A kind of polyurethane soft foam anti-yellowing agent
A polyurethane soft foam and anti-yellowing technology, which is applied in the field of polyurethane, can solve the problems of polyurethane soft foam aging, appearance deformation, and insignificant anti-yellowing effect
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[0053] The second aspect of the present invention provides a kind of preparation method of polyurethane soft foam anti-yellowing agent, comprising:
[0054] (1) Stir the powdery hindered phenol antioxidant, ultraviolet absorber and heat stabilizer evenly to obtain a solid mixture;
[0055] (2) Deep processing the solid mixture in (1) by means of grinding or hot melting;
[0056] (3) Add liquid phosphite to the mixture in step (2) and stir evenly to obtain the product.
[0057] In a preferred embodiment, the preparation method of yellowing agent for flexible polyurethane foam is as follows:
[0058] (1) The liquid components are divided into three groups according to their properties: liquid heating group, liquid grinding group and final addition group. The powdered components are divided into two groups according to their properties: powder heating group and powder grinding group.
[0059] (2) Heat the liquid heating group in step 1 to a suitable temperature, slowly add the...
Embodiment 1
[0072] Preparation of polyurethane soft foam anti-yellowing agent:
[0073] Heat 10g of hindered phenol antioxidant β-(3,5-di-tert-butyl-4-hydroxyphenyl) isooctyl propionate to 100°C, add triethylene glycol bis[β -(3-tert-butyl-4-hydroxyl-5-methylphenyl) propionate] 0.5g, hydroxylamine 0.3g, cool to room temperature, then add fluorescent whitening powder and other powdery components, using a three-roll mill After grinding, add 10 g of phosphite triphenyl phosphite and 2 g of ultraviolet absorber N'-methyl-N'-phenylformamidine and stir evenly to obtain the anti-yellowing agent.
[0074] Preparation of polyurethane soft foam:
[0075] At room temperature, the prepared anti-yellowing agent (5g) was added to polyoxypropylene glycol 100g, deionized water 7g, MC foaming agent 6.5g, silicon surfactant 6.5g, amine catalyst A-33 (2.8g) Stir rapidly for 150s. Add TDI80 / 20 (140g) to the above mixed solution, pour the mixed solution into a mold at 75°C for foaming, stop foaming whe...
Embodiment 2
[0077] Preparation of polyurethane soft foam anti-yellowing agent:
[0078] 10g of hindered phenol antioxidant β-(3,5-di-tert-butyl-4-hydroxyphenyl) isooctyl propionate, 2g of ultraviolet absorber N'-methyl-N'-phenylformamidine, Hydroxylamine 0.3g, fluorescent whitening agent 1g, after stirring and mixing, after adopting three-roller grinder to grind, obtain the anti-yellowing agent precursor, add phosphite poly(dipropylene glycol) phenyl phosphite 10g and stir and mix, namely Resistant to yellowing agents.
[0079] The preparation method of the flexible polyurethane foam is prepared with reference to the method in Example 1.
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