Patents
Literature
Patsnap Eureka AI that helps you search prior art, draft patents, and assess FTO risks, powered by patent and scientific literature data.

156results about "Sub-atmospheric pressure processes" patented technology

System and method for pulping and sealing carbon dioxide by using coal-based solid waste and mine water

The invention relates to the technical field of mine solid waste treatment and carbon dioxide sealing and storage, and particularly discloses a system and a method for sealing and storing carbon dioxide by utilizing coal-based solid waste and mine water to prepare slurry. The system comprises a cement bin, a gangue bin, a coal ash bin, a gasified slag bin, a mine water storage tank, a stirring reaction kettle, a carbon dioxide storage tank, a slurry temporary storage tank, a vacuum pump and a slurry pump, and the stability and adsorption efficiency of carbon dioxide fixation are improved in the mode that coal-based solid waste, mine water and carbon dioxide are subjected to chemical reaction and physical adsorption; meanwhile, the prepared backfill slurry has high-strength anti-pressure ability, the stability of the backfilled underground goaf is better improved, further, coal-based solid waste and mine water are utilized for waste recycling, and the carbon dioxide storage cost is reduced.
Owner:ORDOS ZHONGYU TAIDE COAL CO LTD +1

Palladium-carbon catalytic hydrogenation reaction material treatment system

The invention relates to the technical field of chemical engineering, and particularly discloses a palladium-carbon catalytic hydrogenation reaction material treatment system, which comprises a three-dimensional workshop structure, an air-operated hoist, an air supply system, an air supply system and an air supply system, wherein the top of the three-dimensional workshop structure is provided with an elevator and a hoisting ton bag; the palladium-carbon circulating unit comprises a palladium-carbon preparation kettle, a hydrogenation reaction kettle, a decarbonization filter, a filter pressing cylinder, a sample splitter and a glove box which are connected in sequence, and the sample splitter is connected back to the palladium-carbon preparation kettle through a closed pipeline; the solid feeding unit comprises a ton bag feeder, a pneumatic valve and a spiral conveying pipe, and the tail end of the solid feeding unit is connected with a top feeding hole of the hydrogenation reaction kettle; the gas supply system comprises a hydrogen cylinder group and is connected to a gas distributor at the bottom of the hydrogenation reaction kettle through a pressure reducing valve and a flow regulating valve; through the multi-stage separation design and the safety interlocking mechanism of the palladium-carbon circulating unit, the recovery rate of the catalyst is increased, meanwhile, the pressure, temperature and stirring state are monitored in real time to trigger nitrogen purging or pressure relief, and the risks of hydrogen leakage and reaction out-of-control are reduced in combination with inert gas protection of the glove box.
Owner:徐致诚

Preparation method and system of high-molecular-weight polyethylene glycol oxalate

The invention relates to a preparation method and system of high-molecular-weight polyethylene glycol oxalate, and the preparation method comprises the following steps: adding oxalic acid diester, ethylene glycol and a first catalyst, and carrying out transesterification to obtain an ester; adding a second catalyst, and carrying out a pre-polycondensation reaction on the esterified product to obtain a glycol oxalate oligomer; polymerizing the ethylene glycol oxalate oligomer, and carrying out final polymerization reaction to obtain polyethylene glycol oxalate; the molar ratio of the oxalic acid diester to the ethylene glycol is (1.05-1.3): 1. Compared with the prior art, by controlling excessive oxalic acid diester in the raw material ratio, namely controlling the molar ratio of oxalic acid diester to ethylene glycol to be greater than 1, the reaction rate of ethylene glycol is improved, self-polycondensation of ethylene glycol is prevented, further increase of molecular weight is facilitated, and meanwhile, the thermal performance of the product is improved.
Owner:SHANGHAI PUJING CHEM NEW MATERIALS

