Dyeing process of red vegetable dyes

A technology for red plants and dyes, applied in the field of dyeing technology, can solve the problems of reducing the purity of red pigments, unable to produce large-scale production, and increasing costs, and achieve the effects of improving extraction efficiency and extraction volume, facilitating understanding and operation, and reducing production costs.

Active Publication Date: 2017-01-25
义乌市惠侬丝服饰有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Red has been a color that has been loved by the people since ancient times in China. China has long had the technology of extracting red pigment from plants for dyeing, especially safflower; because safflower has medicinal value, so The cloth dyed with its dyes also has certain health effects, but the price of safflower is relatively high at present. If only safflower is used as raw material for dyeing, the cost of dyeing will be increased; and compared with chemically synthesized dyes, the traditional The red dyes produced by the method are unsatisfactory in terms of color uptake and color fixation; at the same time, the manufacturing process of traditional plant dyeing is lengthy and complicated, and the dyeing process and quality are carried out by the experience of workers, which cannot be achieved. mass production
In addition, because safflower contains yellow and red pigments, the yellow pigments need to be removed because they have no dyeing value. At present, yellow pigments are generally removed by using the characteristics of being easily soluble in water and acidic solutions, but the removal effect is not ideal. , causing the extracted red pigment to be doped with yellow pigment, reducing the purity of the red pigment. The traditional red pigment extraction method cannot efficiently extract the red pigment, resulting in part of the red pigment remaining in the safflower cells, resulting in waste of resources and improving Production costs; and because safflower is an annual plant, in order to ensure the normal amount of dye used throughout the year, it is usually necessary to reserve a large amount of safflower, but safflower is prone to deterioration during storage and the red pigment inside it is destroyed
Therefore, the existing technology has problems such as high production cost, unsatisfactory coloring effect, low color fastness, inability to scale production, low red pigment extraction rate, low impurity removal rate and difficult storage of safflower.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Example 1. A kind of preparation technology of red vegetable dye, comprises the following steps:

[0029] a. Soak the safflower cake in an acetic acid solution with a pH value of 5-6 for 60-70 minutes, filter to obtain the A safflower cake, and then decoct the A safflower cake with ebony water at a temperature of 50°C-60°C for 100-150 minutes Minutes to obtain the mixed solution A1 of A safflower cake and ebony water, and then heat the mixed solution A1 to 80℃-90℃ at a speed of 2°C / min-4°C / min, and then continue to decoct for 150-200 minutes to obtain the mixed solution A2, the mixture A2 is filtered and cooled to obtain filter residue A; after multiple treatments, the yellow pigment in the safflower cake can be effectively removed and the purity of the red pigment can be improved.

[0030] b. Put the filter residue A in a plant ash solution with a pH value of 9-11 and a temperature of 25°C-40°C for rinsing for 40-50 minutes, and filter to obtain the dye liquor B1 and ...

Embodiment 2

[0051] Example 2. A kind of preparation technology of red vegetable dye, comprises the following steps:

[0052] a. Soak the safflower cake in an acetic acid solution with a pH value of 5 for 60 minutes, filter to obtain A safflower cake, and then decoct A safflower cake in ebony water at a temperature of 50°C for 100 minutes to obtain A safflower cake and ebony Mixed solution A1 of water, then heated mixed solution A1 to 80°C at a rate of 2°C / min and continued to decoct for 150 minutes to obtain mixed solution A2, which was filtered and cooled to obtain filter residue A;

[0053] b. Put the filter residue A into a plant ash solution with a pH value of 9 and a temperature of 25°C for rinsing for 40 minutes, filter to obtain the dye solution B1 and filter residue b1; put the filter residue b1 into a plant ash solution with a pH value of 9 and a temperature of 50°C Rinse in the solution for 20 minutes, filter to obtain dye liquor B2 and filter residue b2; put filter residue b2 ...

Embodiment 3

[0072] Example 3. A kind of preparation technology of red vegetable dye, comprises the following steps:

[0073] a. Soak the safflower cake in acetic acid solution with a pH value of 6 for 70 minutes, filter to obtain A safflower cake, and then decoct A safflower cake in ebony water at a temperature of 60°C for 150 minutes to obtain A safflower cake and ebony Mixed solution A1 of water, then heated mixed solution A1 to 80°C-90°C at a rate of 4°C / min and then continued to decoct for 200 minutes to obtain mixed solution A2, which was filtered and cooled to obtain filter residue A;

[0074] b. Put the filter residue A into a plant ash solution with a pH value of 11 and a temperature of 40°C for rinsing for 50 minutes, filter to obtain the dye solution B1 and filter residue b1; put the filter residue b1 into a plant ash solution with a pH value of 11 and a temperature of 60°C Rinse in the solution for 30 minutes, filter to obtain dye liquor B2 and filter residue b2; put filter re...

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Abstract

The invention discloses a dyeing process of red vegetable dyes. The process comprises the following steps: a, treating safflower cakes by an acidic solution, so as to obtain a filter residue A; b, rinsing and filtering the filter residue A by an alkaline solution, so as to obtain a dyeing liquor; c, making a dye C1; d, mixing the dye C1 and a dye C2, so as to obtain a dye D; e, mixing the dye D and a weakly alkaline aqueous solution, so as to obtain a dyeing liquor E1 and a dyeing liquor E2; f, respectively pretreating the heated dyeing liquors (E1 and E2), so as to obtain the dyeing liquors (F1 and F2); g, pretreating a silk fabric, so as to obtain a product G; h, adding the product G into the dyeing liquor F1 for dyeing, so as to obtain a product H; i, adding the product H into the dyeing liquor E2 for dyeing, so as to obtain a product I; j, treating the product I, so as to obtain a finished product J. The dyeing process disclosed by the invention has the characteristics of low production cost, good coloring effect, high color fastness, convenience in large-scale production, and capacities of improving the extraction rate of haematochrome and the impurity removal rate and facilitating safflower storage.

Description

technical field [0001] The invention relates to a dyeing process, in particular to a red vegetable dye dyeing process. Background technique [0002] In order to meet the production needs, textile factories use a large number of dyes made of chemical synthetic dyes for dyeing. However, chemically synthesized dyes often contain carcinogenic substances in their raw materials and intermediates, which will have a certain impact on the health of consumers after long-term use. , and the waste will also pollute the environment. Compared with chemically synthesized dyes, plant dyes use pigments from natural plants without adding any chemical substances during the dyeing process, and some natural pigments also have certain health care functions, which are very popular among people. Red has been a color that has been loved by the people since ancient times in China. China has long had the technology of extracting red pigment from plants for dyeing, especially safflower; because safflo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/34D06P1/46D06P1/673D06P1/613D06P3/04D06P5/02C09B67/22C09B61/00
CPCC09B61/00C09B67/0034D06P1/34D06P1/46D06P1/6138D06P1/6735D06P3/04D06P3/045D06P5/02
Inventor 楼听松楼清明
Owner 义乌市惠侬丝服饰有限公司
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