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Anti-wrinkle finishing agent and preparation and padding method

An anti-wrinkle finishing agent and finishing agent technology, which can be used in the processing of textile material equipment configuration, fiber processing, textile and paper making, etc.

Active Publication Date: 2019-04-09
河南嘉豪帽业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] 1. Formaldehyde will be released during use and storage, which will endanger people's health;
[0004] 2. After finishing, the fabric will be seriously yellowed;
[0005] 3. After finishing, the strength of the fabric is greatly reduced
However, there are also disadvantages of yellowing of the finished fabric and serious decline in strength during use.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] 1) React citric acid and glyoxal at a molar ratio of 1:6 at 40°C for 6 hours to prepare glyoxal-modified citric acid;

[0030] 2) Add 60 kg of glyoxal-modified citric acid, 2.0 kg of fatty alcohol polyoxyethylene ether, 10 kg of cross-linking agent, and 30 g of catalyst sodium nitrate into the container, and replenish the liquid to the liquid level of 1000L. Finishing agent;

[0031] 3) The padding finishing liquid adopts the process of two dipping and two rolling, and the excess rolling rate is 78%;

[0032] 4) The pre-baking temperature is 100°C, and the baking time is 2 minutes;

[0033] 5) Baking The baking temperature is 160°C, the baking time is 150s, and then the fabric is finished.

Embodiment 2

[0035] 1) React citric acid and glyoxal at a molar ratio of 1:6 at 40°C for 6 hours to prepare glyoxal-modified citric acid;

[0036] 2) Add 60 kg of glyoxal-modified citric acid, 2.0 kg of fatty alcohol polyoxyethylene ether, 10 kg of cross-linking agent, and 30 kg of catalyst sodium citrate into the container, and replenish the liquid to the liquid level of 1000L. Finishing agent;

[0037] 3) The padding finishing liquid adopts the process of two dipping and two rolling, and the excess rolling rate is 78%;

[0038] 4) The pre-baking temperature is 100°C, and the baking time is 2 minutes;

[0039] 5) Baking The baking temperature is 160°C, the baking time is 150s, and then the fabric is finished.

Embodiment 3

[0041] 1) React citric acid and glyoxal at a molar ratio of 1:6 at 40°C for 6 hours to prepare glyoxal-modified citric acid;

[0042] 2) Add 60 kg of glyoxal-modified citric acid, 2.0 kg of fatty alcohol polyoxyethylene ether, 10 kg of cross-linking agent, and 30 kg of sodium hypophosphite catalyst into the container, and add liquid to 1000L liquid level, and prepare the product Finishing agent;

[0043] 3) The padding finishing liquid adopts the process of two dipping and two rolling, and the excess rolling rate is 78%;

[0044] 4) The pre-baking temperature is 100°C, and the baking time is 2 minutes;

[0045] 5) Baking The baking temperature is 160°C, the baking time is 150s, and then the fabric is finished.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The invention discloses an anti-crease finishing agent as well as a preparation method and a padding method thereof, belonging to the technical field of fabric anti-crease finishing. The anti-crease finishing agent is characterized by consisting of 55-65g / L glyoxal modified citric acid, 1.3-2.6g / L fatty alcohol-polyoxyethylene ether, 6-15g / L crosslinking agent and 24-37g / L catalyst. The preparation method comprises the following steps: enabling citric acid and glyoxal in a molar ratio of 1 to (5.4-6.6) to react for 5.7-6.5h at 38-43 DEG C to obtain glyoxal modified citric acid; and preparing the anti-crease finishing agent according to the dosage. The application comprises a step of padding the finishing liquid, a pre-baking step and a baking step, wherein the baking time is 2-3min; and the baking temperature in the baking step is 140-180 DEG C, and the baking time is 1-3min. The product avoids the problem of formaldehyde release and does not harm human health.

Description

technical field [0001] The anti-wrinkle finishing agent and its preparation and padding method belong to the technical field of fabric anti-wrinkle finishing. Background technique [0002] N-methylolamide resin is a kind of anti-wrinkle finishing agent commonly used in industry. It is used for anti-wrinkle finishing of cellulose fiber fabrics and can obtain good anti-wrinkle effect. Among them, 2D resin is the most widely used. The fabric finished with 2D resin has good durable pressing finishing effect. But there are following defects: [0003] 1. Formaldehyde will be released during use and storage, which will endanger people's health; [0004] 2. After finishing, the fabric will be seriously yellowed; [0005] 3. After finishing, the strength of the fabric is greatly reduced. [0006] In the traditional treatment process, citric acid is also often used as an anti-wrinkle finishing agent. Citric acid has the advantages of safety, non-toxicity and low cost. However, th...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M13/207D06M15/53D06B3/18D06B23/22
CPCD06B3/18D06B23/22D06M13/207D06M15/53D06M2200/20
Inventor 张莉莉李顺涛申万意于子建
Owner 河南嘉豪帽业有限公司