A super-tough abs masterbatch composite material
A composite material and masterbatch technology, applied in the field of polymer materials, can solve the problems of inability to meet the living needs of functional bathroom products, easy aging, and low temperature resistance.
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[0051] The preparation method of described modified ABS is as follows:
[0052] (1) Functionalized ABS
[0053] Add quantitative sodium pyrophosphate, anhydrous glucose and FeSO 4 After fully dissolving, add polybutadiene latex, adjust the pH value to 10, turn on the stirring device after purging with nitrogen, raise the temperature to 65°C, and continuously add styrene, acrylonitrile, glycidyl methacrylate, and isohydrogen peroxide dropwise. The monomer mixture of propylbenzene and tert-dodecyl mercaptan, continue to react for 1.5 hours after the dropwise addition, add antioxidant 1010, after demulsification, washing and filtration, dry at 100°C for 12 hours under reduced pressure;
[0054] (2) Functionalized ABS grafted sulfonated polyphenylene sulfide
[0055] Sulfonated polyphenylene sulfide: dissolve polyphenylene sulfide in concentrated sulfuric acid, the weight ratio of the polyphenylene sulfide to the concentrated sulfuric acid is 1: (10-20), react at 80°C-120°C for ...
Embodiment 1
[0098] A super-tough ABS masterbatch composite material, calculated in parts by weight, comprising the following raw materials:
[0099]
[0100] The preparation method of described super-tough ABS masterbatch composite material is as follows:
[0101] (1) Weigh the raw materials of each component according to the parts by weight, mix the ABS high rubber powder, modified ABS, and EMA compatibilizer, add it to a high-speed mixer, and stir at 90°C for 60 minutes;
[0102] (2) Add in step (1), add modified nano-calcium carbonate, photostabilizer and titanium dioxide, continue to stir for 40min, obtain mixed material; Described photostabilizer is 2,2 ', 4,4'-four Hydroxybenzophenone and 2-(2'-hydroxy-5'-methylphenyl)benzotriazole, the 2,2',4,4'-tetrahydroxybenzophenone and 2-(2 The weight ratio of '-hydroxy-5'-methylphenyl) benzotriazole is 1:0.3;
[0103] (3) Put the mixed material in step (2) into the twin-screw extruder, control the screw speed to 240r / min, and the tempera...
Embodiment 2
[0115] A super-tough ABS masterbatch composite material, calculated in parts by weight, comprising the following raw materials:
[0116]
[0117] The preparation method of described super-tough ABS masterbatch composite material, the preparation method of described modified ABS and the preparation method of described modified nano calcium carbonate are the same as embodiment 1; The grafting of described acrylic acid nano calcium carbonate grafted chitosan Branch rate is 2.3%.
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