Single-component photocuring composite with fluoride ion release property for dental restoration and application of composite
A technology for tooth restoration and composite materials, applied in dental prostheses, dentistry, dental preparations, etc., can solve the problem of unsustainable fluoride ion release, and achieve the effect of good physical and chemical properties
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Embodiment 1
[0034] Embodiment 1: The preparation method of the one-component light-cured dental restoration composite resin of formula 1
[0035] The final calculated one-component light-curing polymerized composite resin of formula 1 is as shown in the above table 1, and the actual preparation process of the composition of formula 1 is demonstrated in the following steps:
[0036] (1) Weigh 9.43 grams of HEMA-Phosphate, 3.44 grams of HEMA, and 12.3 grams of distilled water, place them together in a 100-ml capacity PP plastic beaker and mix to form an acidic aqueous solution, and use pH test paper to test the acidity of the solution , between pH=0-1;
[0037] (2) 24.83 grams of barium-calcium-F-Al-Si glass ionomer cement fillers whose average particle size is 4.5 microns are added in the acidic aqueous solution prepared in step (1), and are adjusted with dental polytetrafluoroethylene plastics Rapid blending: The mixture reacts quickly to thicken and form lumps, but the resulting lumps h...
Embodiment 2
[0042] Embodiment 2: The preparation method of the one-component light-curing dental restoration composite resin of formula 2
[0043] The final calculated one-component light-curing polymerized composite resin of formula 2 is as shown in the aforementioned table 1, but the actual preparation process of the composition of formula 2 is demonstrated in the following steps:
[0044] (1) Prepare a resin liquid according to the following material mixing ratio: 29.88 grams of 4-META, 39.17 grams of UDMA, 15 grams of HEMA, 14.83 grams of TEGDMA, 0.2 grams of CQ, 0.40 grams of EDMAB; test with pH test paper, the pH value is about 2.
[0045] (2) Take 80 grams of the resin liquid prepared in step (1), add 20 grams of distilled water, and make it mix to form a suspension mixture. Glass ionomer cement filler G018090 111 grams was then mixed in to form a thicker paste with a milky white color indicating excess water in the mixture.
[0046] (3) On the second day, the consistency of the w...
Embodiment 3
[0048] Embodiment 3: The preparation method of the one-component light-cured dental restoration composite resin of formula 3
[0049] The final calculated one-component photocurable polymerized composite resin of formula 3 is shown in the aforementioned Table 1, but the actual preparation process of the composition of formula 3 is demonstrated in the following steps.
[0050] (1) Similar to the step (1) of the above-mentioned Example 2, prepare a resin liquid with the following composition: 4-META 29.88 grams, UDMA 20 grams, BisGMA 19.17 grams, HEMA 15 grams, TEGDMA 14.23 grams, CQ 0.2 grams , EDMAB 0.40 grams; with pH test paper detection, the pH value is about 2.
[0051] (2) Take 1 gram of 4-META resin, add 2.2 grams of distilled water in a molar ratio of 1:36, and add absolute ethanol to a capacity of 50 ml to dissolve 4-META in the solution and convert it into an acid form (4- MET). Then add 25 grams of G18090 glass ionomer cement filler and continue to stir for 15 minu...
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