Liquid-core waveguide Raman spectrum detection device based on centrifuging

A Raman spectroscopic detection and liquid-core waveguide technology, applied in Raman scattering, material excitation analysis, etc., can solve problems such as poor performance, difficulty in removing bubbles from liquid-core waveguides, space obstruction, etc.

Pending Publication Date: 2017-05-10
BEIJING ABILITY TECH CO LTD
View PDF17 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] There are two ways to eliminate the bubbles in the tube. One is to use the centrifugal method, let the liquid core waveguide rotate around the axis, and use the increase in the buoyancy of the bubbles under the centrifugal condition of the liquid to achieve the removal of the bubbles. However, with the increase of the centrifugal force, The bubbles in the tube are rapidly increased by the pressure of the solution, the volume is continuously compressed, and the increase in buoyancy is not obvious. Coupled with the obstruction of the space, it is difficult to remove all the bubbles; another method is to use vacuum degassing method, such as the application number 201310415459.3 The Chinese invention patent proposes the use of negative pressure sampling to eliminate the air bubbles in the liquid core waveguide while feeding the liquid

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Liquid-core waveguide Raman spectrum detection device based on centrifuging
  • Liquid-core waveguide Raman spectrum detection device based on centrifuging
  • Liquid-core waveguide Raman spectrum detection device based on centrifuging

Examples

Experimental program
Comparison scheme
Effect test

example 1

[0042] Add 5 microliters of 10% ethanol solution to the liquid reservoir (i.e. the tapered positioning groove 311) on the sample disk (i.e. the pan head 31), rotate the sample disk at a speed of more than 500rpm so that the solution passes through the liquid reservoir and Fill the 10cm long Teflon AF tube (ie liquid core waveguide 4). The Raman signal of the 10% ethanol solution can be measured by inserting the Raman detection probe (i.e. the light source probe 21), and the signal strength is more than 50 times higher than the intensity measured in the cuvette, and the stability repeatability is good, indicating that the The device can effectively realize bubble-free sampling of liquids in Teflon AF tubes.

example 2

[0044] Add 100 microliters of DNA extraction solution to the liquid reservoir (i.e. the tapered positioning groove 311) on the sample disk (i.e. the disk head 31), and rotate the sample disk at a speed of more than 500rpm so that the solution passes through the liquid reservoir and is full of 20cm Long Teflon AF tube (ie liquid core waveguide 4). Connect the optical fiber receiving probe (i.e. light source probe 21) of 260nm LED light source to measure the absorption signal of DNA solution to 260nm light. All are good, indicating that the device can effectively realize the bubble-free sampling of liquid in Teflon AF tube.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention provides a liquid-core waveguide Raman spectrum detection device based on centrifuging. The liquid-core waveguide Raman spectrum detection device comprises a bracket, a multi-head spiral disc body and a light source probe translation stage, wherein the bracket is provided with a motor; the multi-head spiral disc body is fixed on the bracket and can horizontally rotate around a vertical rotary shaft of the motor; the multi-head spiral disc body comprises a disc head and a circular platform located below the disc head; the disc head is provided with a plurality of through holes; a positioning groove is formed in the upper part of each through hole; spiral channels, which have the quantity the same as that of the through holes, are opposite to the through holes, and are used for containing liquid-core waveguide tubes, are arranged on a side wall of the circular platform; the spiral channels are spirally diffused from top to bottom; the light source probe translation stage is fixed on the bracket, is located above the multi-head spiral disc body, and comprises a light source probe capable of moving linearly and a positioning mechanism matched with the positioning grooves; the positioning mechanism is located at the front end of the light source probe, can move forward along with the light source probe, and abuts against the positioning grooves.

Description

technical field [0001] The invention relates to a spectrum testing device, in particular to a device for obtaining a liquid-core waveguide with sufficient optical path and no bubbles by using a centrifugal method and performing Raman spectrum detection. Background technique [0002] Teflon AF has a lower refractive index than water, so when a pipe made of Teflon AF is filled with water or an aqueous solution, the interface between water and Teflon AF can meet the conditions of total reflection, and conduct light incident at a certain angle like an optical fiber. capability to form so-called liquid-core waveguides. Because the liquid core waveguide has a strong light guiding ability, a longer optical path can be obtained in it, so as to realize the sensitization of various optical detection technologies based on the principles of emission, absorption, fluorescence, and scattering, which is very good. Application prospect. [0003] For example, it can be used in the field of...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): G01N21/65
CPCG01N21/65
Inventor 张珊珊张东明张晓红
Owner BEIJING ABILITY TECH CO LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products