The invention discloses an online continuous detection
system and method for
cation exchange capacity of
montmorillonite slurry. The
system is composed of a sampling module, a
solid content determination module, a flow path control module, a closed circular reaction unit, a bypass
solid-liquid separation module, an online optical detection module, a
data processing module, a control module and a cleaning module. The method comprises the following steps: automatically diluting a sample according to the
solid content, mixing with a Cu-Trien
reagent pre-balanced by
carbonate, and fully reacting in a closed circular reaction channel; in the reaction process, low-
turbidity clarified liquor is continuously obtained by bypass micro /
cross flow filtration and enters a flow-through optical detection
pool for real-time
absorbance measurement. The
system adopts a dual-
stability criterion triggering
terminal point, the residual Cu-Trien concentration is inversely calculated according to a
calibration curve, and CEC is calculated by combining the
solid content. According to the scheme, full reaction and non-
turbidity interference of an online spectrophotometric method are considered,
carbonate errors are reduced, and real-time, accurate and
continuous monitoring of CEC in the production process is achieved.