Multifunctional chemical synthesis reaction kettle

ActiveCN120022811AProductsReagents
A multifunctional chemical synthesis reaction kettle belongs to the technical field of chemical synthesis equipment and comprises a reaction kettle body, a reaction kettle cover is arranged at the top end of the reaction kettle body, and a synergistic reaction unit is arranged in an inner cavity of the reaction kettle body; the collaborative reaction unit comprises a reaction bin, the center of the reaction bin and the center of the reaction kettle body are located on the same vertical line, a top plate is installed at the top end of an inner cavity of the reaction bin, and a stirring shaft is rotationally arranged in the center of the reaction bin in the vertical direction. Aiming at the limitation of a traditional chemical synthesis reaction kettle, a vacuum space and dynamic pressure change mechanism is adopted, periodic vacuum pressure change is realized through reciprocating lifting, the static flowing limitation of materials is effectively broken through, the reaction kettle deeply acts on the materials with different viscosities and densities, the problems of non-uniform mixing and dead angles are solved, and mechanical stirring is combined. Double synergistic mixing is achieved, the mixing efficiency and uniformity are remarkably improved, the reaction process is accelerated, and the product quality is guaranteed.
Owner:SHENYANG ZHONGKE ENVRIONMENTAL ENG TECH DEV CO LTD

Interfacial polycondensation tubular reactor for preparing polycarbonate

The invention relates to an interfacial polycondensation tubular reactor for preparing polycarbonate, which is characterized in that a U-shaped structure is adopted, a spiral turbulent flow device is arranged in a straight pipe section, and a high-viscosity melt is disturbed, laminar flow is eliminated and mixing is enhanced in an active or passive mode; a multi-stage independent temperature control module is arranged outside, so that the temperature of each reaction section is accurately regulated and controlled. The inlet, the outlet and the temperature control interface of the reactor adopt high-temperature-resistant and corrosion-resistant sealing design, and U-shaped modular flange connection is convenient for disassembly, assembly, cleaning and continuous expansion. The design solves the problems of non-uniform heat transfer and material residue of a traditional horizontal disc reactor, poor flow distribution of a tubular reactor and the like, and has the following advantages: the melt flow uniformity is improved, and local overheating and excessive polycondensation are avoided; the reaction efficiency and molecular weight distribution are optimized through segmented temperature control; the structure is compact without dead angles, the side reaction and inner wall corrosion risks are reduced, and the device is suitable for efficient continuous synthesis of polycarbonate.
Owner:BEIJING UNIV OF CHEM TECH

Process and equipment for continuously producing high-purity selenium dioxide

The invention relates to the field of inorganic chemical industry production, and discloses a high-purity selenium dioxide continuous production process and equipment, the equipment comprises a cooling crystallization barrel, one side of the cooling crystallization barrel is provided with a selenium dioxide production mechanism, the selenium dioxide production mechanism is used for selenium dioxide production, and the cooling crystallization barrel is provided with a cooling crystallization barrel. An air pressure generation mechanism is arranged outside the cooling crystallization barrel, a gas on-off mechanism is arranged at the top of the air pressure generation mechanism, an air exhaust filtering mechanism is arranged at the top of the cooling crystallization barrel, and a tail barrel is arranged on the side, away from the selenium dioxide production mechanism, of the cooling crystallization barrel; the air pressure generating mechanism is used for keeping the negative pressure state in the cooling crystallization barrel and the tail barrel. According to the selenium dioxide production device, the inside of the feeding pipeline is filled with the materials, so that the materials can be supplemented in time after the materials are consumed, and selenium dioxide can be continuously and efficiently produced, so that the yield and the purity are improved, economic benefits are directly brought, energy waste is avoided, and economic loss is avoided.
Owner:JIANGXI YINGZE ENVIRONMENTAL PROTECTION TECH CO LTD

System and method for the unloading and inertization of tanks used in a physical, chemical and / or biological process

The present invention relates to a system, method, and use for the unloading of solid material particles used in a physical, chemical, and / or biological process in a tank and for the inertization of the tank. The receiving tank and the pump are fluidically connected. The inert gas supply device is fluidically connected to the tank and to at least one injector. The at least one injector is arranged along the transport line that connects the tank to the receiving tank and is configured to inject inert gas into the transport line. The pump is configured to generate negative pressure in the receiving tank and in the tank, and the inert gas supply device is configured to insert inert gas into the tank and supply inert gas to at least one injector, to allow the displacement of solid material particles from the tank to the receiving tank.
Owner:DYNAMIC AIR LTDA

Meltable polytetrafluoroethylene unstable terminal group treatment method and device

