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Rare earth formula salt for deep qpq technology and preparation method thereof

A technology, rare earth technology, applied in the field of rare earth formula salt and its preparation, can solve the problems of high applicable temperature of nitriding base salt, insufficient depth of nitride layer, unsuitable for low temperature treatment, etc., achieve a wide melting point temperature range, improve resistance Abrasiveness and corrosion resistance, low melting point effect

Active Publication Date: 2018-01-23
ZAOZHUANG HAIDI ENERGY TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the current salt bath nitriding treatment technology applied to stainless steel has the following disadvantages: the nitriding base salt is suitable for high temperature, generally between 520-600 ° C, which is not suitable for low temperature treatment; the depth of the nitride layer is not thick enough, resulting in most The application field is relatively limited, and the present invention can provide a kind of liquid nitrogen that expands the melting point temperature range of known nitride salts, and can carry out deep QPQ technology treatment on medium and low carbon steels with a compound layer depth of 70 μm or more. Nitride Salt of Rare Earth Formula

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] Rare earth formula salt raw material for deep QPQ technology: 4kgCO(NH 2 ) 2 , 2kgNa 2 CO 3 , 2kgK 2 CO 3 , 0.5kgNaCl, 0.5kgKCl, 0.3kgNa 2 SO 3 , 0.3kg portion of La 2(CO 3 ) 3 , 0.3kgCe 2 (CO 3 ) 3 .

[0034] The preparation method of the rare earth formula salt used in the deep QPQ technology: mix CO(NH 2 ) 2 、Na 2 CO 3 、K 2 CO 3 , NaCl, KCl, Na 2 SO 3 , La 2 (CO 3 ) 3 、Ce 2 (CO 3 ) 3 Mix evenly, put it into a crucible at 400°C, and keep it warm for 5 hours to get the rare earth formula salt for deep QPQ technology.

Embodiment 2

[0036] Rare earth formula salt raw material for deep QPQ technology: 4kgCO(NH 2 ) 2 , 2kgNa 2 CO 3 , 2kgK 2 CO 3 , 0.5kgNaCl, 0.5kgKCl, 0.3kgNa 2 SO 3 , 0.6kg portion of La 2 (CO 3 ) 3 .

[0037] The preparation method of the rare earth formula salt used in the deep QPQ technology: mix CO(NH 2 ) 2 、Na 2 CO 3 、K 2 CO 3 , NaCl, KCl, Na 2 SO 3 , La 2 (CO 3 ) 3 Mix evenly, put it into a crucible at 400° C., and keep it warm for 5 hours to obtain the rare earth formula salt for deep QPQ technology in Example 2.

Embodiment 3

[0039] Rare earth formula salt raw material for deep QPQ technology: 4kgCO(NH 2 ) 2 , 2kgNa 2 CO 3 , 2kgK 2 CO 3 , 0.5kgNaCl, 0.5kgKCl, 0.3kgNa 2 SO 3 , 0.6kgCe 2 (CO 3 ) 3 .

[0040] The preparation method of the rare earth formula salt used in the deep QPQ technology: mix CO(NH 2 ) 2 、Na 2 CO 3 、K 2 CO 3 , NaCl, KCl, Na 2 SO 3 、Ce 2 (CO 3 ) 3 Mix evenly, put it into a crucible at 400° C., and keep it warm for 5 hours to obtain the rare earth formula salt for deep QPQ technology in Example 3.

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PUM

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Abstract

The invention discloses a rare earth formula salt for a deep QPQ technology and a preparation method thereof. The rare earth formula salt is prepared from 35-45 parts by weight of CO(NH2)2, 15-25 parts by weight of Na2CO3, 15-25 parts by weight of K2CO3, 3-7 parts by weight of NaCl, 3-7 parts by weight of KCl, 1-5 parts by weight of Na2SO3, 1-5 parts by weight of La2(CO3)3 and 1-5 parts by weight of Ce2(CO3)3. The nitrided salt contains lanthanum carbonate, cerous carbonate and reasonable other components. In a work state, cyanate ions are decomposed to form active nitrogen atoms and the active nitrogen atoms permeate into the surface of an iron base material and form a hard and compact iron nitride on the material surface so that material wear resistance and corrosion resistance are improved. The salt has a low melting point, can keep a certain nitrogen potential at a low temperature, is stable at a high temperature, has a wide melting point temperature range and can form a deep compound layer through nitridation treatment.

Description

technical field [0001] The invention relates to a rare earth formula salt used in deep QPQ technology and a preparation method thereof. Background technique [0002] In the hydraulic transmission with water as the working medium, the hydraulic components are required to have high wear resistance and corrosion resistance at the same time. At present, the commonly used materials for hydraulic components include: corrosion-resistant alloys, engineering plastics, ceramics and their coating materials, etc. Most of these materials have the problems of high price, complicated processing technology or high requirements for working conditions, so it is necessary to find a Inexpensive materials to replace traditional hydraulic transmission element materials. At present, there are many surface modification methods, such as ion nitriding, surface spraying and QPQ salt bath composite treatment technology, etc. These surface modification methods have their own advantages and disadvantage...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23C8/50
CPCC23C8/50
Inventor 黄美蓉
Owner ZAOZHUANG HAIDI ENERGY TECH
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