Composition, film, preparation method and detection method for ultraviolet light intensity detection
A technology of intensity detection and ultraviolet light, applied in the field of optical detection, can solve problems such as limited area and complicated detection process
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[0067] see image 3 , the present invention also provides a method for preparing a thin film to prepare and provide the above-mentioned thin film; the preparation method includes:
[0068] In the first step, the photopolymerizable monomer, the photoinitiator, the cholesteric liquid crystal, the azobenzene-based monomer, the nematic mixed crystal and the chiral additive are mixed to form a mixed system;
[0069] In the second step, the mixed system is spread to form a prefabricated film layer of the mixed system, and the prefabricated film layer of the mixed system is irradiated with light, so that the photoinitiator in the mixed system initiates the polymerization of the photopolymerizable monomers to obtain a UV Thin films for light intensity detection.
[0070] Compared with the prior art, the preparation method of the film provided by the present invention has the same beneficial effect as the composition provided, and will not be repeated here.
[0071] It is worth notin...
Embodiment 1
[0086] The composition for ultraviolet light intensity detection provided in this example includes nematic mixed crystals, chiral additives, azobenzene-based monomers, photopolymerizable monomers and benzoin dimethyl ether; nematic mixed crystals The mass ratio of , chiral additive, azobenzene monomer, photopolymerizable monomer and benzoin dimethyl ether is 71.3:8:5:15.2:0.5.
[0087] Nematic mixed crystal is SLC-1717, manufacturer: Shijiazhuang Chengzhi Yonghua Display Materials Co., Ltd.
[0088] Chiral additives are:
[0089]
[0090] Azobenzene monomers are:
[0091]
[0092] The photopolymerizable monomers are:
[0093]
[0094] see image 3 , this embodiment also provides a film for ultraviolet light intensity detection, the film includes the composition for ultraviolet light intensity detection, and its preparation method is as follows:
[0095] In the first step, according to the mass ratio of 71.3:8:5:15.2:0.5, nematic mixed crystals, chiral additives, a...
Embodiment 2
[0099] The composition for ultraviolet light intensity detection provided in this embodiment includes nematic mixed crystals, chiral additives, cholesteric liquid crystals, azobenzene-based monomers, photopolymerizable monomers and photoinitiators; nematic The mass ratio of mixed crystal, chiral additive, cholesteric liquid crystal, azobenzene monomer, photopolymer monomer and benzoin ether is 26:19:20:11:22:2.
[0100] Nematic mixed crystal is MAT 09-1284, manufacturer: Merck, Germany.
[0101] Chiral additives include the following two chiral additives with a mass ratio of 1:1:
[0102]
[0103] The cholesteric liquid crystal is:
[0104]
[0105] Azobenzene monomers are:
[0106]
[0107] The photopolymerizable monomers are:
[0108]
[0109] see image 3 , this embodiment also provides a film for ultraviolet light intensity detection, the film is a network structure, which includes the composition for ultraviolet light intensity detection, and its preparati...
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