The invention relates to the technical field of manufacturing of fusible polytetrafluoroethylene resin, in particular to a method for treating an unstable terminal group of fusible polytetrafluoroethylene, which is used for solving the problem that the unstable terminal group cannot be thoroughly treated in the prior art. The method comprises the following steps: heating fusible polytetrafluoroethylene resin to a molten state, after self-reaction, introducing high-purity fluorine-nitrogen mixed gas to carry out fluoridation reaction, and extracting impurities generated by the reaction to obtain unstable soluble polytetrafluoroethylene resin with a treated terminal group; according to the method, soluble polytetrafluoroethylene resin is heated to a molten state, and unstable terminal groups are thoroughly treated through self-reaction and fluorination reaction.
Owner:SICHUAN HONGHUA IND

Thermochemical gas decomposition reactor system and method for thermochemical decomposition of gas

Thermochemical gas decomposition reactor systems and methods of decomposing gas are disclosed herein. The system includes a reactor including a reaction zone comprising an active material, a gas heating zone, and a gas distribution plate assembly interposed between the reaction zone and the gas heating zone. An exemplary system may include a plurality of reactors. Methods may include providing one or more reactors, and performing one or more of oxidation and / or reduction processes using each of the reactors.
Owner:THE REGENTS OF THE UNIVERSITY OF COLORADO

Reaction device and method for narrow-band light-emitting indium phosphide quantum dots

The invention discloses a narrow-band light-emitting indium phosphide quantum dot reaction device and a method thereof. The reaction device comprises a supergravity device and a photo-thermal device, the supergravity device comprises a shell, a motor, a turntable, a shear filler, a liquid distributor, a reaction cavity, a filler cover, a gas outlet, a liquid outlet and a liquid inlet; the photo-thermal device comprises a laser heating device, a circuit and water cooling device, a reflecting layer and a laser controller; infrared laser is coupled into the supergravity reactor, water or organic matter and other solvent media are used for absorbing infrared light and converting the infrared light into heat energy to increase the temperature of the supergravity reactor, the nucleation reaction of reactant precursors in the micro-droplet reactor is excited, controllable growth of quantum dots in the micro-droplet reactor is achieved, and the quantum dots are obtained. And finally, nano-particles with uniform sizes are obtained by controlling the laser irradiation heating time.
Owner:BEIJING UNIV OF CHEM TECH

Hydrocarbon pyrolysis via joule heating of powder

Systems and methods for producing hydrogen, or gaseous mixtures containing a substantial proportion of hydrogen, by electrical pyrolysis of hydrocarbons, and, more particularly, electrical pyrolysis of methane to produce hydrogen or gaseous mixtures containing a substantial proportion of hydrogen via the use of joule heating of powders and gases. The systems and methods utilize joule heating of powders and gases to enable thermal decomposition of the gases in a volume of electrically conductive powder that is confined inside a joule heated reactor. The systems and methods can be used in the thermal decomposition of methane gas into at least hydrogen gas and carbon inside a reactor, wherein the methane is infused within a volume of gas permeable electrically conductive powder and the heat for the thermal decomposition is provided by joule heating the powder.
Owner:MANCEVSKI VLADIMIR

Reaction kettle for cable adhesive production

The invention relates to the technical field of cable adhesive production, and particularly discloses a reaction kettle for cable adhesive production, which comprises a kettle body and a stirring mechanism, the stirring mechanism comprises a stirring rod and a stirring blade, the stirring rod is rotatably arranged in the kettle body, the stirring blade is connected to the stirring rod, the stirring rod can rotate, and the reaction kettle also comprises an apportionment mechanism, the apportioning mechanism comprises a lifting part and an apportioning part, the lifting part comprises a mounting cylinder, a rotating cylinder and a spiral blade, the mounting cylinder is connected to the kettle body, the rotating cylinder is connected to the stirring rod, the spiral blade is connected to the stirring rod, the apportioning part is mounted on the mounting cylinder, the spiral blade is located in the mounting cylinder, and the mounting cylinder can extend into the upper-layer cable glue; the stirring rod rotates to drive the spiral blade to rotate, so that the spiral blade lifts the cable adhesive upwards and conveys the cable adhesive to the allocation part for allocation; according to the reaction kettle for cable adhesive production, cable adhesive can be conveyed to the allocation part and is allocated, and the speed of eliminating bubbles in the cable adhesive is increased.
Owner:SHANGHAI YININGJU INFORMATION TECHNOLOGY CO LTD +1

