Fast disintegrating nonwoven binder
A non-woven and adhesive technology, used in non-woven fabrics, textiles and papermaking, preparations for skin care, etc., can solve problems such as inability to disperse, difficult to transport, and must be prepared on site
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[0044] all abbreviations used
[0045] AA = acrylic acid
[0046] EA = ethyl acrylate
[0047] IA = itaconic acid
[0048] MMA = methyl methacrylate
[0049] Sty = styrene
[0050] polymer synthesis
[0051] To a 5000 ml round bottom flask equipped with a stir bar, condenser, temperature monitor, heating mantle and nitrogen inlet was added 1850 grams of deionized water which was subsequently heated to 85°C. A monomer premix was prepared from 800 grams of deionized water, 26.7 grams of Disponil FES 993 (polyethylene glycol ether sulfate sodium salt), 8.0 grams of itaconic acid, 16.0 grams of styrene, 1424 grams of ethyl acrylate, and 152 grams of glacial acrylic acid. With the reactor water at 84°C, 7.2 grams of ammonium persulfate (APS) dissolved in 51 grams of water were added. The premix feed was started at 12.1 g / min. After 20 minutes, the feed rate was increased to 24.3 g / min. Simultaneously, a feed of 2.4 grams of ammonium persulfate dissolved in 200 grams of ...
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