702 results about "Coal gasification" patented technology

The invention discloses a coal gasification slag-based backfill material for replacing flow-state solidified soil, a preparation method and an application, utilizes a synergistic gelling effect among three raw materials, breaks through a material strength forming mechanism of traditional flow-state solidified soil, solves the problems of multiple components and high cost of a flow-state solidified soil material in the prior art, and has the advantages of low raw material cost, low raw material cost, low raw material cost, low raw material cost and the like. And the product popularization is facilitated. The specific scheme is as follows: the coal gasification slag-based backfill material for replacing the fluidized stabilized soil comprises coal gasification slag, carbide slag and titanium gypsum, the ratio of the coal gasification slag to the carbide slag to the titanium gypsum is 6-8: 1.5-3.5: 0.5-1.5, and an alkaline activator is also added; the coal gasification slag is a slag block with a set particle size formed after slag at the bottom of a gasification furnace is cooled, the carbide slag is waste slag which takes calcium oxide as a main component after acetylene gas is obtained by hydrolyzing calcium carbide, and under the action of an exciting agent, the coal gasification slag and the carbide slag are fully activated to release polyhedrons; part of the polyhedrons form a gelling product so as to improve the early strength of the coal gasification slag-based backfill material.

The invention relates to the technical field of adsorbent preparation, in particular to an ammonia modified porous carbon adsorbent and a preparation method thereof. The preparation method of the ammonia modified porous carbon adsorbent comprises the following steps: carrying out hydrothermal acid leaching on gasified fine residues and an acid solution to obtain acid leaching residues; stirring the acid leaching residues in an alkali solution, washing and drying to obtain a porous carbon material; and dipping the porous carbon material in a tetraethylenepentamine solution, and then drying to obtain the ammonia modified porous carbon adsorbent. The ammonia modified porous carbon adsorbent is successfully constructed by taking a porous carbon material derived from coal gasification fine slag as a substrate and further adopting a surface ammonia functionalization modification strategy. The preparation method is simple, the raw materials are easy to obtain, and the prepared ammonia modified porous carbon adsorbent has a good adsorption effect on methylene blue and hexavalent chromium. According to the method, high-added-value resource utilization of the coal gasification solid waste is achieved, and a solution is provided for treatment of the dye wastewater and the heavy metal wastewater.

The invention discloses a carbon / nano zero-valent iron composite material based on coal gasification slag and a preparation method of the carbon / nano zero-valent iron composite material. The method comprises the following steps: performing component separation on the coal gasification slag to obtain an iron-rich residual carbon component, mixing and grinding the iron-rich residual carbon component and sodium hydroxide according to a specific mass ratio, performing high-temperature calcination treatment in a nitrogen protective atmosphere, and performing hydrothermal activation reaction, solid-liquid separation, washing and drying to obtain the carbon / nano zero-valent iron composite material. The material shows excellent hexavalent chromium removal performance, can realize efficient removal of Cr (VI) in water within 5 minutes (the removal rate reaches 78.9%), and has remarkable structural stability. Synergistic activation of the endogenous iron-carbon components in the industrial solid waste is creatively achieved, a green and environment-friendly novel functional material solution is provided for heavy metal pollution treatment, and the method has important environmental benefits and industrial application value.

The invention discloses a method for preparing silicon carbide materials by using coal gasification slag, belonging to the field of solid waste recycling. The solution of the invention includes first pre-treating the coal gasification slag, then performing acid leaching, water washing, suction filtration and drying on the pre-treated coal gasification slag, and then performing Joule heating treatment. After calcination, silicon carbide is obtained; in the Joule heating treatment, the discharge voltage is set to 120V-150V, and the number of discharges is 1-5 times. By performing Joule heating treatment on the coal gasification slag, the reaction time of each Joule heating reaction is extremely short, greatly reducing the energy consumption, and sharply shortening the reaction time, solving the technical problem of high energy consumption caused by the long reaction time in the traditional carbothermal reduction for preparing silicon carbide materials in the prior art.

