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2275results about How to "Simple preparation steps" patented technology

Tungstic oxide nano-wire and method for preparing tungstic oxide nano-wire ammonia sensitive sensor

The invention relates to a tungsten oxide nano-wire ammonia-sensitive sensor and a preparation method thereof, belonging to the gas sensor technical field. The method comprises the following steps that: sodium tungstate is dissolved in deionized water to prepare a sodium tungstate solution; a hydrochloric acid and an oxalic acid are dripped slowly and stirred; a flaxen micellar solution is transferred into a reaction kettle, added with 25 to 30 grams of potassium sulfate and uniformly stirred, and the mixture undergoes hydrothermal treatment for 12 to 144 hours at a temperature of 180 DEG C; hydrothermal products are washed and fully dried in the presence of air with a temperature of 65 DEG C, and then a tungsten oxide nano-wire is prepared; adhesives and frit are added according to the tungsten oxide nano-wire prepared to prepare gas-sensitive materials slurry; and then the tungsten oxide nano-wire ammonia-sensitive sensor is prepared after element sintering and ageing. The method has simple steps, easily controlled parameters, and low energy consumption during the whole preparation process; the tungsten oxide nano-wire prepared has a large specific surface area; and the tungsten oxide nano-wire ammonia-sensitive sensor prepared has high sensitivity on low-concentration ammonia (between 1 and 100 pars per million), good repeatability and high stability.
Owner:TSINGHUA UNIV

A preparation method of a simple, low-cost, multi-channel microfluidic chemiluminescent paper chip and an on-site detection method by using the same

The present invention discloses a preparation method of a simple, low-cost, multi-channel microfluidic chemiluminescent paper chip and an on-site detection method by using the same. By using a full print mode, a plurality of multi-channel microfluidic chemiluminescent paper chips are printed out on a common A4-size filter paper in batch. The printing process includes: printing hydrophobic wax patterns in batch; melting wax for molding; printing chemiluminescent reagent ink patterns in batch; printing oxidase ink pattern in batch; cutting the microfluidic chemiluminescent paper chips into certain shape; and performing plastic package to the prepared microfluidic chemiluminescent paper chips. An on-site detection method by using the microfluidic chemiluminescent paper chip comprises the steps of: placing the plastic packaged microfluidic chemiluminescent paper chip into the cartridge of a handheld luminescent detector; dropwise adding a sample solution into the sample region; then covering the cartridge with a lid, and starting the test. The existence and contents of glucose, polyphenols, xanthine, cholesterol, uric acid, and hemoglobin are sequentially determined via the size of six chemiluminescence peaks sequentially appearing.
Owner:UNIV OF JINAN

Preparation method of ozone catalytic oxidation catalyst used for treating oil refining waste water

The invention relates to a preparation method of ozone catalytic oxidation catalyst used for treating oil refining waste water. Amorphous aluminium oxide powder and ferric hydroxide powder are mixed by dry basis weight ratio of 100: 1-30, and rolling pelleting, maintaining, drying and roasting are carried out, thus obtaining the finished product catalyst. The method includes the following steps: (a) amorphous aluminium oxide and ferric hydroxide powder are mixed to be uniform; (b) the mixture is placed into a rotary pelleting machine, binder is sprayed, and rolling pelleting is carried out, the binder is sprayed in solution or colloid form in an atomizing way, and the amount of binder sprayed into the pelleting machine is 2-50% of total mass of amorphous aluminium oxide; and diameter of pelleting is controlled to be 1-8mm; (c) particle matter is maintained for 3-24 hours under the condition that temperature of water vapour is 100-110 DEG C; (d) catalyst is dried, drying temperature is 50-180 DEG C, drying time is 2-10 hours, and then roasting is carried out; and roasting temperature of catalyst is 400-600 DEG C, roasting time is 2-8 hours, and finished product catalyst is obtained.
Owner:CHINA NAT OFFSHORE OIL CORP +2

