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57results about How to "High surface coverage" patented technology

Preparation of silver-doped nickel oxide film and application of nickel oxide film in perovskite solar cell as hole transport layer

The invention provides preparation of a silver-doped nickel oxide film and an application of the nickel oxide film in a perovskite solar cell as a hole transport layer. The preparation of the silver-doped nickel oxide film includes: dissolving nickel nitrate hexahydrate and silver nitrate in a diethylamine-containing glycol solution, stirring the mixture at a room temperature for 12-16 h, preparing a mixed precursor solution of nickel nitrate and silver nitrate with the metallic ion total concentration of 0.5-1.5 M, wherein the ratio of Ag to Ni is 1-2:100; and performing spin coating of the mixed precursor solution of nickel nitrate and silver nitrate on a substrate with the rotating speed of 2500-3500 rmp, and then performing heating at the temperature of 300 DEG C for 60-80 min. According to the silver-doped nickel oxide film, the light transmission and the hole transport capability are better, the degree of crystallization and the surface coverage rate of the perovskite film grown on the silver-doped nickel oxide film are higher compared with the pure nickel oxide film, and the reverse planar perovskite solar cell prepared by the nickel oxide film as the hole transport layer is advantaged by higher photoelectric conversion efficiency and environmental stability.
Owner:NANCHANG UNIV

Method and device for repairing concrete crack by pulse electrodeposition

The invention discloses a method for repairing a concrete crack by means of pulse electrodeposition, wherein a reinforcing steel bar in concrete is taken as a cathode and a titanium screen is taken as an anode, and the reinforcing steel bar and the titanium screen are arranged near the concrete; a 0.05-0.50 mol per liter zinc saline solution or magnesium saline solution is taken as an electrodeposition solution, and the concrete is immersed into the electrodeposition solution; a pulse power source is adopted, and the on/off time of pulse is between 0.6 and 1 ms; the current density exerted on the surface of the concrete is between 0.25 and 3 amperes per square meter; and the concrete provided with the crack is repaired by means of electrodeposition. The invention also discloses an applicable device for the method for repairing the concrete crack by means of pulse electrodeposition. The method for repairing the concrete crack by means of pulse electrodeposition and the repairing device thereof have the advantages of simple structure, convenient operation, low cost, good effect and so on, and are suitable for concrete structures in a water environment and concrete structures which are difficult to be repaired by the prior repairing technology or have high repairing cost.
Owner:HOHAI UNIV

Viscosity reduction type polycarboxylate superplasticizer with microcrosslinking structure and preparation method of viscosity reduction type polycarboxylate superplasticizer

The invention discloses a viscosity reduction type polycarboxylate superplasticizer with a microcrosslinking structure. The viscosity reduction type polycarboxylate superplasticizer is prepared from unsaturated acids, unsaturated anhydride, isopentene polyoxyethylene ether, a crosslinking agent and a reactive cosolvent as polymerization raw materials through free radical pauperization under actions of an initiator and chain transfer, components and structures take mutual synergetic effects into play, and compared with a viscosity reduction type polycarboxylate superplasticizer synthesized in the prior art, the viscosity reduction type polycarboxylate superplasticizer has an excellent viscosity reduction effect and has collapse prevention and regulation and control on early strength functions as well; meanwhile, due to introduction of the structure, the thickness of an adsorption layer on the surface of cement granules can be increased, the cement granule surface covering rate can be increased, the concentration of the polycarboxylate superplasticizer retained in a cement pore liquid can be reduced, surface activation performance of the polycarboxylate superplasticizer can be enhanced, and a good viscosity reduction effect can be achieved. Due to adoption of the reactive cosolvent, the intermiscibility of monomers can be effectively improved, and the polymerization efficiency ofa polymer and structure arrangement of effective molecules can be improved. Due to adoption of a bifunctionality crosslinking agent in the polycarboxylate superplasticizer, the molecular structure ofthe polycarboxylate superplasticizer can be improved, and the viscosity reduction performance of the polycarboxylate superplasticizer can be improved.
Owner:CHINA WEST CONSTR GRP +2

Preparation method of fluorescent coding microsphere coated with metal nano shell layer

The invention provides a preparation method of a fluorescent coding microsphere coated with a metal nano shell layer. Different types of fluorescent materials with different contents are doped into a polymer microsphere by using a metal nano material modified with a certain ligand as a new surfactant in an emulsification process through an SPG method so as to prepare the fluorescent coding microsphere with different fluorescent coding signals inside and uniformly coated with the metal nano shell layer on the surface in one step. The prepared fluorescence coding microsphere comprises the metal nano shell layer, a polymer and a fluorescence coding material, the particle size of the fluorescence coding microsphere is 1-20 [mu]m, the coefficient of variation (CV) is less than 10%, and the fluorescence coding microsphere can be used for detecting protein / nucleic acid. The preparation method is simple in preparation process, high in surface coating rate, good in uniformity and controllable in LSPR peak, and the problems of low surface coating rate, poor uniformity, complex preparation process, uncontrollable local surface plasma resonance (LSPR) peak and the like in the current common precious metal nano shell coating method are solved.
Owner:HANGZHOU SHINEDO BIOTECH CO LTD