Particulate matter drying method, and method for manufacturing drying device

An object is to provide a drying method for continuous processing under reduced pressure, which affords high drying efficiency by bringing about an ideal fluidized state of a process product, the method including, with a median diameter (D50) of a granular starting material ranging from 1 µm to 1000 µm and under reduced pressure at an absolute pressure of 4 to 30, performing a drying treatment by fluidizing the granular starting material, through heating with a heating medium at a temperature 15 to 120°C higher than the boiling point of a solvent in the granular starting material under the above reduced pressure.
Owner:NARA MACHINERY

A reaction device and method for narrow-band luminescent indium phosphide quantum dots

The present invention discloses a reaction device and method for narrow-band luminescent indium phosphide quantum dots. The reaction device comprises a hypergravity device and a photothermal device. The hypergravity device comprises a housing, a motor, a turntable, a shear filler, a liquid distributor, a reaction chamber, a filler cover, a gas outlet, a liquid outlet, and a liquid inlet. The photothermal device comprises a laser heating device, a circuit and a water cooling device, a reflective layer, and a laser controller. The present invention couples an infrared laser into a hypergravity reactor, utilizes a solvent medium such as water or organic matter to absorb the infrared light and convert it into heat energy to increase its temperature, stimulates the nucleation reaction of a reactant precursor in a "micro-droplet reactor", realizes the controllable growth of quantum dots in the micro-droplet reactor, and finally obtains nanoparticles of uniform size by controlling the laser irradiation and heating time.
Owner:BEIJING UNIV OF CHEM TECH

Salting-polymerizing integrated production device and method for bio-based nylon 56

The invention relates to a salification-polymerization integrated production device and a production method of bio-based nylon 56. The device comprises a salification tank, an additive storage tank, a reaction kettle, a vacuum system, a granulator, a drying device and a control system. The control system of the method adopts a PLC (Programmable Logic Controller), the control systems of all main devices are mutually independent and have certain relation, all the devices are divided into different process stages according to different functions in the implementation process, and when the conditions meet the pre-designed process conditions, the system can automatically enter the next process stage without manual intervention. According to the present invention, the bio-based nylon 56 salt solutions with different pH values and different concentrations can be blended, and the blended raw materials are subjected to concentration, polymerization, granulation and drying so as to obtain the integrated polymerization method, such that the time is saved for the subsequent production, the production efficiency is improved, the environmental protection is provided, and the good market prospect and the good development space are provided for the prior art.
Owner:PINGDINGSHAN SHENMA ENG PLASTICS TECH DEV CO LTD

Production apparatus for cyclic esters

A production apparatus for cyclic esters, the production apparatus comprising: a barrel (10), which comprises a material chamber (101), and a feed inlet, a melt outlet (112) and at least one vacuum vent that are in communication with the material chamber (101); a hollow shaft (20) passing through the barrel (10) along a material feeding direction, wherein the hollow shaft (20) is provided with a medium chamber (201) therein; and several hollow disks (30) disposed in the barrel (10) along the feeding direction, wherein the hollow disks (30) are disposed on the outer periphery of the hollow shaft (20); and a medium flow channel (301) in communication with the medium chamber (201) is provided in each hollow disk (30), at least part of the medium flow channel (301) being a spiral from the outside to the inside, and / or the medium flow channel (301) comprising a plurality of parallel medium sub-channels (305). After entering the medium chamber (201), a heat medium flows into the medium flow channels (301) and is uniformly distributed within the hollow disks (30) via the medium flow channels (301). The hollow shaft (20) and the hollow disks (30) cooperate with each other to uniformly heat oligomers in the material chamber (101), thereby avoiding carbonization and coking caused by the non-uniform heating of the oligomers.
Owner:PUJING CHEMICAL INDUSTRY CO LTD

Systems, Methods and Apparatus for Gas Contamination Migration Management

A system and method of preventing reverse migration of contaminant molecules includes an enclosure and a quantity of metal materials included within the enclosure. The quantity of metal materials includes multiple metal material surfaces. The metal material surfaces are conditioned to be attractive to at least a first portion of contaminant molecules. The first portion of contaminant molecules are adsorbed on the multiple metal material surfaces. The enclosure can be a canister with UHP gas flowing from an inlet to an outlet and the first portion of contaminant molecules randomly pass through the canister outlet into the canister.
Owner:MATHESON TRI GAS INC

Device and method for generating glycolonitrile through reaction of gas-phase hydrocyanic acid