The invention discloses multi-scale toughened full-solid-waste ultrahigh-ductility concrete, which is prepared from the following raw materials in parts by weight: 500 to 650 parts of full-solid-waste cementing materials, 110 to 150 parts of calcined coal gasification slag, 190 to 250 parts of calcined fly ash, 20 to 40 parts of silica fume, 10 to 30 parts of metakaolin, 780 to 930 parts of washed sand, 10 to 25 parts of fly ash fibers, 0.6 to 0.9 part of hydroxypropyl methyl cellulose, 20 to 30 parts of polycarboxylic acid water reducing agents and 300 to 400 parts of water. The calcined coal gasification slag is subjected to gradient heating to 800-960 DEG C, heat preservation is conducted for 30-60 min, then the calcined coal gasification slag is cooled to the room temperature at the cooling rate of 10-15 DEG C / min, and the calcined coal gasification slag is obtained after powder grinding. According to the multi-scale toughened full-solid-waste ultrahigh-ductility concrete provided by the invention, the toughness and the mechanical property of the concrete can be enhanced, the performance of the concrete in an extreme environment is improved, meanwhile, the solid waste utilization rate is increased, and the production cost of the concrete is reduced.

The invention relates to the technical field of coal chemical industry, in particular to a coal gasification black water circulation and black water waste heat recycling system and method. The coal gasification black water circulation and black water waste heat recycling system comprises a synthesis gas washing tower, a high-pressure flash tank, a low-pressure flash tank, a black water heat exchanger, a vacuum flash tank, a settling tank, a grey water tank, a low-pressure flash steam stripping tower and a high-pressure flash steam stripping tower. The coal gasification black water treated by the coal gasification black water circulating and black water waste heat recycling system can be reused as circulating water of a synthesis gas washing tower, so that the cyclic utilization of water resources is realized, the use of fresh water and the discharge of waste water are reduced, and the production cost and the environmental pressure are reduced. Meanwhile, the problem that a black water pipeline is scaled and blocked due to high temperature is solved, waste heat of the black water can be fully replaced for effective utilization, carbon is reduced, energy is saved, the purpose of cooling the black water is achieved, the cooling cost of a vacuum flash evaporation system is saved, and continuous and reliable economic benefits are created for enterprises.

The invention relates to the technical field of coalification black water treatment, and particularly discloses a coal gasification black water flash steam waste heat steam turbine gradient utilization system which comprises a black water flash steam turbine module and a steam exhaust condensation module. The black water flash steam turbine module comprises a high-pressure flash evaporator, a low-pressure flash evaporator, a vacuum flash evaporator, a supplementary condensing steam turbine, a generator and a settling tank, and a water outlet of the vacuum flash evaporator is connected with the settling tank; the steam exhaust condensation module comprises an evaporative condenser and a condensate pump. Through the design of the scale scraping and water uniformizing piece, part of cooling water falling around the heat exchange coil from top to bottom falls on the water uniformizing plate to drive the water uniformizing plate to rotate, when the water uniformizing plate rotates, water on the water uniformizing plate is thrown out under the action of centrifugal force, cooling water without heat exchange can be uniformized to other heat exchange pipes for heat exchange, and the heat exchange efficiency is improved. Therefore, the cooling water flows more uniformly among the heat exchange coils, the utilization rate of the cooling water is improved, and the heat exchange efficiency is improved.

The application discloses a coal gasification slag heavy metal oxidation leaching separation processing system and method in the technical field of mine solid waste treatment, which comprises a multi-radical pre-oxidation device, a primary slag slurry separation and recovery device, a three-stage leaching device and a secondary slag slurry separation and recovery device. The multi-radical pre-oxidation device adds an oxidizing agent solution to the coal gasification slag in three stages and simultaneously performs ozone oxidation and mixing and stirring to obtain coal gasification slag slurry. The primary slag slurry separation and recovery device separates the coal gasification slag slurry, recovers excess oxidizing agent solution and screens out the coal gasification slag. The three-stage leaching device adds mixed organic acid solution to the screened coal gasification slag in three stages, performs mixing and stirring, gradually transfers the heavy metals in the coal gasification slag from the solid phase to the liquid phase, and obtains tail slurry. The application has the advantages of simple operation, low cost, good separation effect and the purpose of effectively controlling the risk of coal gasification slag heavy metal leakage.

