Preparation method for environment-friendly corrosion-free wax-removing cleaning compound used for stainless steel
A non-corrosion, stainless steel technology, applied in the field of wax removal cleaning agent preparation, can solve the problems of low wax removal efficiency, corrosion of workpiece base material, poor decontamination ability, etc., achieve high wax removal efficiency, simple preparation steps, wax removal The effect of improving efficiency
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example 1
[0019] First, weigh 35g of soybean lecithin and 80mL of deionized water, add them to the reactor in turn, raise the temperature to 70℃, keep stirring at 300r / min for 1h, stir and let stand for stratification, remove the lower water phase, and collect the upper oil phase , Put it into a three-necked flask, and add 3g rice starch to the three-necked flask, then put the three-necked flask into a water bath, heat up to 40℃, stir at 60r / min for 30min; after the above-mentioned stirring is completed, add Add 60mL of deionized water to 70℃, stir for 1min, stir and transfer to ice water at 0℃, cool for 30min, put it in a centrifuge, centrifuge at 5000r / min to obtain a precipitate, freeze-dry it, Dry matter; Weigh 40g of the above dry matter and mix it with 85% sulfuric acid solution at a mass ratio of 1:10. Stir at 50°C for 80h, then suction filter to obtain a filter residue, wash with deionized water to neutral, and wash After drying, the natural emulsifier is obtained for use; then m...
example 2
[0022] First, weigh 40g of soybean lecithin and 90mL of deionized water, add them to the reactor in turn, heat up to 73°C, heat and stir at 350r / min for 2h, after stirring, let stand for stratification, remove the lower water phase, and collect the upper oil phase , Put it into a three-necked flask, and add 4g rice starch to the three-necked flask, then put the three-necked flask into a water bath, heat up to 43℃, stir at 70r / min for 40min; after the above-mentioned stirring is completed, add Add 65mL of deionized water to 70℃, stir for 2min, stir, transfer into ice water at 3℃, cool for 35min, put it in a centrifuge, centrifuge at 5500r / min to obtain a precipitate, freeze-dry it, Dry matter; Weigh 50g of the above dry matter and mix it with 85% sulfuric acid solution at a mass ratio of 1:10, stir at 55°C for 90h, and then suction filter to obtain a filter residue, wash with deionized water to neutral, and wash After drying, the natural emulsifier is obtained for use; then meas...
example 3
[0025] First, weigh 45g of soybean lecithin and 100mL of deionized water, add them to the reactor in turn, increase the temperature to 75℃, keep stirring at 400r / min for 2h, stir and let stand for stratification, remove the lower water phase, and collect the upper oil phase , Put it into a three-necked flask, and add 4g rice starch to the three-necked flask, then put the three-necked flask into a water bath, heat up to 45℃, stir at 80r / min for 50min; after the above-mentioned stirring is completed, add Add 70 mL of deionized water to 70 ℃, stir for 3 min, stir, transfer to 5 ℃ ice water, cool for 40 min, then put it in a centrifuge, centrifuge at 6000r / min speed to separate the precipitate, freeze-dry, get Dry matter; Weigh 60g of the above dry matter and mix it with 85% sulfuric acid solution at a mass ratio of 1:10, stir at 60°C for 100h, and then suction filter to obtain a filter residue, wash with deionized water to neutral, and wash After drying, the natural emulsifier is ...
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