Waterborne vacuum plastic-absorbing glue and preparing method thereof

The invention discloses a waterborne plastic-absorbing glue and a preparing method thereof. The waterborne plastic-absorbing glue is prepared from, by weight, 40-60 parts of aromatic aqueous polyurethane dispersion, 40-60 parts of ethylene-vinyl acetate emulsion, 0-10 parts of tackifying resin, 0.05-0.5 part of antifoaming agent, 0.1-1 part of wetting agent, and 0.1-1 part of thickening agent. The plastic-absorbing glue has excellent heat-resistant performance, pickup rate, bordure performance, low-temperature viscosity stability, and low activation temperature. The preparing method comprises the steps of adding aqueous polyurethane dispersion and ethylene-vinyl acetate emulsion into a high-speed dispersing kettle, then adding the tackifying resin, wetting agent, and antifoaming agent in sequence under a stirring condition, and finally adding the thickening agent to adjust the mixture into suitable viscosity to obtain the waterborne vacuum plastic-absorbing glue. According to the waterborne plastic-absorbing glue and the preparing method thereof, it is not necessary to adjust the pH of the ethylene-vinyl acetate emulsion in advance, and thus preparation procedures of traditional plastic-absorbing glue are simplified, and deslagging risks in the preparing process are lowered.
Owner:WANHUA CHEM GRP CO LTD

Tungstic oxide nano-wire and method for preparing tungstic oxide nano-wire gas-sensitive sensor

The invention relates to a method for preparing a tungsten oxide nano-wire and a tungsten oxide nano-wire ammonia-sensitive sensor, belonging to the one dimensional nano oxide material preparation and gas-sensitive technical field. The method comprises the following steps that: sodium tungstate is dissolved in deionized water to prepare a sodium tungstate solution; a hydrochloric acid is dripped slowly to prepare a flaxen micellar solution which is then centrifugally separated; products are uniformly dispersed in a potassium sulfate solution which is then transferred into a reaction kettle for hydrothermal reaction, and then the tungsten oxide nano-wire is prepared; adhesives and frit are added into the tungsten oxide nano-wire, and then the tungsten oxide nano-wire ammonia-sensitive sensor is prepared after element sintering and ageing. The method has simple steps, easily controlled technological parameters during the preparation process, and very low energy consumption during the whole preparation process; the tungsten oxide nano-wire prepared has a large specific surface area and high thermal stability; and the tungsten oxide nano-wire ammonia-sensitive sensor prepared has high sensitivity on low-concentration (between 1 and 100 pars per million) H2, CO and NH3, good repeatability and high stability.
Owner:TSINGHUA UNIV

Preparation method of linear water-based polyurethane thickener containing hydrophobic side bases

The invention relates to a linear water-based polyurethane thickener containing hydrophobic side bases and a preparation method of the linear water-based polyurethane thickener. The preparation method is characterized in that 40 weight percent to 60 weight percent of dibasic alcohol polymers, 10 weight percent to 30 weight percent of diisocyanate and 0 weight percent to 5 weight percent of catalysts are mixed, under the condition of N2 gas existence and the temperature being 50 DEG C to 100 DEG C, the stirring is carried out for 1 to 6 hours, then, 10 weight percent to 30 weight percent of end-capping agents are added, under the condition of the temperature being 50 DEG C to 100 DEG C, the stirring is carried out for 1 to 6 hours, polyurethane prepolymers are prepared, then, 5 weight percent to 20 weight percent of chain extenders are added into the prepared polyurethane prepolymers, the stirring is carried out for 1 to 6 hours under the condition of the temperature being 50 DEG C to 100 DEG C, and the linear water-based polyurethane thickener containing hydrophobic side bases is prepared. The linear water-based polyurethane thickener and the preparation method have the characteristics that no solvent exists, the toxicity is low, the environment is protected, the preparation process is simple, and the like. The prepared linear water-based polyurethane thickener containing hydrophobic side bases is applicable to the thickening of water-based paint, and the obvious thickening effect is realized.
Owner:LISHUI UNIV

