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Preparation method of low-temperature composite foam glass

A composite foam and glass technology, which is applied in glass manufacturing equipment, glass molding, manufacturing tools, etc., can solve the problems of excessive heating rate, insufficient heat preservation time, and low mechanical strength, so as to reduce surface tension and compressive strength Improve the effect of fine pore structure

Inactive Publication Date: 2018-01-19
薛向东
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The technical problem mainly solved by the present invention is that the preparation temperature is too high, the holding time is insufficient, the heating rate is too fast and other reasons lead to the generation of large bubbles, easy hole connection, low mechanical strength and poor water resistance in the current common foam glass materials. etc., thereby affecting the defects of the use range of foam glass, a preparation method of low-temperature composite foam glass is provided

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 3

[0022] Example 3 Add 5 g of boric acid to 125 ml of sodium silicate solution with a mass fraction of 30%, and stir and mix for 100 min at a speed of 3000 r / min to obtain a high-viscosity liquid sol; then add 100 ml of castor to the liquid sol Sesame oil and continue to stir for 60 minutes to obtain a fermentation substrate, then add 10 g of fresh grape skins of the fermentation substrate to the fermentation substrate, stir for 15 minutes, put it into a fermenter, and seal and ferment at 33°C for 10 days to obtain a fermentation product; The product was dried at 110° C. to obtain a composite solid sol with a moisture content of 55%, and 50 g of limestone and 50 g of borax were added to the composite solid sol, and mixed to obtain a mixed sol; the above mixed sol was packed into a mold with a size of 90mm×70mm×40mm, Move the sealed mold into an oven, preheat at 100°C for 10 minutes, then place the mold in an oven at 300°C for 2.5 hours of heat preservation and foaming, then cool ...

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Abstract

The invention discloses a preparation method of low-temperature composite foam glass and belongs to the technical field of foam glass preparation. The preparation method comprises adding boric acid into a sodium silicate solution, carrying out uniform mixing to obtain high-viscosity liquid sol in the premise of no gelling, then adding a vegetable oil emulsion into a solution, carrying out uniformstirring, adding fermented broth obtained by fresh grape skin fermentation into the solution, adding the fermented broth into the liquid sol, drying the composite liquid sol to obtain composite solidsol, adding limestone as a foaming agent into the sol, adding borax as a cosolvent into the sol, uniformly mixing the sol, foaming agent and borax to obtain mixed sol, designing unit weight of 260-270kg / m<3>, putting the fine composite solid sol corresponding to the designed unit weight into a mold, sealing the mold, transferring the sealed mold into a heating device, carrying out preheating, carrying out melting heat-preservation foaming in an oven, carrying out cooling to the room temperature and carrying out annealing and demolding to obtain the low-temperature composite foam glass.

Description

technical field [0001] The invention discloses a method for preparing low-temperature composite foam glass, which belongs to the technical field of foam glass preparation. Background technique [0002] Foam glass is a kind of waste flat glass and bottle glass as raw materials, adding foaming agent, modified additive and foaming accelerator, etc., after finely pulverizing and uniformly mixing, then melting at high temperature, foaming and annealing. Inorganic non-metallic glass materials. It is composed of a large number of uniform bubble structures with a diameter of 1 to 2 mm. Among them, the sound-absorbing foam glass is more than 50% open-cell bubbles, and the heat-insulating foam glass is more than 75% closed-cell bubbles. The product density is 160-220 kg / m3, which can be adjusted by changing the production technical parameters according to the requirements of use. . [0003] Foam glass is a light-weight and high-strength building material and decoration material wit...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C11/00C03B19/08
Inventor 李华何俊欣陈莉莉
Owner 薛向东
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