solution at 60°C, keep warm, and set aside. The above desloratadine absolute ethanol solution was slowly dripped into the stirred saturated aqueous solution, and when turbidity appeared, a white precipitate gradually precipitated out. After continuing to stir for 1 hour, continue stirring to room temperature, and finally cooled with an ice bath, and waited for the precipitate to separate out. After completion, suct...
Embodiment 3
[0045] Prescription composition of montelukast sodium / desloratadine chewable tablets: specification 5mg / 5mg (calculated as montelukast / desloratadine), prescription quantity is 1000 tablets.
[0046]
[0047] Preparation Process:
[0048] 1) Preparation of desloratadine-β-cyclodextrin inclusion compound
[0049] Add 5.30g of desloratadine to the reactor at room temperature and dissolve in 50ml of absolute ethanol; obtain the absolute ethanol solution of desloratadine; add 20.00g of β-cyclodextrin to the reactor and add 250ml of distilled water , make a saturated aqueous solution at 60°C, keep warm, and set aside. The above desloratadine absolute ethanol solution was slowly dripped into the stirred saturated aqueous solution, and when turbidity appeared, a white precipitate gradually precipitated out. After continuing to stir for 1 hour, continue stirring to room temperature, and finally cooled with an ice bath, and waited for the precipitate to separate out. After completi...
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