The purpose of this invention is to provide a method for preparing cemented backfill materials based on response surface methodology using composite activating coal gasification slag. This method belongs to the field of mining engineering technology. Based on sorting and removing impurities from the coal gasification slag and drying it, the invention obtains ultrafine powder of the coal gasification slag for preparing the backfill material through ball milling. Then, coal gangue is crushed and screened using a crusher to obtain coarse, medium, and fine aggregates for the backfill material. Finally, cement, ultrafine coal gasification slag powder, coal gangue aggregate, activator, and water are mixed evenly to prepare the cemented backfill material. This invention not only solves the problem of low activity of coal gasification slag volcanic ash but also effectively controls the shortage of cemented backfill materials and high backfilling costs during cemented backfill mining, ensuring sustainable development. Furthermore, it effectively utilizes the widely accumulated coal gasification slag, reducing pollution and large-scale land occupation of the surrounding environment.

The invention discloses a rock permeability testing system in a high-temperature and high-pressure environment and a using method thereof, and belongs to the technical field of geothermal development or coal in-situ gasification mining. The test system is composed of a stress loading system, a test kettle assembly and a magnetic particle imaging system. When in use, the stress loading system and the test kettle assembly provide conditions such as high temperature, high pressure, seepage fluid and the like for a test piece; and detecting the spatial distribution state of the nano magnetic induction particles added in the seepage fluid through a magnetic particle imaging system to observe the pore and crack distribution characteristics in the test piece or detecting the nano magnetic induction particles added in the pollutant solution to observe the pollutant migration condition. The test system is scientific in design, simple in structure and easy to operate and maintain, can monitor pore fracture distribution and pollutant migration conditions in the test piece in real time under high-temperature and high-pressure conditions, provides accurate dynamic observation data, and provides important technical support for reservoir assessment and optimization in a complex environment.

The invention discloses a coal gasification slag-steel slag-based high-carbon-storage type filling material and a preparation method thereof, and belongs to the field of coal-based solid waste resource utilization and carbon emission reduction. The filling material comprises the following components in parts by weight: 100 parts of a cementing material, 10-20 parts of aggregate and 10-20 parts of water. 38 to 52 parts of aggregate; 24 to 40 parts of water; the cementing material comprises the following raw materials: 65-85 parts of coal gasification slag; 15 to 35 parts of steel slag; and 3.0 to 10.5 parts of a composite exciting agent. According to the method, the coal gasification slag can be consumed on a large scale, CO2 is fixed and stored through the carbonization reaction, and stable storage of CO2 is achieved through engineering application of a filling material; the problems of industrial solid waste treatment, carbon emission control, natural resource consumption, environmental pollution and the like are effectively solved, and good environmental protection benefits and practical values are achieved; the invention provides a new technical path for realizing solid waste resource utilization and carbon neutralization targets.

The invention relates to the technical field of coal gas water treatment, and discloses a purification treatment system for coal gas water after coal gasification, which comprises a pretreatment tank, a biochemical treatment tank is arranged on one side of the pretreatment tank, a deep treatment tank is arranged on one side of the biochemical treatment tank, a pipe frame is arranged in the biochemical treatment tank, and the pipe frame is arranged in the deep treatment tank. Membrane filaments are arranged in the pipe frame. In the coal gas water treatment process, when the membrane wires are broken, two-stage plugging of the pipeline can be achieved, so that the coal gas water which is sucked into the membrane wires due to the fact that the membrane wires are broken and not filtered cannot enter the transverse pipe, the coal gas water cannot enter the pipe frame to pollute the pipe frame and the transverse pipe, the plugging effect is good through two-stage plugging of the pipeline, and the sealing effect is good. The anti-pollution effect on the pipe frame and the transverse pipe is improved, it can be guaranteed that no impurity is accumulated at the end of the circular ring before plugging is conducted, and a pipeline can be better plugged in cooperation with a plugging ball without impurity accumulation.

