Benzoin spice and preparation method thereof

A technology of benzoin and benzoin resin, which is applied in the direction of essential oil/fragrance, fat production, etc., can solve the problems of low yield of benzoin extract, viscous benzoin extract, and easy sticking in the container, so as to achieve low cost and solve the problem of fragrance Not outstanding, solve the effect that is difficult to transfer

Inactive Publication Date: 2016-12-07
YUNNAN LORRAINE AROMATIC PROD CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The obtained benzoin extract is very viscous, and it is difficult to transfer, and it is easy to stick in the container, and the transfer or pouring process brings a lot of trouble to the experimental operator; and the yield of the benzoin extract obtained by ethanol extraction or steam distillation low, less than 80%

Method used

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  • Benzoin spice and preparation method thereof
  • Benzoin spice and preparation method thereof
  • Benzoin spice and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] The benzoin fragrance comprises the following components by weight:

[0039] 50 parts of benzoin resin;

[0040] 50 parts of dipropylene glycol;

[0041] Melt the massive benzoin resin at 80-90°C for 6 hours, filter it while it is hot with a 100-200 mesh sieve to obtain the benzoin resin extract, dissolve the obtained benzoin resin extract in dipropylene glycol, and the yield is 94.85% ( Because the benzoin resin has some solid impurities such as branches and leaves of benzoin tree in the inside), get the benzoin resin extract 2g of gained, be dissolved in 2ml dipropylene glycol, it has the characteristic fragrant and sweet smell of benzoin resin, and with obvious vanilla fragrance, The aroma is stronger than the comparative proportion.

Embodiment 2

[0043] The benzoin fragrance comprises the following components by weight:

[0044]

[0045] Step (1) heat-melt the benzoin resin at 80-90° C. for 6 hours, filter while hot with a 200-mesh sieve to obtain the benzoin resin extract, and dissolve the obtained benzoin resin extract in dipropylene glycol;

[0046] In step (2), benzyl benzoate, benzyl acetate, ethyl benzoate and hot-melted vanillin are added sequentially in proportion, stirred while adding, and mixed uniformly to obtain benzoin fragrance.

[0047] Vanillin was melted in a water bath at 100°C for 20 minutes.

[0048] The prepared benzoin fragrance has the strong sweet smell of benzoin resin and vanilla smell similar to the benzoin obtained by steam distillation.

Embodiment 3

[0050] Benzoin perfume comprises the following components by weight:

[0051]

[0052]

[0053]Step (1) heat-melt the benzoin resin at 80-90° C. for 7 hours, filter while hot with a 200-mesh sieve to obtain the benzoin resin extract, and dissolve the obtained benzoin resin extract in dipropylene glycol;

[0054] In step (2), benzyl benzoate, benzyl acetate, ethyl benzoate and hot-melted vanillin are added sequentially in proportion, stirred while adding, and uniformly mixed to obtain benzoin fragrance.

[0055] Vanillin was melted in a water bath at 95°C for 40 minutes.

[0056] The prepared benzoin fragrance has the strong sweet smell of benzoin resin and vanilla smell similar to the benzoin obtained by steam distillation, and the overall aroma intensity is similar to that of the standard product of benzoin.

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Abstract

The invention discloses a benzoin spice and a preparation method thereof. The benzoin spice is prepared from the following components in parts by weight: 45 to 50 parts of benzoin resin, 45 to 50 parts of dipropylene glycol, 1 to 1.5 parts of benzyl benzoate, 0.5 to 1.0 part of ethyl benzoate, 1.0 to 2.0 parts of benzyl acetate and 1 to 3 parts of vanillin. The benzoin spice provided by the invention has the full-bodied fragrant and sweet smells of the benzoin resin and the flavors of a vanilla; according to the preparation method provided by the invention, after being hot melted and filtered, the benzoin resin is mixed with other raw materials; the operation is simple; the cost is lower; the technical problems that benzoin extractum is difficult to transfer and a perfume is not prominent are solved.

Description

technical field [0001] The invention belongs to the technical field of benzoin fragrance, and in particular relates to a benzoin fragrance and a preparation method thereof. Background technique [0002] Benzoin is the Chinese translation of Persian mukul and Arabic aflatoon. It originated in the ancient countries of Anxi, Kucha, Cao, the Arabian Peninsula and the Iranian Plateau in Central Asia. It was named after the Tang and Song Dynasties. "Youyang Zazu" records that benzoin came out of Persia and was used as a medicinal material. "Newly Revised Materia Medica" says: "Benzoin is pungent, fragrant, flat, and non-toxic. It is mainly used by confidants and evil spirits. Xirong is like turpentine, with yellow and black pieces, and the new ones are also flexible." [0003] Benzoin is a mass of compressed spherical particles, ranging in size, reddish-brown to gray-brown outside, embedded with yellow-white and gray-white opaque almond-like particles, and the surface is rough an...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00
CPCC11B9/00C11B9/0003C11B9/0015C11B9/0019C11B9/0061
Inventor 胡翔飞叶志恒
Owner YUNNAN LORRAINE AROMATIC PROD CO LTD
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