A kind of high-brightness marking paint and preparation method thereof
A marking paint and paint technology, applied in the field of transportation, can solve the problems of reducing the brightness and reflective effect of marking paint, reducing the reflective ability of road markings, and poor compatibility of marking paint, so as to reduce the surface of marking Energy, improve surface properties, improve the effect of gloss
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Embodiment 1
[0023] Component A: DEGAROUTE®465 150g, titanium dioxide 100g, organobentonite 1.5g, vinyltriethoxysilane 50g, triethoxysilane 25g, Shuangfei powder 173.5g, total 500g.
[0024] Add titanium dioxide and organic bentonite to DEGAROUTE®465 and mix well, add Shuangfei powder and stir well, transfer to a sand mill for grinding, after the dispersion is uniform, add vinyltriethoxysilane and triethoxysilane, Continue to stir evenly, and filter to obtain component A.
[0025] Component B: DEGAROUTE®469 150g, titanium dioxide 100g, organic bentonite 1.5g, dibenzoyl peroxide 10g, Shuangfei powder 238.5g, total 500g.
[0026] Add titanium dioxide and organic bentonite to DEGAROUTE®469 and mix well, then add Shuangfei powder and stir well, transfer to a sand mill for grinding, after the dispersion is uniform, add dibenzoyl peroxide and stir evenly, filter to obtain component B .
[0027] The particle size range is 30-100 mesh, and the density is 2.4-2.6g / cm 3 , glass microspheres with ...
Embodiment 2
[0030] Component A: DEGAROUTE®655 150g, titanium dioxide 100g, organobentonite 1.5g, vinyltriethoxysilane 25g, triethoxysilane 50g, Shuangfei powder 173.5g, total 500g. The preparation method is the same as in Example 1.
[0031] Component B: DEGAROUTE®659 200g, titanium dioxide 50g, organic bentonite 1.0g, dibenzoyl peroxide 15g, Shuangfei powder 234g, total 500g. The preparation method is the same as in Example 1.
[0032] Take glass microspheres and add them to aqueous hydrochloric acid solution with a pH value of 4, heat and boil for 20 minutes, and filter out. Mix 500mL of methanol and 500mL of water, add 5g of ammonium chloride and 30g of 3-mercaptopropyltrimethoxysilane, and stir evenly to obtain a post-treatment solution. Use NaOH to adjust the pH value of 1000mL water to 8, add 10g 3-glycidyl etheroxypropyl trimethoxysilane and 20g dodecyl trimethoxysilane dropwise under stirring, continue stirring for 10min, adjust the pH value of the solution with acetic acid to ...
Embodiment 3
[0036]Component A: DEGAROUTE®465 150g, titanium dioxide 100g, organobentonite 1.5g, vinyltriethoxysilane 25g, triethoxysilane 25g, 3-mercaptopropyltriethoxysilane 25g, Shuangfei powder 173.5g , a total of 500g. The preparation method is the same as in Example 1.
[0037] Component B: DEGAROUTE®659 250g, titanium dioxide 75g, organic bentonite 0.5g, dibenzoyl peroxide 25g, Shuangfei powder 149.5g, total 500g. The preparation method is the same as in Example 1.
[0038] Take glass microspheres and add them to aqueous hydrochloric acid solution with a pH value of 4, heat and boil for 30 minutes, and filter out. Mix 500mL of methanol and 500mL of water, add 5g of ammonium chloride and 50g of 3-mercaptopropyltrimethoxysilane, and stir evenly to obtain a post-treatment solution. Use NaOH to adjust the pH value of 1000mL water to 8, add 12.5g 3-glycidyl etheroxypropyl trimethoxysilane and 37.5g dodecyltrimethoxysilane dropwise under stirring, continue stirring for 15min, and adjus...
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