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A kind of method of preparing nitrogen carbon molecular sieve by apple pomace

A carbon molecular sieve and apple pomace technology is applied in the field of preparing nitrogen carbon molecular sieve from apple pomace, and the preparation field of molecular sieve achieves the effects of high specific surface area, low price and wide source.

Active Publication Date: 2019-02-01
湖州度信科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There is no report of using apple or apple pomace as raw material to prepare carbon molecular sieve

Method used

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  • A kind of method of preparing nitrogen carbon molecular sieve by apple pomace

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Experimental program
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Effect test

Embodiment 1

[0017] A method for preparing nitrogen carbon molecular sieves from apple pomace, comprising the steps of:

[0018] Step 1: Pretreatment of raw materials, pretreatment of apple waste resources, after simple cleaning, put the apple waste into a high-speed mixer, add water, stir for 12 minutes at a speed of 1350rpm, and then remove the core part After extraction, the raw materials are made into dry powder by extrusion, drying and crushing, and the pretreated raw materials are obtained by sieving;

[0019] Step 2: carbonization, put the pretreated raw materials into the carbonization furnace, lay the raw materials naturally on the plane, raise the temperature to the carbonization temperature, and carbonize to obtain the final carbon molecular sieve carbon material.

[0020] The powder particle size of the pretreated raw material is 30-50 μm.

[0021] The laying thickness of the carbonized raw materials is 3-5mm.

[0022] The carbonization temperature is 980°C.

[0023] The fin...

Embodiment 2

[0025] A method for preparing nitrogen carbon molecular sieves from apple pomace, comprising the steps of:

[0026] Step 1: Pretreatment of raw materials, pretreatment of apple waste resources, first after simple cleaning, put the apple waste into a high-speed mixer, add water, stir for 15 minutes at a speed of 1200rpm, and then remove the core part After extraction, the raw materials are made into dry powder by extrusion, drying and crushing, and the pretreated raw materials are obtained by sieving;

[0027] Step 2: carbonization, put the pretreated raw materials into the carbonization furnace, lay the raw materials naturally on the plane, raise the temperature to the carbonization temperature, and carbonize to obtain the final carbon molecular sieve carbon material.

[0028] The powder particle size of the pretreated raw material is 30-50 μm.

[0029] The laying thickness of the carbonized raw materials is 3-5mm.

[0030] The carbonization temperature is 950°C.

Embodiment 3

[0032] A method for preparing nitrogen carbon molecular sieves from apple pomace, comprising the steps of:

[0033] Step 1: Pretreatment of raw materials, pretreatment of apple waste resources, first after simple cleaning, put the apple waste into a high-speed mixer, add water, stir for 10 minutes at a speed of 1500rpm, and then remove the core part After extraction, the raw materials are made into dry powder by extrusion, drying and crushing, and the pretreated raw materials are obtained by sieving;

[0034] Step 2: carbonization, put the pretreated raw materials into the carbonization furnace, lay the raw materials naturally on the plane, raise the temperature to the carbonization temperature, and carbonize to obtain the final carbon molecular sieve carbon material.

[0035] The powder particle size of the pretreated raw material is 30-50 μm.

[0036] The laying thickness of the carbonized raw materials is 3-5 mm.

[0037] The carbonization temperature is 1000°C.

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Abstract

The invention discloses a method for preparing a nitrogen carbon molecular sieve from apple pomace. According to the method, the main part, namely, apple pits, in waste of apples serves as the raw materials; the method is newly improved based on an original preparing method, the source is wide, and the price is low; the prepared carbon molecular sieve material suitable for preparing nitrogen has a very high specific surface area.

Description

technical field [0001] The invention relates to a method for preparing molecular sieves, belonging to the field of carbon materials, in particular to a method for preparing nitrogen carbon molecular sieves from apple pomace. Background technique [0002] my country's apple production is abundant, and a large number of apples rot every year due to the decoupling of supply and marketing, backward storage technology and apple deep processing. On the other hand, a large amount of apples are used for juicing, and a large amount of by-product-apple pomace has not been found suitable for processing. There are patent reports that apple pomace is used to produce fertilizers, and there are studies that use apple pomace as a raw material to prepare general activated carbon materials. In addition, there are no other research reports on the application of apple pomace. [0003] Carbon molecular sieve is a kind of carbonaceous porous material, which belongs to a kind of activated carbon....

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B32/05
CPCC01P2006/12C01P2006/17
Inventor 钱林月任剑英
Owner 湖州度信科技有限公司