Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

A method of rapidly evaluating quality of tobacco essence and spices

A technology for tobacco flavors, flavors and fragrances, which is applied in the directions of measuring devices, material separation, analysis materials, etc., can solve the problems of increased analysis time, difficulty in wide application, and impact on production efficiency, and achieves simplified pretreatment process, simple and fast process, and high efficiency. Contamination-free reproducible effect

Inactive Publication Date: 2016-12-21
CHINA TOBACCO YUNNAN IND +1
View PDF4 Cites 11 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, researchers mainly use chromatographic fingerprints to identify the quality of flavors and fragrances. Although the results are relatively accurate, due to the need to separate the ingredients in flavors and fragrances by chromatography, the analysis time is greatly increased, which affects production efficiency and is difficult to be widely used in industry.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A method of rapidly evaluating quality of tobacco essence and spices
  • A method of rapidly evaluating quality of tobacco essence and spices
  • A method of rapidly evaluating quality of tobacco essence and spices

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Embodiment 1---Evaluate the quality of type A tobacco flavor and fragrance

[0033] (1) Randomly select standard products of 25 production batches of Type A essence and mark them as A1, A2...A25 in turn, and obtain the mass spectrometry fingerprints of each batch of standard products according to the following operations respectively;

[0034] ①Weigh 100mg type A flavor standard and place it in a sealed 22mL headspace bottle, let it stand at room temperature (20°C) for 2min, then insert the solid-phase microextraction fiber DVB / CAR / PDMS into the headspace bottle, (20°C) enrich the sample for 10 minutes;

[0035] ②The chromatographic column in the gas chromatography-mass spectrometer is replaced by a deactivated empty fused silica capillary tube with a length of 5 meters and an inner diameter of 0.25 microns. At this time, the deactivated fused silica capillary tube is used as a connection between the gas chromatograph inlet and the mass spectrometer. transmission line ...

Embodiment 2

[0055] Repeat Example 1, with the following differences:

[0056] (1) Randomly extract 10 production batches of standard products of Type B flavor, and obtain the mass spectrometry fingerprints of each batch of standard products; among them, the solid phase microextraction fiber is DVB / PDMS, and the temperature of the injection port is 270°C. Set time 5min; image 3 It is the mass spectrometry fingerprint of the first batch (B1) standard product of Type B essence;

[0057] (2) The ions that exist in 8 (80% principle) samples are regarded as the common ions of the B-type flavor, and the result is that there are 155 common ions in the B-type flavor of 10 different batches, so finally 10 × 155 matrix (Table 4), where each row represents a sample and each column represents a variable. And the values ​​of the same variable of different samples are averaged to obtain the average value of 155 variables, which is the digital standard mass spectrum fingerprint of type B essence ( F...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a method for quickly evaluating the quality of flavor and fragrance for tobacco. It includes the steps of sample processing of flavors and fragrances, collection of mass spectrum fingerprints of flavors and fragrances without separation, establishment of digital standard mass spectrum fingerprints, determination of similarity thresholds of flavors and fragrances, comparison of similarities of flavors and fragrances to be tested, etc. The invention combines the headspace solid-phase microextraction technology and the non-separation mass spectrometry method to realize the rapid acquisition of the mass spectrum fingerprint of the flavor and fragrance, and then obtains the quality data of the flavor and fragrance by using multivariate statistical analysis, providing a fast method for the quality control of the flavor and fragrance , reliable and stable method can better and more scientifically monitor the quality of flavors and fragrances. The method is applicable to all types of flavors and fragrances for tobacco, including flavors, feed liquids, tinctures, extracts and various flavor raw materials, and has good application prospects.

Description

technical field [0001] The invention belongs to the application field of flavors and fragrances for tobacco, and relates to a method for evaluating the quality of flavors and fragrances for tobacco, in particular to a method for rapidly evaluating the quality of flavors and fragrances for tobacco combined with solid-phase microextraction-mass spectrum fingerprint technology and multivariate statistical analysis technology method. Background technique [0002] Tobacco flavor and fragrance is a mixture made of various additives and appropriate amount of solvents. It is mainly used to make up for the deficiencies in the leaf group formula and to give cigarette products a special aroma style, so that cigarette products have a unique and stable aroma. and smoking flavor, which are closely related to the establishment and development of cigarette brands. Since the 1970s, the rapid development of tobacco technology and analysis technology has led to the discovery of many aromatic ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): G01N30/88G01N30/02G01N30/06G01N30/08
CPCG01N30/88G01N30/02G01N30/06G01N30/08G01N2030/025G01N2030/062G01N2030/8809
Inventor 王明锋廖头根段忆翔朱保昆侯雯倩张翼鹏曾熠程李源栋刘秀明高莉
Owner CHINA TOBACCO YUNNAN IND
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com