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Acetonitrile production reactor and preparing method thereof

A technology for reactors and acetonitrile, applied in chemical instruments and methods, chemical/physical/physical chemical fixed reactors, methods for chemically changing substances using atmospheric pressure, etc., can solve the problem of damage to stirring devices and easy clogging of feed materials Pipelines, troublesome handling, etc., to prevent the hazards caused by overpressure, facilitate the handling of pipeline blockages, and reduce the effect of connecting devices

Active Publication Date: 2017-02-01
JIANGSU SAILBOAT PETROCHEMICAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In the existing acetonitrile reactor, sodium hydroxide solution and formaldehyde solution are generally directly added to the feed line of the acetonitrile reactor. Since the sodium hydroxide solution and formaldehyde solution contain particles, it is easy to block the feed pipeline and troublesome to deal with.
In addition, the mixing of various materials in the existing acetonitrile reactor is realized through the stirring device in the reactor. The stirring device directly contacts the materials, and the materials will corrode the parts in the stirring device, which may easily cause damage to the stirring device. , short service life, high maintenance cost, and the existing acetonitrile reactor only has a heating system, but no cooling system. If the temperature is too high, it will affect the reaction of acetonitrile and reduce the reaction efficiency

Method used

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  • Acetonitrile production reactor and preparing method thereof
  • Acetonitrile production reactor and preparing method thereof

Examples

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Embodiment 1

[0023] Embodiment 1, a kind of acetonitrile production reactor, is provided with the reactor 1 with jacket, is provided with the clapboard 6 that vertically is arranged in the reactor 1, and the reactor 1 is separated by the clapboard 6 and has two left and right sides that the upper part communicates with each other. The top of each chamber is provided with a feed port 5, and the bottom of each chamber is provided with a discharge port 4. The reactor 1 is provided with a material mixing pipeline connecting the two chambers, which can be connected Two different chambers can also be communicated with the same chamber, and the supply pipelines for supplying sodium hydroxide solution and formaldehyde solution are connected on the material mixing pipeline, and the supply pipelines are provided on the reaction kettle 1. control mechanism.

Embodiment 2

[0024] Embodiment 2, with reference to figure 1 , the acetonitrile production reactor described in embodiment 1, described material mixing pipeline comprises the feed pipe 7 that joins with one chamber top and the discharge pipe 13 that joins with another chamber bottom, discharge A mixing pump 8 is provided between the pipe 13 and the feed pipe 7 .

Embodiment 3

[0025] Embodiment 3, with reference to figure 2 , the acetonitrile production reactor described in embodiment 1, described material mixing pipeline is provided with the backflow pipeline 15 that has backflow pump 16, and the liquid inlet of backflow pipeline 15 is connected with two chambers by liquid outlet split pipeline 17 The bottoms are connected, and the liquid outlet of the return pipe 15 is connected to the tops of the two chambers through the liquid inlet split pipe 14 .

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Abstract

The invention discloses an acetonitrile production reactor and a preparing method thereof. The acetonitrile production reactor comprises a reaction kettle provided with a clamping sleeve. A vertically-arranged partition plate is arranged in the reaction kettle, and the reaction kettle is divided by the partition plate into a left cavity and a right cavity, wherein the upper portion of the left cavity and the upper portion of the right cavity are communicated; feeding inlets are formed in the tops of the cavities, and discharging openings are formed in the bottoms of the cavities; a material mixing pipe for being communicated with the two cavities is arranged on the reaction kettle, feeding pipes for feeding a sodium hydroxide solution and a formaldehyde solution are connected on the material mixing pipe, and a control mechanism for the feeding pipe is arranged on the reaction kettle. According to the acetonitrile production reactor and the preparing method thereof, the two cavities are formed in the reaction kettle, cross flowing of materials in the two cavities is achieved through the material mixing pipe, and all the materials are more fully and evenly mixed; as the sodium-hydroxide-solution feeding pipe and the formaldehyde-solution feeding pipe are additionally arranged on the material mixing pipe, pipe plugging can be conveniently treated.

Description

technical field [0001] The invention relates to chemical equipment, in particular to an acetonitrile production reactor and a preparation method thereof. Background technique [0002] Acetonitrile, also known as methyl cyanide, is a colorless liquid, highly volatile, has a special odor similar to ether, has excellent solvent performance, and can dissolve various organic, inorganic and gaseous substances. It has certain toxicity and is infinitely miscible with water and alcohol. Acetonitrile can undergo typical nitrile reactions and is used to prepare many typical nitrogen-containing compounds. It is an important organic intermediate. Acetonitrile can be used as a solvent for the synthesis of vitamin A, cortisone, carbon amine drugs and their intermediates, and as an active medium solvent for the manufacture of vitamin B1 and amino acids. Can replace chlorinated solvents. It is used in vinyl paints, as an extractant of fatty acids, alcohol denaturants, butadiene extractant...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J19/24B01J3/02
CPCB01J3/006B01J3/02B01J19/0013B01J19/002B01J19/006B01J19/2465B01J2219/00094B01J2219/00686B01J2219/0072B01J2219/00768
Inventor 袁之清吴斌宋国君潘武李建甫
Owner JIANGSU SAILBOAT PETROCHEMICAL CO LTD
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