Perovskite LED taking ZnO nanometer wall network as electron injecting layer and preparation method thereof

ActiveCN105789398AHigh surface coverageEfficient Radiative RecombinationSemiconductor devicesQuantum efficiencyGeneration rate
The present invention provides a perovskite LED taking a ZnO nanometer wall network as an electron injecting layer and a preparation method thereof. The perovskite LED taking the ZnO nanometer wall network as the electron injecting layer and the preparation method thereof are able to effectively limit the generation of drain current in a device, reduce the generation rate of nonradiative recombination of a carrier, and finally realize the preparation of a high-external quantum efficiency perovskite green ray LED. The perovskite LED comprises a transparent conductive substrate, and the substrate is provided with an n-type ZnO nanometer wall network, a CH3NH3PbBr3 luminescent layer, a p-type cavity supplying layer and an electrode. The perovskite LED taking the ZnO nanometer wall network as the electron injecting layer and the preparation method thereof employ a two-dimensional ZnO nanometer wall network as the electron injecting layer of the perovskite green ray LED and adopt the nanometer wall network frame structure to limit the diffusion of the perovskite forerunner liquid in the stage of the solvent drying so as to improve the surface coverage rate of the CH3NH3PbBr3 luminescent layer. Besides, the defect of a traditional perovskite LED is overcome, the generation channel of drain current in a device is effectively inhibited, and the efficient radiative recombination of carriers in the condition of the electron injection is prompted.
Owner:ZHENGZHOU UNIV

Alkali metal air chamber manufacturing method for improving relaxation resistance of coating based on Plasma hydroxylation

ActiveCN109518177AReduce pollutionImproved anti-relaxation propertiesMetallic material coating processesProblem of timeEngineering
The invention relates to an alkali metal air chamber manufacturing method for improving the relaxation resistance of a coating based on Plasma hydroxylation. According to the method, a plasma cleaningmachine is adopted for hydroxylating the inner surface of an air chamber; since a tail pipe of the alkali metal air chamber is thin, the operation that a thick cleaning solution needs to be extractedby adopting a capillary glass tube after cleaning through a traditional hydroxylation method is omitted, so that the air chamber is prevented from being pricked during a cleaning solution extractionprocess, and the problems of time waste, effort waste, nonideal consistency and nonideal relaxation resistance during the current air chamber manufacturing process are solved; and meanwhile, more hydroxide radicals can be formed on the glass surface, and no cleaning solution removal and follow-up drying is needed, so that the contact time of the hydroxide radicals and the outside environment is shortened, the hydroxide radical pollution is reduced, more hydroxide radical number can be maintained, a smooth and uniform covering surface is realized during the organochlorosilane reaction process,the surface covering rate on paramagnetic impurities is increased, and the relaxation resistance of the coating is improved. In addition, multiple air chambers can be processed at the same time, so that the consistency and the repeatability in manufacturing the coating are improved.
Owner:杭州诺驰生命科学有限公司

Method for Producing Structured Sintered Connection Layers, and Semiconductor Element Having a Structured Sintered Connection Layer

ActiveUS20140225274A1Satisfactory electric connectionSatisfactory thermal connectionSemiconductor/solid-state device detailsSolid-state devicesSurface coverMechanical tension
A method for producing a sinter layer connection between a substrate and a chip resulting in an electric and thermal connection therebetween and in reduced mechanical tensions within the chip. The method produces a sinter layer by applying a multitude of sinter elements of a base material forming the sinter layer in structured manner on a contact area of a main surface of a substrate; placing a chip to be joined to the substrate on the sinter elements; and heating and compressing the sinter elements to produce a structured sinter layer connecting the substrate and chip and extending within the contact area, the surface coverage density of the sinter elements on the substrate in a center region of the contact area being greater than the surface coverage density of the sinter elements in an edge region of the contact area, and at least one through channel, extending laterally as to the substrate's main surface being provided towards the contact area's edge. A large-area sinter element is situated in the contact area's center region, and circular sinter elements is situated in a contact area edge region. The sinter elements may also have notches. Also described is a related device.
Owner:ROBERT BOSCH GMBH

Inorganic low smoke zero halogen fire retardant and preparation method thereof

The invention relates to an inorganic low smoke zero halogen fire retardant and a preparation method thereof, which relates to surface modification processing and a processing method of the inorganic fire retardant and the method for preparing the low smoke zero halogen fire retardant. The method includes starting a heating system, enabling temperature to reach 80-260 DEG C which is required by process requirements, starting a continuous activation machine, adding 0.1 micrometer to 100 micrometer inorganic fire retardant into a feeding system, stably and evenly conveying materials to the activation chamber through the feeding system, conveying mixed liquid composed of coupling agents, adsorbents and dispersing agents dosed through a metering device to a nozzle, spraying the active agents into the active chamber quantitatively through the nozzle, completely mixing the inorganic fire retardants and the active agents under the processing temperature of 80 DEG C to 260 DEG C through an agitator blade of 2000 to 4000 turn / min, processing materials in the active chamber for 5 to 20 minutes and obtaining products through a dust removing system. The products of the fire retardant and the preparation method are good in quality stability, short in product production period, low in cost and friendly to environment and human.
Owner:大连亚泰科技新材料股份有限公司
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