The invention relates to the technical field of adsorbent preparation and hexavalent chromium Cr (VI) adsorption, in particular to application of an ammonia modified porous carbon adsorbent in Cr (VI) adsorption. According to the method, an ammonia modified porous carbon adsorbent is added into a water sample containing Cr (VI) for adsorption, so that Cr (VI) in the water sample is removed; the preparation method of the ammonia modified porous carbon adsorbent comprises the following steps: carrying out hydrothermal acid leaching on gasified fine residues and an acid solution to obtain acid leaching residues; stirring the acid leaching residues in an alkali solution, washing and drying to obtain a porous carbon material; and dipping the porous carbon material in a tetraethylenepentamine solution, and then drying to obtain the ammonia modified porous carbon adsorbent. The ammonia modified porous carbon adsorbent is successfully constructed by taking a porous carbon material derived from coal gasification fine slag as a substrate and further adopting a surface ammonia functionalization modification strategy. The ammonia modified porous carbon adsorbent has a good adsorption effect on Cr (VI).

The invention discloses a dehydration, crushing and curing integrated treatment method for sand washing mud. Comprising the following steps: mixing a conditioner with sand washing mud, dehydrating and crushing, mixing and stirring with a curing material, extruding, vibrating and molding, and curing to obtain the sand washing mud-based cured body. According to the invention, polyacrylamide, polyaluminum chloride and fly ash / coal gasification slag are used as conditioners, colloidal particles are flocculated and precipitated under the effects of electrical neutralization, adsorption bridging and net capturing of the conditioners, and fly ash / coal gasification slag plays a role in a skeleton, so that a drainage channel can be provided inside the sand washing mud, the problem of crushing of a filter cake is solved, and the service life of the filter cake is prolonged. The method realizes the spanning of high pollution and low efficiency of sand washing mud treatment to recycling and high performance, has triple values of process innovation, environmental protection standard reaching and economic feasibility, and provides an efficient solution for recycling of building wastes. Meanwhile, the invention is suitable for multi-scene building application of roadbed materials, baking-free bricks, artificial aggregates and the like.

The invention relates to the technical field of adsorbent preparation and methylene blue adsorption, in particular to application of an ammonia modified porous carbon adsorbent in methylene blue adsorption. An ammonia modified porous carbon adsorbent is added into a water sample containing methylene blue for adsorption, so that the methylene blue in the water sample is removed; the preparation method of the ammonia modified porous carbon adsorbent comprises the following steps: carrying out hydrothermal acid leaching on gasified fine residues and an acid solution to obtain acid leaching residues; stirring the acid leaching residues in an alkali solution, washing and drying to obtain a porous carbon material; and dipping the porous carbon material in a tetraethylenepentamine solution, and then drying to obtain the ammonia modified porous carbon adsorbent. The ammonia modified porous carbon adsorbent is successfully constructed by taking a porous carbon material derived from coal gasification fine slag as a substrate and further adopting a surface ammonia functionalization modification strategy. The ammonia modified porous carbon adsorbent has a good adsorption effect on methylene blue.

The invention discloses a method for preparing a porous carbon material by recycling coal gasification slag and semi-coke wastewater, which comprises the following steps: by taking coal gasification fine slag as a carrier and semi-coke wastewater as a phenol source, carrying out flotation-acid leaching modification on the fine slag to purify a carbon-rich component and optimize the surface adsorption activity of the carbon-rich component; then fully adsorbing phenolic substances in the wastewater by utilizing the modified slag body; introducing a composite aldehyde cross-linking agent, and initiating an in-situ phenolic aldehyde polymerization reaction to generate a composite precursor; the precursor is subjected to high-temperature carbonization and alkali activation pore forming, and finally the porous carbon material with the characteristics of high specific surface area, rich graded pores and low ash content is prepared. According to the process, full-amount collaborative recycling of the two wastes is achieved, and the process is green and free of secondary pollution. The obtained material is high in carbon content and rich in defect structure and surface functional groups, shows excellent adsorption capacity and catalytic carrier performance, can be widely applied to the fields of deep purification of water pollutants, adsorption of volatile organic compounds, energy catalysis and the like, and has remarkable environmental protection benefits and resource economic values.

