Method for detecting ethanol in live bacteria type lactic acid bacteria beverage
A technology of lactic acid bacteria beverage and ethanol, which is applied in the direction of measuring devices, material separation, and analysis of materials, etc., can solve the problems of ethanol that need to be improved, and achieve the effects of fast operation, high precision, and strong accuracy
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Embodiment 1
[0055] In this embodiment, the ethanol in the live bacteria type lactic acid bacteria beverage is detected through the following steps:
[0056] The first step is to draw 5mL live lactic acid bacteria beverage test sample into a 25mL volumetric flask, dilute to the mark with acetonitrile, mix well, centrifuge at 5000rpm for 5 minutes, collect the supernatant, and pass through a 0.22μm organic filter membrane. Obtain the solution to be tested.
[0057] In the second step, the liquid to be tested is detected by gas chromatography:
[0058] (1) Determine the detection limit of gas chromatography
[0059] The ethanol can be qualitatively determined by a 3-fold signal-to-noise ratio (S / N=3), and the ethanol can be quantified by a 10-fold signal-to-noise ratio (S / N=10). When the content is 2mg / 100mL, the peak height signal is 2146.8, the noise is 70, and the signal-to-noise ratio at this time is 30.7. Based on 10 times the signal-to-noise ratio, the quantitative detection limit of...
Embodiment 2
[0069] Detect ethanol in the live bacteria type lactic acid bacteria beverage according to the method of Example 1, the difference is that in the first step,
[0070] Draw 5mL of live bacteria type lactic acid bacteria beverage to be tested into a 10mL volumetric flask;
[0071] Centrifugation is carried out at a speed of 3000r / min for 10 minutes.
Embodiment 3
[0073] Detect ethanol in the live bacteria type lactic acid bacteria beverage according to the method of Example 1, the difference is that in the first step,
[0074] Draw 5mL of live bacteria type lactic acid bacteria beverage to be tested into a 50mL volumetric flask;
[0075] Centrifugation is carried out at a speed of 8000r / min for 3 minutes.
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