Method for preparing ultraviolet-resistant and antistatic superfine-denier polyester fibers
An ultra-fine denier polyester, anti-ultraviolet technology, applied in the manufacture of conductive/anti-static filaments, chemical characteristics of fibers, rayon manufacturing, etc. To achieve the effect of good improvement and low cost
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Embodiment 1
[0024] A kind of preparation method of anti-ultraviolet, antistatic ultra-fine denier polyester fiber, carry out according to the following steps:
[0025] A, adopt the mode of high-energy ball mill to grind sericite into superfine powder, and screen out the sericite superfine powder between 10-30 microns in particle diameter;
[0026] B. Use a nano grinder to grind high-purity iron oxide and natural tourmaline to 100-500 nanometers;
[0027] C. Stir the polyester resin at a low speed (125rpm) at 290°C in a molten state, and add molybdenum disulfide, glycerin and sericite superfine powder in turn, and stir for 25 minutes;
[0028] D, adjust stirring speed to medium speed (250rpm), and add high-purity iron oxide nanopowder and natural tourmaline nanopowder successively, stir 60min; Make modified polyester resin slice;
[0029] E. The modified polyester resin slices are spun at high speed on a spinning machine to produce superfine denier fibers. The specific process conditions ...
Embodiment 2
[0034] A kind of preparation method of anti-ultraviolet, antistatic ultra-fine denier polyester fiber, carry out according to the following steps:
[0035] A, adopt the mode of high-energy ball mill to grind sericite into superfine powder, and screen out the sericite superfine powder between 10-30 microns in particle diameter;
[0036] B. Use a nano grinder to grind high-purity iron oxide and natural tourmaline to 100-500 nanometers;
[0037] C. Stir the polyester resin at a low speed (150 rpm) at 300°C in a molten state, and add molybdenum disulfide, glycerin and sericite superfine powder in turn, and stir for 30 minutes;
[0038] D, adjust stirring speed to medium speed (280rpm), and add high-purity iron oxide nanopowder and natural tourmaline nanopowder successively, stir 50min; Make modified polyester resin slice;
[0039] E. The modified polyester resin slices are spun at high speed on a spinning machine to produce superfine denier fibers. The specific process conditions...
Embodiment 3
[0044] A kind of preparation method of anti-ultraviolet, antistatic ultra-fine denier polyester fiber, carry out according to the following steps:
[0045] A, adopt the mode of high-energy ball mill to grind sericite into superfine powder, and screen out the sericite superfine powder between 10-30 microns in particle diameter;
[0046] B. Use a nano grinder to grind high-purity iron oxide and natural tourmaline to 100-500 nanometers;
[0047] C. Stir the polyester resin at a low speed (100 rpm) at 280°C in a molten state, and add molybdenum disulfide, glycerin and sericite superfine powder in turn, and stir for 25 minutes;
[0048] D, adjust stirring speed to medium speed (300rpm), and add high-purity iron oxide nanopowder and natural tourmaline nanopowder successively, stir 45min; Make modified polyester resin slice;
[0049] E. The modified polyester resin slices are spun at high speed on a spinning machine to produce superfine denier fibers. The specific process conditions...
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