The utility model relates to a raw gas source upgrading system for an internal heating type vertical furnace. The raw gas source upgrading system comprises a dry distillation furnace, a carbon dioxide removal device and a pure oxygen preparation device, the device further comprises a first multi-stage mixer, a second multi-stage mixer, a gas sampling analysis tube and a gas component detector. Pure oxygen is adopted as a combustion improver, so that the content of nitrogen in the raw gas is greatly reduced, and the application scene of coal gasification production and deep processing of the internal heating type vertical furnace is expanded; the components of combustion-supporting gas, combustible gas and inert gas in mixed gas in a lattice wall of the dry distillation furnace are controlled by adopting double-circulation control of carbon dioxide and recirculated gas, the combustion intensity and the uniformity degree are strictly controlled under the condition that dry distillation heat supply is met, and scabbing and burning loss of a dry distillation furnace body are avoided.

In view to the technical problems of low recovery rate of metal elements in metallurgical slag and the problem of inefficient recovery of residual heat of metallurgical slag generated by traditional technology, the present application provides a technology and method for preparing microporous-rich metallurgical slag particles based on carbon etching and efficiently recovering residual heat of metallurgical slag in coal gasification, mainly including four parts of granulation system, etching powder adhesion system, etching gasification system and screening separation system which are sequentially connected, and mainly through four steps of molten metallurgical slag granulation, etching powder adhesion, etching gasification reaction, screening and separation, the efficient recovery and utilization of residual heat of metallurgical slag and the high value conversion of metallurgical slag particle products are realized. The utilization value of metallurgical slag particles is increased by 10-15 times through the system.

The invention provides anti-crack foam concrete as well as a preparation method and application thereof, and belongs to the technical field of building materials. The added quick lime can generate a certain micro-expansion effect when encountering water, shrinkage of the material caused by hydration can be compensated to a certain extent, an alkaline environment can be provided for the foaming agent, and smooth foaming is guaranteed; the magnesite tailing powder is added, so that dicalcium silicate, tricalcium silicate and periclase crystal phases with relatively high fire resistance can be obtained when a fire disaster occurs; the phosphogypsum is added as an activator of the coal gasification slag, so that the hydration induction period is shortened, the later strength development is promoted, and the crack resistance of the foam concrete is improved; the modified fibers are added, the fibers form an irregular supporting structure in the multi-bubble slurry to play a role in protecting the foam, meanwhile, the fibers can improve the pore structure and also have an effect of hindering microcrack propagation, and the three fibers have a synergistic effect, so that the crack resistance of the foam concrete is improved.

The application discloses an energy-saving, efficient and adjustable alcohol pre-gas ammonia production process method, and particularly comprises the following steps: S1, a raw material gas is separated from a pressurized coal gasification methanol device as alcohol pre-gas and is sent to a shift device of synthetic ammonia through a sealed pipeline; S2, when entering the shift device, the alcohol pre-gas is mixed with a crude synthetic gas to form a mixed gas, then high-pressure steam is introduced to adjust the water-gas and increase the mixed temperature, carbon monoxide is reacted with water vapor in the shift device, and hydrogen gas is prepared as a shift gas; S3, the shift gas is subjected to low-temperature methanol washing and liquid nitrogen washing, then nitrogen gas produced by air separation is added, a synthetic gas is prepared, and the synthetic gas is sent to an ammonia synthesis device. The energy-saving, efficient and adjustable alcohol pre-gas ammonia production process method is adopted, raw material gas is comprehensively utilized in an energy-saving mode, the methanol and synthetic ammonia production yield is flexibly adjusted, and enterprise benefits are improved.

The invention discloses a method for preparing a porous carbon / hydrotalcite-like compound adsorbent from fine coal gasification slag, which comprises the following steps: by taking the fine coal gasification slag as a raw material, sequentially carrying out alkali activation desiliconization and ion regulation, adding a pH regulator, stirring, and carrying out one-pot hydrothermal synthesis to obtain the porous carbon / hydrotalcite-like compound adsorbent. And carrying out solid-liquid separation and washing on the hydrothermal composition to obtain a solid phase, namely the porous carbon / hydrotalcite-like compound adsorbent. According to the invention, the pore structure of carbon is expanded while alkali activation desiliconization is carried out, so that the formation of porous carbon is ensured; the porous carbon / hydrotalcite-like compound adsorbent meets the requirement of forming a hydrotalcite-like compound with better crystallinity through ion regulation and control, provides an alkaline environment for synthesizing the hydrotalcite-like compound by adding a pH regulator, ensures the formation of the hydrotalcite-like compound through one-pot hydrothermal synthesis, and is obtained through solid-liquid separation and washing, the aggregation state in the hydrotalcite-like compound synthesis process is improved, and the stability and adsorption active sites of the composite adsorption material are increased.

