The invention relates to the technical field of
bentonite adsorption material preparation, and discloses a composite modified
bentonite adsorption material and a preparation process thereof, the preparation process comprises the following steps: S1, coarsely crushing
bentonite raw ore into particles, then finely
grinding, sieving with a 200-mesh
sieve, and collecting undersize
bentonite powder; s2, adding
bentonite powder and
hydrochloric acid into a reaction kettle, and carrying out a stirring reaction; s3, carrying out filter pressing on the acidified bentonite
slurry, washing the acidified bentonite
slurry with deionized water until the pH value of filtrate is 6.5-7.0, and then
drying a
filter cake to obtain a pre-dried acidified bentonite
filter cake; s4, the pre-dried
filter cake passes through a
rotary kiln,
microwave heating is arranged in the
rotary kiln, and finally heat activated bentonite is obtained; and S5, mixing the thermally activated bentonite with CTAB at 70 DEG C. According to the preparation process of the composite modified bentonite adsorption material, through the synergistic effect of acidification,
microwave activation and organic intercalation, the comprehensive adsorption performance of bentonite is remarkably improved, interlayer water is rapidly removed through
microwave activation, a skeleton structure is stabilized, and the risk of thermal collapse is avoided.