The invention discloses a device and a method for generating hydroxyacetonitrile through reaction of gas-phase hydrocyanic acid. The device comprises a hydroxylation reaction tower I and a hydroxylation reaction tower II. Gas-phase hydrocyanic acid enters the first hydroxylation reaction tower from a tower kettle inlet of the first hydroxylation reaction tower to react with a formaldehyde solution, and the proportion, temperature and pH of raw materials and the retention time of the materials in the glycolonitrile reaction kettle are controlled; unreacted gas-phase hydrocyanic acid is conveyed to a tower kettle gas-phase inlet of the second hydroxylation reaction tower from a tower top gas-phase outlet of the second hydroxylation reaction tower to continuously react with fresh formaldehyde, and completely reacted glycolonitrile tower kettle liquid is conveyed to the first hydroxylation reaction tower. According to the invention, gas-phase hydrocyanic acid is directly reacted with formaldehyde, the conditions of the reaction process are controlled, the reaction rate is accelerated, the residence time of tower bottoms is prolonged, meanwhile, the emission of cyanogen-containing waste gas is reduced, the utilization rate of raw materials and the production safety are improved, and the purpose of continuously producing formaldehyde with the content of 1t is achieved; the content of the hydrocyanic acid is less than or equal to 1%.
Owner:SHAANXI TAIFENG YONGXING NEW MATERIAL TECH CO LTD

Polydextrose continuous polymerization production system and method thereof

The invention belongs to the technical field of polydextrose preparation, and relates to a polydextrose continuous polymerization production system and a method thereof. The system comprises a pre-polymerization tank and at least three polymerization tanks which are sequentially communicated through pipelines, the pre-polymerization tank pretreats a mixed solution to be polymerized entering through a feeding pipe, the mixed solution pretreated by the pre-polymerization tank is subjected to continuous polymerization reaction in the polymerization tanks, and polydextrose generated by the polymerization reaction is input to the next procedure through a liquid outlet pipe; a liquid level meter is arranged on the pre-polymerization tank, a liquid conveying pump is arranged on the liquid conveying pipe, a pneumatic control valve is arranged on a high-temperature heat conduction oil inlet pipeline of each polymerization tank, and a thermometer is arranged on each polymerization tank; the frequency of the infusion pump is in signal linkage with the liquid level meter so as to adjust the infusion flow of the infusion pipe, and the pneumatic control valve of each polymerization tank is in signal linkage with the thermometer so as to adjust the polymerization temperature in the tank. The automatic continuous polymerization production of polydextrose is realized, the labor cost is saved, and the production operation is stable.
Owner:ZHEJIANG HUAKANG PHARMA

Reaction device for preparing magnesium hydroxide flame retardant based on gas phase method and preparation method thereof

The invention relates to a reaction device for preparing a magnesium hydroxide flame retardant based on a gas phase method and a preparation method thereof, and belongs to the technical field of chemical engineering equipment and inorganic non-metallic material preparation. The reaction device comprises a precursor precise conveying system, a multi-temperature-zone laminar flow reaction system, an efficient particle collecting system and a central process control system. According to the method, a magnesium source precursor gas-phase flow, a hydrolytic agent gas-phase flow and a surface modifier gas-phase flow are respectively provided by the precursor precision conveying system, are introduced into the multi-temperature-zone laminar flow reaction system through the three coaxial laminar flow nozzles, and are sequentially subjected to controlled mixing in the preheating mixing zone. The whole process is carried out in a gas-phase low-pressure laminar flow environment, hard agglomeration of particles is effectively avoided, the prepared magnesium hydroxide flame retardant has the advantages of being uniform in primary particle size, good in dispersity and high in surface organification degree, and the compatibility and flame retardant efficiency of the magnesium hydroxide flame retardant in a polymer matrix are remarkably improved.
Owner:YINGKOU DONGTENG NEW MATERIALS CO LTD

Energy-saving and consumption-reducing system and method based on alkoxylation device

The invention discloses an energy-saving and consumption-reducing system and method based on an alkoxylation device.The system comprises a pretreatment kettle, the discharging end of the bottom of the pretreatment kettle is communicated with the top of the pretreatment kettle sequentially through a pretreatment kettle outer circulating pump and a pretreatment kettle outer circulating heater, and the discharging end of the pretreatment kettle outer circulating pump is further communicated with a reaction kettle; the bottom discharge end of the reaction kettle is sequentially communicated with a reaction kettle circulating pump and a reaction kettle circulating heat exchanger, the discharge end of the reaction kettle circulating heat exchanger is respectively communicated with the reaction kettle and a gas-liquid mixer, and the discharge end of the reaction kettle circulating heat exchanger is also communicated with a reaction heat recovery system; the discharging end of the reaction kettle circulating pump is also communicated with the feeding end of a post-treatment kettle, and the bottom of the post-treatment kettle is provided with a discharging end; the method comprises the steps of pretreatment, alkylation reaction, aftertreatment and tail gas washing. According to the scheme, the energy-saving and consumption-reducing effects are remarkable.
Owner:LEVIMA ADVANCED MATERIALS CORP

