Nanoparticle static blasting agent for shale gas development and manufacturing method thereof

A static blasting agent and nano-particle technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of increasing steam pressure, low work efficiency, poor safety, etc., and achieve uniform blasting expansion force and stable blasting time , high work efficiency

Active Publication Date: 2018-06-29
QINZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The technical methods disclosed in the invention patents CN102168543B, CNl102877823A and CN103161434A all utilize the principle of blasting to transform oil and gas reservoirs to increase oil and gas recovery. The disadvantage is that the conventional explosive blasting method is used, and there are problems such as poor safety in use.
However, the static blasting agent used in this static blasting and fracturing method is a lime-based or magnesium oxide-based or ettringite-based powdered blasting agent. In actual construction, it is necessary to accurately measure the amount of water to mix the powder. Not only The work efficiency is low, and the heat of hydration generated by the hydration reaction increases the vapor pressure inside the downhole pores, resulting in spout phenomenon, which makes it difficult for water vapor to pass through the filled gaps, resulting in long blasting time, blasting agent greatly affected by temperature, and unstable blasting time. Problems such as uneven blasting expansion force

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] A shale gas development adopts a nano-particle static blasting agent, which includes a base material and a grain binder, the weight part of the base material is 80, and the weight part of the grain binder is 10, The matrix material is calcium oxide with a particle size of less than 100 nm, and the grain binder is a nano-mixed oxide with a particle size of less than 80 nm. The nano-mixed oxide includes the following oxide components mixed together in parts by weight: Fe 2 O 3 : 0.1, Al 2 O 3 : 0.5, SiO 2 : 8, MgO: 0.5, SO 3 : 0.1.

Embodiment 2

[0035] A shale gas development adopts nano-particle static blasting agent, which includes a base material and a grain binder, the weight part of the base material is 90, and the weight part of the grain binder is 20. The matrix material is calcium oxide with a particle size of less than 100 nm, and the grain binder is a nano-mixed oxide with a particle size of less than 80 nm. The nano-mixed oxide includes the following oxide components mixed together in parts by weight: Fe 2 O 3 : 1, Al 2 O 3 : 2, SiO 2 : 15, MgO: 2, SO 3 :1.

Embodiment 3

[0037] A shale gas development adopts a nano-particle static blasting agent, which includes a matrix material and a grain binder, the weight part of the matrix material is 82, and the weight part of the grain binder is 15. The matrix material is calcium oxide with a particle size of less than 100 nm, and the grain binder is a nano-mixed oxide with a particle size of less than 80 nm. The nano-mixed oxide includes the following oxide components mixed together in parts by weight: Fe 2 O 3 : 0.5, Al 2 O 3 : 1.0, SiO 2 : 10, MgO: 1, SO 3 : 0.5.

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Abstract

The invention discloses a nanoparticle static blasting agent for exploiting shale gas and relates to the field of shale gas exploitation. The blasting agent is prepared from the following raw materials in parts by weight: 80 to 90 parts of matrix material and 10 to 20 parts of crystal grain binding material, wherein the matrix material is calcium oxide of which the grain size is smaller than 100nm, and the crystal grain binding material is a nano mixed oxide of which the grain size is smaller than 80nm. The method comprises the following steps of A, preparing a mixed raw material; B, mixing: uniformly mixing the matrix material, the crystal grain binding material and a proper amount of water; C, grinding: feeding into a ball mill for grinding to obtain aggregated particles; D, screening: screening to obtain granules with 20 to 30 meshes and high roundness; E, firing: feeding the screened granules into a kiln for firing to obtain the nanoparticle static blasting agent for exploiting the shale gas. The nanoparticle static blasting agent disclosed by the invention has the characteristics of uniform blasting expansibility, short and stable blasting time, high working efficiency, simplicity in construction, safety, environmental protection, good fracture effect, low cost and the like, and is easy for popularization and use.

Description

Technical field [0001] The invention relates to the field of unconventional natural gas resource shale gas exploitation, in particular to a shale gas exploitation using nano-particle static blasting agent and a manufacturing method thereof. Background technique [0002] Shale gas is an important unconventional natural gas resource. Its main body is located in dark mud shale or high-carbon mud shale. It accumulates in shale-like interlayers mainly in adsorption or free state. It is not only a potential alternative energy source for conventional energy natural gas, but also a clean and environmentally friendly new energy source. Its main component is methane, which is a new type of natural gas to be used on a large scale in the future. Due to the complex genesis of shale gas, its storage form is complicated. About 50% exist in fractures, pores and other storage spaces, about 50% exist in the surface of clay particles and pores in an adsorbed state, and a very small amount is store...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/62
CPCC09K8/62C09K2208/10
Inventor 卢炳雄于景维黄远林徐文礼
Owner QINZHOU UNIV
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