Orderly arranged In2O3 nanofibers and application of same in preparation of ultra-fast response alcohol sensor

The invention belongs to the technical field of preparation of one-dimensional metal oxide nano-materials and semiconductor gas sensors therefrom, in particular relates to orderly arranged In2O3 nanofibers and application of same in preparation of an ultra-fast response alcohol semiconductor sensor. The process for preparing the orderly arranged In2O3 nanofibers comprises the following steps of: preparing a precursor solution from soluble nitrate, high polymer materials and a solvent; preparing orderly arranged composite nanofibers with a magnetic-field-induced electrostatic spinning technology; and performing high-temperature sintering to remove an organic high polymer template and further obtain the orderly arranged In(NO3)3 nanofibers. The alcohol gas sensor prepared from the orderly arranged In(NO3)3 nanofibers and a planar alumina substrate structure has the advantages that: the response time of the alcohol gas sensor to alcohol gas at the working temperature of 275 DEG C is 0.4 s, and the recovery time is 3 s; and the reversibility and repeatability of the sensor are good and far superior to the traditional alcohol sensor made of nano-powder materials of the same type. In the invention, the advantages of simple process, low cost and high yield are achieved.
Owner:JILIN UNIV

Photo-cured medical catheter hydrophilic lubrication coating and preparation method thereof

The invention discloses a photo-cured medical catheter hydrophilic lubrication coating and a preparation method thereof. The hydrophilic lubrication coating comprises a bottom coating and a lubrication coating, wherein the bottom coating is attached to the surface of an instrument, and the lubrication coating is attached to the bottom coating. The bottom coating comprises 1-10 parts of polyester acrylate, 50-90 parts of solvents, 0.5-5 parts of photoinitiators, 0.5-2 parts of wetting agents and 0.5-5 parts of reactive diluents; the lubrication coating comprises 1-10 parts of water soluble macromolecules, 1-5 parts of crosslinking macromolecules, 0-1 part of photoinitiators, 0.1-1 part of surfactants and 50-98 parts of mixed solvents. The preparation method of the hydrophilic lubrication coating is simple and easy in operation, substance residues caused by complicated high-temperature chemical reaction are avoided, the cured coating forms a crosslinking structure, has good adhesion on the surface of a medical catheter and has excellent and lasting lubricity in an aqueous medium, the friction coefficient of the surface of the medical catheter is reduced, and harm to human tissues andadhesion of macromolecules in blood are decreased.
Owner:ORBUSNEICH MEDICAL SHENZHEN CO LTD

Microtube device and using method thereof

The invention relates to a microtube device and a using method thereof. The microtube device is characterized by comprising an upper layer of top cap layer and a lower layer of substrate layer, wherein the top cap layer is tightly connected with the surface of the substrate layer; the top cap layer and / or the substrate layer are / is provided with a branch microtube; the branch microtube consists of at least one activity screening tube, a buffer cavity and at least two branch tubes which are symmetrically distributed to the center of the buffer cavity; the buffer cavity is connected with the activity screening tube and the branch tube; meanwhile, the top cap layers corresponding to all the end positions of the branch microtube are provided with a hole respectively to form a sample inlet pool and a sample outlet pool; the sample inlet pools are communicated with the corresponding activity screening tube respectively; and the sample outlet pools are communicated with the corresponding branch tubes respectively. Cells can be cultured in situ in the sample outlet pool and can continuously generate a chemotactic matter by selectively adding cells capable of releasing the chemotactic matter into one or more sample outlet pools, so that uniform and stable chemical gradient fields are generated in the buffer cavity and the branch tubes. The microtube device has the advantages of simple manufacturing steps, low cost, quick and effective screening process, and easy popularization and use in ordinary laboratories.
Owner:CAPITALBIO CORP +1