The utility model belongs to the technical field of coal gasification high-pressure flash steam purification, and particularly relates to a coal gasification high-pressure flash steam purification device. The purification section is arranged above the heat exchange section of the hot water tower, high-pressure flash steam subjected to heat exchange with grey water is washed and purified, ammonium salt and ash in the high-pressure flash steam are removed, meanwhile, the flushing device is arranged on the cooler, the tube pass of the cooler is flushed, and the heat exchange efficiency is improved. Ammonium salt and ash attached to the inner wall of the cooler tube pass are flushed, so that the cooler tube pass can be efficiently prevented from being blocked; and the cooled high-pressure flash steam is subjected to gas-liquid separation, so that ammonium salt, ash and moisture in the high-pressure flash steam are greatly reduced, the high-pressure flash steam is purified and fed into a compressor, and the load and damage frequency of the compressor are reduced.

The invention discloses a method for solidifying chromium in coal gasification ash and an obtained low-chromium-mobility large-dosage coal gasification ash-based cemented filling material, and relates to the technical field of solid waste resource utilization and heavy metal solidification. The curing method comprises the following steps: mixing the coal gasification ash with gangue, steel slag, a cementing material and water to prepare the low-chromium-mobility large-dosage coal gasification ash-based cemented filling material so as to realize the curing of chromium in the coal gasification ash, the cementing material is prepared from the following raw materials: slag and an alkali activator. The low-chromium-mobility large-dosage coal gasification ash-based cemented filling material prepared by the curing method is high in chromium fixing capacity, low in cost, high in coal-based solid waste utilization rate and remarkable in comprehensive benefit.

The invention discloses a method for preparing a roadside support filling body from coal gasification ash solid waste, and belongs to the technical field of coal-based solid waste resource utilization. The roadside filling body is formed by mixing coal gangue, coal gasification ash coarse slag, coal gasification ash fine slag and alkaline water; coal gangue serves as coarse aggregate, coal gasification ash coarse slag serves as fine aggregate, and the coal gasification ash fine slag is activated to replace cement to serve as a cementing material. The coal gangue, the coal gasification ash coarse slag, the coal gasification ash fine slag and the alkaline water are mixed to prepare the roadside filling body cementing material, other cementing materials and aggregates do not need to be added, after curing is conducted for 28 days, solidification of filling slurry is achieved through the activation characteristic of the coal gasification ash, and the performance of the filling slurry meets the performance requirement of the roadside filling material. The method is low in material cost, large in solid waste disposal amount and good in environmental benefit, a new way is provided for disposal of solid waste such as coal gasification ash, and sustainable development of the coal industry can be promoted.

The invention belongs to the technical field of neutralization treatment, and discloses a coal gasification slag and tail gas neutralization treatment device based on amino catalysis, which comprises a working frame, when amino-catalyzed coal gasification slag particles and tail gas are mixed and float upwards, the particles are arranged by the conical surface of a conical block; amino-catalyzed coal gasification slag particles move towards the periphery of the inner wall of a fixed shell, then the amino-catalyzed coal gasification slag particles slide to the top of a lifting table along the inclination angle of a conical annular plate in the natural falling process, and active particles fall into a sedimentation shell through filter holes. In the process, the particles can be screened and separated through floating and falling, when the particles with high activity are mixed with the tail gas, chemical reaction or harmful substance adsorption can be more effectively carried out, and the active particles can fall back to the settling shell through the filter holes to be further treated. Therefore, the cyclic utilization of the particulate matters is ensured.

