Unlock instant, AI-driven research and patent intelligence for your innovation.

A method for separating coking dry gas

A technology for coking dry gas and catalytic hydrogenation, which is applied in the processing of gas mixtures, hydrocarbon oil treatment, petroleum industry, etc., and can solve the problems of large circulating amount of C4 absorbent, small circulating amount of C4 absorbent, and large investment. , to achieve the effect of low cost, reduced circulation and less investment

Active Publication Date: 2018-09-21
CHINA PETROLEUM & CHEM CORP +1
View PDF5 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] The purpose of the present invention is to provide a method for separating coking dry gas in order to overcome the problems of large investment, high energy consumption, and large circulation of carbon four absorbents in the existing method for separating coking dry gas in refineries. Small investment, low energy consumption, small carbon four absorbent circulation, etc.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A method for separating coking dry gas
  • A method for separating coking dry gas

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0044] This example is used to illustrate the method for separating coking dry gas of the present invention.

[0045] The coking dry gas with a pressure of 0.6MPaG from the delayed coking unit of the refinery is supplied to the dry gas compressor 1, and the pressure of the dry gas is increased to 4MPaG after three-stage compression treatment. Then the dry gas after the pressurization is supplied to the hydrogenation reactor 2, and the hydrogenation catalyst Co-Mo-Ni series catalyst (purchased from Beijing Research Institute of Chemical Industry, China Petrochemical Corporation, model BY-5) is contacted to catalyze For hydrogenation reaction, control the reaction temperature at 180°C, the reaction pressure at 4MPaG, and the volumetric space velocity at 100h -1 , The molar content of ethylene in the hydrogenation reactor 2 outlet gas was reduced to 0.1%. Then the outlet gas of the hydrogenation reactor 2 is cooled to 15° C. through the dry gas cooler 3 with 7° C. cold water pre...

Embodiment 2

[0053] This example is used to illustrate the method for separating coking dry gas of the present invention.

[0054] The coking dry gas with a pressure of 0.6MPaG from the delayed coking unit of the refinery is supplied to the dry gas compressor 1, and the pressure of the dry gas is increased to 3MPaG after three-stage compression treatment. Then the dry gas after the pressurization is supplied to the hydrogenation reactor 2, and a catalytic hydrogenation reaction occurs in contact with the hydrogenation catalyst Ni-based catalyst (purchased from Beijing Research Institute of Chemical Industry, China Petrochemical Corporation, model YN-1), Control the reaction temperature to 220°C, the reaction pressure to 3MPaG, and the volumetric space velocity to 500h -1 , The molar content of ethylene in the hydrogenation reactor 2 outlet gas was reduced to 0.1%. Then the outlet gas of the hydrogenation reactor 2 is cooled to 10° C. through the dry gas cooler 3 with 7° C. cold water prep...

Embodiment 3

[0062] This example is used to illustrate the method for separating coking dry gas of the present invention.

[0063] The coking dry gas with a pressure of 0.6 MPaG from the delayed coking unit of the refinery is supplied to the dry gas compressor 1, and the pressure of the dry gas is increased to 5 MPaG after three-stage compression treatment. Then the dry gas after the pressurization is supplied to the hydrogenation reactor 2, and the catalytic hydrogenation reaction occurs in contact with the hydrogenation catalyst Ni-based catalyst (purchased from Beijing Research Institute of Chemical Industry, China Petrochemical Corporation, model YN-S), Control the reaction temperature to 150°C, the reaction pressure to 5MPaG, and the volumetric space velocity to 400h -1 , The molar content of ethylene in the hydrogenation reactor 2 outlet gas was reduced to 0.1%. Then the outlet gas of the hydrogenation reactor 2 is cooled to 15° C. through the dry gas cooler 3 with 7° C. cold water ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
recovery rateaaaaaaaaaa
recovery rateaaaaaaaaaa
Login to View More

Abstract

The invention relates to the field of dry gas treatment and discloses a method for separating coking dry gas. The method comprises orderly carrying out catalytic hydrogenation, cooling treatment and C4 sorbent-based absorption treatment on coking dry gas, respectively carrying out gasoline sorbent-based absorption and C4 desorption treatment on a gas phase material and a liquid phase material obtained by the C4 sorbent-based absorption treatment, recovering a gas phase material obtained by C4 desorption treatment, returning a liquid phase material obtained by C4 desorption treatment into a C4 sorbent and carrying out absorption treatment. The method has the characteristics of small investment, low energy consumption and small circulation amount of the C4 absorbent.

Description

technical field [0001] The invention relates to the field of dry gas treatment, in particular to a method for separating coking dry gas. Background technique [0002] Refinery coking dry gas comes from the delayed coking unit of the refinery. Usually, the molar content of ethane in coking dry gas is about 20%, the molar content of ethylene is above 2%, and the remaining components are methane, hydrogen, propane, saturated water, etc. At present, coking dry gas in refineries is mainly burned as fuel, and its utilization value is low. If the ethane component in the coking dry gas is recovered and sent to the ethylene plant as the raw material for the ethane cracking furnace, the cracking raw material oil can be saved, the production cost of ethylene can be reduced, and the economic and social benefits are very obvious. [0003] At present, the methods for recovering carbon two components from coking dry gas in refineries mainly include cryogenic separation method, pressure sw...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C10G70/02C10G70/04C10G70/06
CPCC10G70/02C10G70/043C10G70/06C10G2300/10
Inventor 邵华伟李东风刘智信张敬升邹弋胡志彦杜周柴忠义
Owner CHINA PETROLEUM & CHEM CORP