Dimethyl carbonate supported catalyst directly synthesized by methanol and carbon dioxide

The invention discloses a dimethyl carbonate supported catalyst directly synthesized by methanol and carbon dioxide and a preparation method and a use method. The catalyst adopts diatomite as carrier, transition metal copper and nickel as main components of active components and zinc, iron, cobalt and the like as additives, wherein, the weight percent of diatomite in the catalyst is 60-95%, the weight percent of the transition metals is 5-30% and the weight percent of the additives is 0-15%. The preparation method comprises the following steps: soaking the carrier in a mixed solution of soluble transition metal salt and the additives, dispersing with ultrasound, evaporating and drying, calcining and reducting with hydrogen to obtain the supported catalyst. The use method comprises the following steps: placing the catalyst in a reaction device, adjusting the molar ratio of gas phase methanol to carbon dioxide to 2:1-3:1, and performing a reaction at 110-140 DEG C under the pressure of 0.6-3.0 MPa. The catalyst has the advantage of simple preparation steps, good stability and high catalytic efficiency and overcomes the defect that the carrier used by the existing catalyst needs be processed through complicated steps for pretreatment and has high price and instable catalytic performance.
Owner:SUN YAT SEN UNIV

Micro-fluidic apparatus integrated with PDMS film, manufacturing method and application thereof

The invention relates to a micro-fluidic apparatus integrated with a polydimethyl siloxane (PDMS) film, which is structurally characterized in that a flat glass sheet is pasted with a PDMS sheet, the pasting face of the PDMS sheet and the glass is provided with a groove to form a micro-fluidic pipeline, the surface of the PDMS sheet on the upper part of the central position of the micro-fluidic pipeline is a concave spherical surface, the thickness of the PDMS sheet between the lowest point of the concave spherical surface and the micro-fluidic pipeline is less than or equal to 10 microns, the PDMS sheet at two ends of the micro-fluidic pipeline is respectively provided with pores, and the pores are communicated with the micro-fluidic pipeline so as to form a fluid storage tank. The micro-fluidic apparatus can be applied to experiments such as film evaporation and crystallization or biological molecule concentration and the like in a micro-fluidic system. Special equipment is not needed to manufacture the micro-fluidic apparatus, the manufacturing step is simple, the cost is low, and the micro-fluidic apparatus is easily popularized and used in common laboratories. The invention also discloses a method for manufacturing the micro-fluidic apparatus.
Owner:NANJING UNIV

Preparation of nitrogen-doped orderly-graded mesoporous carbon catalyst as well as carbon catalyst and application of carbon catalyst

The invention discloses a preparation method of a nitrogen-doped orderly-graded mesoporous carbon catalyst and application of the nitrogen-doped orderly-graded mesoporous carbon catalyst to proton exchange membrane fuel cells. The catalyst is prepared though a binary mixing template method; a triblock copolymer is used as a soft template agent and one or more of a Y-type molecular sieve, an MCM-41 molecular sieve and a ZSM-5 molecular sieve are used as a hard template agent; soluble resin is used as a carbon source; in a preparation process, a transition metal salt is added and a transition metal element is introduced in situ; meanwhile, a nitrogen element is introduced through roasting in an ammonia atmosphere. The nitrogen-doped orderly-graded mesoporous carbon material provided by the invention has an ordered mesoporous structure (with the size of 3nm to 5nm) generated by soft template induction and a three-dimensional through mesoporous structure (with the size of 10nm to 50nm) generated by hard template etching, has a high-activity specific surface and good mass-transferring performance and has excellent oxygen reduction catalysis performance and good electrochemical stability. By adopting the carbon material provided by the invention, application of the binary mixing template method to preparation of an oxygen reduction carbon-based catalyst is realized for the first time; meanwhile, the carbon material has the advantages of good process repeatability, low cost, good environmental friendliness and the like.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI
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