The invention discloses a coal gasification black water multi-stage deep treatment device and method, and relates to the technical field of water treatment.The coal gasification black water multi-stage deep treatment device comprises a flash tank, a settling tank, a mixing and clarifying tank, a partition plate, an overflow opening, a mixing cavity, a clarifying and stirring mechanism, a pressing plate, a water inlet tank and a fixed bin, the two sides of the fixed bin are open, and an adjusting plate is clamped in the fixed bin and horizontally and freely slides in the fixed bin; a water storage space is defined by the adjusting plate, the fixed bin and the partition plate. According to the device, the pressing plate moves downwards, so that the pressing plate extrudes an extraction liquid in the mixing cavity, part of the extraction liquid enters the water storage space from the water inlet groove under the action of pressure, then along with downward movement of the pressing plate, the liquid level of the extraction liquid in the water storage space rises, and the extraction liquid flows into the clarifying cavity from the overflow port; after entering the water storage space, the extraction liquid loses the acting force of the stirring mechanism, so that a relatively large turbulence phenomenon is avoided, the extraction liquid can flow into the clarification cavity at a relatively low flow speed, and the clarification efficiency is prevented from being influenced.

The present invention discloses a preparation method of a carbon-rich coal gasification slag-based iodine-doped C / SiO x composite lithium battery anode material, belonging to the field of lithium battery anode materials; First, the present invention uses a nitric acid solution to pretreat the carbon-rich coal gasification slag to remove metal impurities and obtain a solid residue; Then, the pore channels of the solid residue are modified and reformed by chemical activation to prepare a porous C / SiO x composite material; Finally, iodine (I2) is deposited on the surface and inner pore walls of the porous C / SiO x composite material by fumigation to finally obtain the anode material.

The invention discloses a full-size-fraction coal gasification slag in-situ carbon ash water synergistic efficient separation method, which belongs to the technical field of coal chemical industry, and comprises the following steps: converting gasification fine slag and gasification coarse slag to form gasification ash water; sorting the gasified ash water to obtain high-carbon slag and high-ash slag; filtering and dehydrating the high-carbon slag and the high-ash slag; and dehydrating the dehydrated high-carbon residues and high-ash residues by adopting a high-speed rotational flow low-temperature activation method to obtain the high-carbon residues with the water content of less than 33% and the high-ash residues with the water content of less than 8%. The method is adopted at the tail end of the gasification process, and efficient in-situ carbon ash water separation of the whole-size-fraction coal gasification slag is achieved.

The invention belongs to the technical field of coal mine filling and solid waste resource utilization, and particularly relates to an abandoned roadway coal gasification ash full-solid waste filling material CO2 mineralization storage method which comprises the following steps that stability evaluation is conducted on a target abandoned roadway, and the roadway end of the target abandoned roadway is blocked; preparing a filling material; the prepared filling material is filled into a target abandoned roadway, and a reserved gas injection pipe and a roadway side gas injection pipe are arranged in the filling material in the filling process; cO2 is injected into the filling material through the reserved gas injection pipe and the laneway side gas injection pipe; and detecting the CO2 injection pressure and concentration to complete mineralization sealing. According to the method, by evaluating the stability of the target abandoned roadway, preparing the coal gasification ash full-solid waste filling material and carrying out CO2 gas injection storage, CO2 mineralization storage of the coal gasification ash full-solid waste filling material of the abandoned roadway is achieved, and coal-based solid waste resource utilization and negative carbon efficient filling popularization and utilization can be promoted.

The invention discloses a quality-divided separation and high-valued utilization method of coal gasification slag, a generated product and application, and belongs to the technical field of high-valued recycling of coal gasification slag. According to the method, the coal gasification slag is classified by adopting an alkali fusion-acid leaching two-step method, components in the coal gasification slag are classified into pure carbon components and a metal-containing acid leaching salt solution, a high-valued utilization method is provided for the classified components, and the carbon components are activated into an active carbon electrode material with a high specific surface area and applied to the field of energy storage. The metal-containing acid leaching salt solution is prepared into the metal cross-linked hydrogel, and the metal cross-linked hydrogel is applied to the field of coal flame retardance. The method can effectively solve the technical problem that the overall utilization is restricted by carbon ash caused by multi-metal component mixing and high carbon content of the coal gasification slag in the prior art.