Pretreatment method of coal tar
A coal tar and pretreatment technology, applied in tar processing, petroleum industry, etc., can solve the problems of low utilization rate of coal tar, waste of heavy fractions, reduction of economic benefits, etc., and achieve high utilization rate, easy realization, and simple process Effect
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Embodiment 1
[0018] 2369g coal tar, its properties are shown in Table 1, mix homogeneously with 2087g refined diesel oil by volume ratio 1: 1.04, be heated to 50 ℃, add 200ml water then, 20ml sodium carbonate solution (mass concentration 5%) adjust pH value to be 9, add 2ml of polyether demulsifier, stirred for 2 hours and then left to stand for 6 hours, layered to obtain 4022g of refined diesel solubles, 257g of water and 353g of insolubles; 353g of insolubles and 372g of toluene were mixed uniformly at a volume ratio of 1:1.25, and the control of 60 ℃ temperature, separate 128g of toluene insoluble matter; distill the toluene in the toluene soluble matter to obtain 225g of distilled residue. The residue is uniformly mixed with refined diesel solubles to obtain pretreated coal tar. The utilization rate of coal tar is 91.18%. , the properties of coal tar after pretreatment are shown in Table 1.
[0019] Table 1. Properties of coal tar and coal tar after pretreatment
[0020] pr...
Embodiment 2
[0023] 1790g coal tar, its properties are shown in Table 2, mixed with 1826g coal tar hydrogenated oil by volume ratio 1: 1.2, heated to 150 ° C, then added 200ml water, 20ml sodium carbonate solution (mass concentration 5%) to adjust the pH value If it is 9, add 2ml polyether demulsifier, stir for 0.5h and then let it stand for 24h, and separate layers to obtain 3502g of oil soluble matter, 280g of water and 55g of insoluble matter; 55g of insoluble matter and 92g of toluene by volume ratio 1:2.0 Mix evenly and dissolve at 100°C to separate out 47g of toluene insoluble matter; distill off the toluene in the toluene soluble matter to obtain 8g of distillate, which is mixed evenly with refined diesel oil soluble matter to obtain pretreatment After coal tar. The utilization rate of coal tar is 94.08%. The properties of coal tar after pretreatment are shown in Table 2.
[0024] Table 2. Properties of coal tar and pretreated coal tar
[0025] project
[0026] ...
Embodiment 3
[0028] 2000g of coal tar, whose properties are shown in Table 3, is mixed with 338g of hydrotreated diesel oil in a volume ratio of 1:0.2, heated to 80°C, then added with 600ml of water and 5ml of sodium carbonate solution (mass concentration 5%), and the pH value is adjusted to 6. Add 1m polyether demulsifier, stir for 1 hour and then let stand for 12 hours to obtain 1665g hydrotreated diesel oil soluble matter, 636g water and 673g insoluble matter; the volume ratio of 673g insoluble matter and 226g toluene is 1:0.4 Mix evenly and dissolve at 55°C, and 475g of toluene insoluble matter can be separated out; distill out the toluene in the toluene soluble matter to obtain 198g of distilled matter, which can be mixed evenly with refined diesel oil soluble matter to obtain pretreatment After coal tar. The utilization rate of coal tar is 90.1%. The properties of coal tar after pretreatment are shown in Table 3.
[0029] Table 3. Properties of coal tar and coal tar after pretreatme...
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