A kind of UV photosensitive negative pure acrylic photoresist and preparation method thereof
A technology of photoresist and pure acrylic, which is applied in the direction of optomechanical equipment, photosensitive material processing, optics, etc., can solve the problems of low resolution, unfavorable human health, etc., and achieve good permeability, small diffraction effect, and large contrast Effect
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example 1
[0034] Example 1, add respectively 15 Kg of styrene, 30 Kg of methyl methacrylate, 3 Kg of n-butyl methacrylate, 7.5 Kg of azobisisobutyronitrile and 9 Kg of isobornyl acrylate in drip irrigation, and stir at room temperature for 0.8 Hour; In reactor, add propylene glycol methyl ether acetate 64.5Kg, stir and its temperature rises to 90 DEG C; The mixed solution in drip irrigation is dripped in reactor, after dripping completes, insulation reaction waits for system acid value After cooling to normal temperature after 65°C, 129Kg of light yellow finished acrylated polyacrylic acid resin was obtained.
example 2
[0035] Example 2: After adding 18Kg of styrene, 37.5 Kg of methyl methacrylate, 7.5 Kg of n-butyl methacrylate, 12 Kg of azobisisobutyronitrile and 13.5Kg of isobornyl acrylate in drip irrigation, stir at room temperature for 0.8 Hour; In reactor, add propylene glycol methyl ether acetate 97Kg, stir and its temperature rises to 90 DEG C; The mixed solution in drip irrigation is dripped in reactor, after dripping, insulation reaction treats system acid value After 65°C, the temperature was lowered to normal temperature to obtain 185.5 Kg of light yellow finished acrylated polyacrylic acid resin.
example 3
[0036] Example 3. Add 60Kg of styrene, 150 Kg of methyl methacrylate, 30 Kg of n-butyl methacrylate, 48 Kg of azobisisobutyronitrile and 54Kg of isobornyl acrylate in drip irrigation, and then stir at room temperature for 0.8 hours Add propylene glycol methyl ether acetate 388Kg in reactor, stir and its temperature rises to 90 DEG C; The mixed solution in drip irrigation is dripped in reactor, and insulation reaction treats that system acid value is 65 after dripping completes After cooling down to normal temperature, 730Kg of light yellow finished product acrylated polyacrylic acid resin was obtained.
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