Portable flexible vacuumizing and inert mixed gas filling device

The invention discloses a portable flexible vacuumizing and inert gas mixture filling device, and relates to the technical field of catalyst preparation, the portable flexible vacuumizing and inert gas mixture filling device comprises a vacuum box, an air extractor and an inert gas generator, the air exhauster and the inert gas generator are connected with the vacuum box through pipelines. Through mutual cooperation of the vacuum box, the air extractor and the inert gas generator, the vacuum box is vacuumized through the air extractor, then the vacuum box is filled with inert gas generated by the inert gas generator all the time, and it is ensured that no oxygen is left in the vacuum box when a conductive carrier such as foamed nickel or carbon cloth passes through the vacuum box; the problem that oxygen participates in the catalyst heating process in the electrode production process of an existing water electrolyzer, and the quality of an electrode product is affected is effectively solved.
Owner:TAIZHOU UNIV

Multifunctional vacuum material neutralization tank

The invention discloses a multifunctional vacuum material neutralization tank which comprises a tank body, a spherical seal head is arranged at the bottom end of the tank body, and a downward discharge hole is formed in the center of the spherical seal head; the stirring device comprises a driving motor, a stirring shaft and a stirring paddle mounted on the stirring shaft, the stirring shaft is transversely mounted in the tank body through a sealing assembly, the driving motor is mounted on one side of the tank body and is in driving connection with the stirring shaft through a reduction gear set, and the stirring paddle is mounted on the stirring shaft in the tank body. The stirring paddles are arranged along the circumferential direction of the stirring shaft and are in arc-shaped fit with the inner wall of the spherical sealing head; the spraying device is arranged in the tank body, is positioned above the stirring device, and comprises a plurality of nozzles which are arranged in rows and are provided with downward spouts; the cleaning device is arranged at the top of the inner cavity of the tank body and comprises a rotary cleaning ball head. The vacuum tank has the beneficial effects that the environment in the tank can reach a more ideal vacuum state and a more ideal sealing effect; and the materials are prevented from blocking the discharging hole, and the tank body can be automatically cleaned.
Owner:SHANGHAI BEYOND MACHINERY

A single-component silicone sealant for solar photovoltaic modules and a preparation method thereof

The application discloses a single-component organic silicon sealant for solar photovoltaic modules and a preparation method thereof, and relates to the technical field of high polymer materials. The single-component organic silicon sealant for solar photovoltaic modules is prepared by mixing 107 silicon oil, reinforcing fillers, a silane coupling agent, a catalyst and a cross-linking agent. The preparation method of the single-component organic silicon sealant for solar photovoltaic modules is realized by a preparation device of the single-component organic silicon sealant for solar photovoltaic modules. The preparation device of the single-component organic silicon sealant for solar photovoltaic modules comprises a reaction kettle. The application can form a continuously shrinking closed space in the reaction kettle, thereby shortening the time required for vacuumizing treatment. Nitrogen can be input into the material from the lower part of the material, thereby effectively improving the heat exchange area of nitrogen and the material, improving the material cooling speed, and thereby obviously improving the preparation efficiency of 107 silicon oil.
Owner:JIANGXI OPT IND CO LTD

Ammonia reaction control method and system for vacuum pushed slab kiln

The invention discloses an ammonia reaction control method and system for a vacuum pushed slab kiln, and belongs to the technical field of special furnaces for chemical engineering, and the method is characterized by comprising the following steps: acquiring sensor data at the current moment; the push plate offset and the material offset are obtained according to the sensor data; according to the push plate offset and the material offset, the residual reaction amount of the current functional area is obtained; the concentration of at least one ventilation pipe in the current functional area is adjusted according to the residual reaction amount, the vacuum pushed slab kiln comprises a plurality of functional areas, each functional area comprises a plurality of ventilation pipes, and all the ventilation pipes are connected with gas storage tanks with different concentrations. The offset of the material is obtained, and the ammonia concentration is adjusted according to the offset of the material, so that the reaction quality of the material is ensured, the loss of the material in the preparation process is reduced, and the production resources and the production time are saved.
Owner:PANZHIHUA JINFENG VANADIUM & TITANIUM TECH CO LTD

