Oil migration direction tracing method
An oil migration and oil technology, applied in the field of tracer, can solve problems such as loss of target compounds, complex pretreatment, secondary pollution of samples, etc., and achieve the effect of simple and clear identification methods
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[0045] 1) Oil sample collection:
[0046] Oil samples from the Rimbey-Meadowbrook biological reef chain oil and gas reservoirs in the Upper Devonian in the Western Canada Basin were collected at multiple points. During the collection process, ensure that the crude oil samples are not subject to secondary pollution. After the samples are collected, they are sealed and stored in low-temperature refrigeration.
[0047] 2) Sample analysis:
[0048] Take about 10 mg of crude oil sample and dissolve it in 1 mL of toluene, then take 20 μL of the sample solution and redissolve it in 1 mL of toluene:methanol (1:1 / V:V) mixed solution, add 10 μL of 28 wt% ammonia water to the resulting solution, shake gently to make It was mixed well and then subjected to Fourier transform ion cyclotron resonance mass spectrometry. The analyzer is an American Bruker solariX FT-ICR MS with a magnetic field strength of 12.0T. Using ESI ionization source, negative ion mode. FT-ICR MS main instrument par...
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