Method for preparing sodium-hydroxide-loaded active clay
A technology of activated clay and sodium hydroxide, applied in chemical instruments and methods, inorganic chemistry, silicon compounds, etc., can solve the problems of high cost, long cycle, low efficiency, etc., and achieve high production efficiency, low energy consumption and cost, Efficient effect
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[0023] Example 1
[0024] A preparation method of sodium hydroxide-loaded activated clay includes the following steps:
[0025] S1: Mix bentonite and activated clay wastewater with a concentration of 12% in a weight ratio of 1.5:8, and stir evenly at a speed of 200r / min to obtain slurry material A;
[0026] S2: Add the slurry material A prepared in step S1 to 15% hydrochloric acid, the weight ratio of slurry material A to hydrochloric acid is 2:10, stir at 500r / min, and heat to 88°C, Keep at 88°C and react for 2h to obtain slurry material B;
[0027] S3: Press filter the slurry material B obtained in step S2 at a pressure of 0.92 MPa to obtain a filter cake A with a water content of 42%;
[0028] S4: Add water to filter cake A prepared in step S3 and stir to dissolve it. The amount of water added is 7 times the weight of filter cake A. After stirring and dissolving filter cake A, add polyferric sulfate and stir for 0.5h to precipitate the solution. Press filtration at 0.92MPa to obtai...
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[0032] Example 2
[0033] A preparation method of sodium hydroxide-loaded activated clay includes the following steps:
[0034] S1: Mix bentonite and activated clay wastewater with a concentration of 8% at a weight ratio of 1.2:4, and stir evenly at a speed of 300r / min to obtain slurry material A;
[0035] S2: Add the slurry material A obtained in step S1 to 13% sulfuric acid, the weight ratio of the slurry material A to sulfuric acid is 1:3, stir at 300r / min, and heat to 85°C, Keep at 85°C and react for 3 hours to obtain slurry material B;
[0036] S3: Press filter the slurry material B prepared in step S2 at a pressure of 0.92 MPa to obtain a filter cake A with a moisture content of 40%;
[0037] S4: Add water to the filter cake A prepared in step S3 and stir to dissolve it. The amount of water added is 6.5 times the weight of filter cake A. After stirring and dissolving filter cake A, add polyaluminum sulfate and stir for 1 hour to precipitate the solution. The precipitate is at a p...
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[0041] Example 3
[0042] A preparation method of sodium hydroxide-loaded activated clay includes the following steps:
[0043] S1: Mix bentonite and activated clay wastewater with a concentration of 10% in a weight ratio of 1.4:6, and stir evenly at a speed of 250r / min to obtain slurry material A;
[0044] S2: Add the slurry material A prepared in step S1 to the nitric acid with a concentration of 14%, the weight ratio of the slurry material A to the nitric acid is 1:4, stir at a speed of 400r / min, and heat to 86°C, Keep it at 86°C and react for 3 hours to obtain slurry material B;
[0045] S3: Press filter the slurry material B prepared in step S2 at a pressure of 0.93 MPa to obtain a filter cake A with a water content of 42%;
[0046] S4: Add water to the filter cake A prepared in step S3 and stir to dissolve it. The amount of water added is 7 times the weight of filter cake A. After stirring and dissolving filter cake A, add polyaluminum sulfate and stir for 0.5h to precipitate the...
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