Synthesis method and synthesis device of solution type polyurethane

The invention belongs to the technical field of polyurethane synthesis, and particularly relates to a synthesis method and a synthesis device of solution type polyurethane. The device comprises a vacuum reaction kettle; the first vacuum material barrel and the second vacuum material barrel are respectively communicated with the vacuum reaction kettle; and the dry nitrogen supply and discharge device is used for continuously inputting nitrogen into the vacuum reaction kettle in the reaction process and simultaneously discharging mixed gas formed in the vacuum reaction kettle. When the device is used for synthesizing solution type polyurethane, the influence of by-product gas, oxygen and moisture in a polymerization reaction on reactants can be reduced, and the labor cost caused by frequent sampling detection in a polyurethane reaction process is reduced.
Owner:稳健医疗(武汉)有限公司

Material dissolution reaction monitoring method, monitoring device and material dissolution reaction system

The present application belongs to the technical field of industrial control, and discloses a material dissolving reaction monitoring method, a monitoring device and a material dissolving reaction system. The material dissolving reaction monitoring method comprises the following steps: based on a reaction equation, calculating a first gas mass of a gas generated in a dissolving reaction according to the mass of all materials; making the environment in a dissolving tank reach a target environment; in the dissolving reaction, when a preset condition is met, making the vacuum degree in the dissolving tank and the vacuum degree in the dissolving tank before the dissolving reaction be the same, calculating the difference between a first mass before the dissolving reaction and a second mass in the dissolving reaction to obtain a second gas mass, the first mass and the second mass being the sum of the mass of the dissolving tank, a first reaction material and a second reaction material, when the difference between the first gas mass and the second gas mass is less than or equal to a preset threshold, determining that the dissolving reaction is completed, otherwise, determining that the dissolving reaction is not completed. The present application can effectively determine whether the dissolving reaction is completed.
Owner:GUANGDONG SOPHON INTELLIGENT TECH CO LTD

System for producing glycolide with low-concentration depolymerization waste gas, preparation method and obtained glycolide

The invention provides a system for producing glycolide with low-concentration depolymerization waste gas, a preparation method and the obtained glycolide. The system comprises a polycondensation reaction kettle, a mixer and a depolymerization reactor, the polycondensation reaction kettle is connected with the mixer, the mixer is provided with an additive adding port, and the mixer is connected with the depolymerization reactor. The preparation method comprises the following steps: reacting a glycollic acid aqueous solution in a polycondensation reaction kettle in the presence of a catalyst to obtain a glycollic acid oligomer; and respectively adding the obtained glycolic acid oligomer and terphenyl and / or a hydrogenated product thereof into a mixer for mixing, then continuously adding into a depolymerization reactor for depolymerization reaction to obtain glycolide, and discharging depolymerization waste gas at the same time. According to the invention, decarboxylation side reaction and thermal degradation side reaction during depolymerization reaction can be inhibited, and generation of by-products such as CO2 and aldehyde ketonic acid small molecular organic matters in depolymerization waste gas can be reduced.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

Trihydroxy stearin as well as preparation process and application thereof

The invention belongs to the technical field of chemical processes, and discloses trihydroxy stearin and a preparation process and application thereof.The trihydroxy stearin comprises a reaction tank connected with a mounting frame and used for mounting and fixing the reaction tank; the tank cover is connected to the reaction tank; the driving structure is connected to the tank cover, and one end of the driving structure is located in the reaction tank; the driving structure comprises a first driving part and is connected with a stirring shaft, a first stirring block and a second stirring block are arranged on the outer side of the stirring shaft and are used for stirring and mixing raw materials in the reaction tank, and a first adjusting structure is arranged on the stirring shaft, the first stirring block and the second stirring block. By adjusting the action of the first stirring block and the adjusting block, the stirring mode is changed according to materials with different viscosities in the reaction tank, so that the materials can be fully mixed and reacted, the overall stirring effect is improved, and the preparation efficiency of the trihydroxy stearin is conveniently improved.
Owner:GUANGZHOU YINGTEMAN BIOTECHNOLOGY CO LTD